chromatography and spectroscopy

Transcription

1 chromatography and spectroscopy consumables and spare parts

2 table of contents chromatography Table of contents 1. Syringe filter units 2. Titan syringe filter 3. Target syringe filter 4. Solid phase extraction (SPE) by Macherey-Nagel 5. Thin layer chromatography (TLC) 6. Tablet Dissolution Accessories 7. Sampling Cannulae 8. Vessels 9. Paddles 10. Baskets 11. Capsule Spiral Sinkers 12. Basket sinkers 13. Sample bottles, micro inserts and closures for HPLC 14. Sample bottles and closures for GC 15. Crimping tools 16. Storage system for HPLC and GC columns 17. Guard columns by Altmann Analytik 18. HPLC columns by Altmann Analytik 19. Akzo Nobel Kromasil Columns 20. Chiral columns by Daicel 21. HPLC columns by Grace 22. HPLC columns by Macherey-Nagel 23. SIELC columns 24. Tubing and Fitting by Upchurch 25. Storage System Consumables 26. Degasser 27. Safety caps/waste cap accessories 28. Deuterium lamps for the HPLC laboratory 29. Tungsten lamps for the HPLC laboratory 30. Lamps for Atom Absorption Spectroscopy (AAS) 31. Graphite Tubes by Altmann Analytik 32. Cuvettes 33. Agilent alternative replacement parts 34. Shimadzu alternative replacement parts 35. Waters alternative replacement parts 36. GC/HPLC-Syringes by Hamilton 37. Manual Syringes 38. GC syringes by SGE 39. Ferrules by SGE 40. GC columns by SGE 41. GC columns by Macherey-Nagel p. 2-3 p. 4-5 p. 5-6 p. 7-8 p p p p p p p. 23 p. 24 p p p p. 36 p p p p p p p p p. 60 p. 61 p. 62 p. 63 p. 64 p p p. 68 p. 69 p. 70 p p p p p p p page 1

3 syringe filter units 1. Syringe filter units always in stock Syringe filters are used for filtration of suspended matter from liquid sample or gases. Rapid purification and removal of particles is very simple: just place the filter on a syringe, and you are ready for filtration. Contamination of sensitive instrumentation by solid impurities can be avoided. Also the lifetime of chromatographic columns and equipmend can be increased. membrane pore size membrane diameter 3 mm 15 mm 25 mm CA 0,2 µm - CA CA ,45 µm - CA CA PA 0,2 µm PA PA PA ,45 µm PA PA PA PES 0,2 µm - - PES ,45 µm - - PES PET 0,2 µm - PET PET ,45 µm - PET PET GF/PET 1,0/0,2 µm - - PETGF ,0/0,45 µm - - PETGF PTFE 0,2 µm PTFE PTFE PTFE ,45 µm PTFE PTFE PTFE PVDF 0,2 µm - PVDF PVDF ,45 µm - PVDF PVDF GF/PVDF 1,0/0,45 µm - - PVDFGF RC 0,2 µm - RC RC ,45µm - RC RC GF/RC 1,0/0,2 µm - - RCGF ,0/0,45 µm - - RCGF GF 1,0 µm - GF GF page 2

4 syringe filter units Selection of the appropriate filter FILTER SIZE: sample volume ml 1-5 ml <1 ml Filter size 25 mm Diameter mm Diameter 3 mm Diameter PORE SIZE: general applications, hplc columns with >3 µm particles uhplc, core-shell and hplc columns with <3 µm particles 0,45 µm 0,2 µm TYPE OF MEMBRANE: properties of the samples membrane type i membrane type ii membrane type iii Aqueous, polar, hydrophilic with low particle load PET RC Aqueous, polar, hydrophilic with high particle load GF/PET GF/RC Semi-polar, e.g. HPLC eluents PET PA RC Sample contains proteins (low bonding capacity of the proteins) Sample contains proteins (high bonding capacity of the proteins) CA PVDF PES GF GF/PET GF/PVDF Strongly acidic or alkaline PTFE Organic, non-polar, hydrophobic with low particle load PTFE PET Organic, non-polar, hydrophobic with high particle load GF/PET GF/PVDF page 3

5 titan syringe filter 2. Titan syringe filter TITAN SYRINGE FILTER NYLON use for: general laboratory filtration filtration for most HPLC samples art.no. description pore size diameter (mm) pack size TF42204-NN Titan Syringe Filter, NYLON 0,2 µm TF44504-NN Titan Syringe Filter, NYLON 0,45 µm TF42213-NN Titan Syringe Filter, NYLON 0,2 µm TF44513-NN Titan Syringe Filter, NYLON 0,45 µm TF42225-NN Titan Syringe Filter, NYLON 0,2 µm TF44525-NN Titan Syringe Filter, NYLON 0,45 µm TF41225-NN Titan Syringe Filter, NYLON 1,5 µm TF45025-NN Titan Syringe Filter, NYLON 5 µm TITAN SYRINGE FILTER PTFE use for: filtration of aggressive organic, highly basic or hot solutions filtering of aqueous solutions after prewetting with an alcohol art.no. description pore size diameter (mm) pack size TF42204-NP Titan Syringe Filter, PTFE 0,2 µm TF44504-NP Titan Syringe Filter, PTFE 0,45 µm TF42213-NP Titan Syringe Filter, PTFE 0,2 µm TF44513-NP Titan Syringe Filter, PTFE 0,45 µm TF42225-NP Titan Syringe Filter, PTFE 0,2 µm TF44525-NP Titan Syringe Filter, PTFE 0,45 µm TITAN SYRINGE FILTER PVDF use for: general biological filtration filtration of samples where high protein recovery is desired art.no. description pore size diameter (mm) pack size TF42204-PV Titan Syringe Filter, PVDF 0,2 µm TF44504-PV Titan Syringe Filter, PVDF 0,45 µm TF42213-PV Titan Syringe Filter, PVDF 0,2 µm TF44513-PV Titan Syringe Filter, PVDF 0,45 µm TF44525-PV Titan Syringe Filter, PVDF 0,45 µm Please note: Other Dimensions are also available! page 4

6 titan syringe filter/target syringe filter TITAN SYRINGE FILTER RC use for: low non-specific binding applications tissue culture media and general biological sample filtration art.no. description pore size diameter (mm) pack size TF52213-RC Titan Syringe Filter, RC 0,2 µm TF54513-RC Titan Syringe Filter, RC 0,45 µm TF52225-RC Titan Syringe Filter, RC 0,2 µm TF54525-RC Titan Syringe Filter, RC 0,45 µm TITAN SYRINGE FILTER CA use for: tissue culture media filtration, sensitive biological samples art.no. description pore size diameter (mm) pack size TF42204-CA Titan Syringe Filter CA 0,2 µm TF44502-CA Titan Syringe Filter CA 0,45 µm TF42213-CA Titan Syringe Filter CA 0,2 µm TF44513-CA Titan Syringe Filter CA 0,45 µm TF42225-CA Titan Syringe Filter CA 0,2 µm TF44525-CA Titan Syringe Filter CA 0,45 µm Target syringe filter TARGET SYRINGE FILTER PVDF use for: general biological filtration filtration where high protein recovery is desired art.no. description pore size diameter (mm) pack size TFF PVDF Target Syringe Filter 0,45 µm TFF PVDF Target Syringe Filter 0,2 µm TARGET SYRINGE FILTER RC use for: low non-specific binding applications Tissue culture media and general biological sample filtration art.no. description pore size diameter (mm) pack size TFF RC Target Syringe Filter 0,45 µm TFF RC Target Syringe Filter 0,2 µm page 5 Please note: Other Dimensions are also available!

7 target syringe filter WHAT IS THE DIFFERENCE BETWEEN TITAN3 AND TARGET2 SYRINGE FILTERS? both titan3 and target2 provide: High-quality filtration solutions Low extractable membranes and housing HPLC performance tested Plain polypropylene housing titan3 is the premium brand that provides: Even higher levels of confidence from stronger housing that prevents leakage and busting 30 mm products pressure rated to 120 psi Most 30 mm devices are provided with a 1 mm boro silicate glass pre-filter (delivering increased filtrate volumes) Color coding for easy identification and selection of the correct membrane and pore size 30mm products pressure rated to 100 psi Enhanced Luer Lock inlet which provides secure attachment to syringes Range of filter sizes from 4 mm to 30 mm Low hold-up volume allows for the treatment of small sample volumes with minimal sample loss TARGET SYRINGE FILTER AND TITAN SYRINGE FILTER page 6

8 solid phase extraction (spe) by macherey-nagel 4. Solid phase extraction (SPE) by Macherey-Nagel Solid-phase extraction (SPE) is a powerful method for sample preparation that is used today in most laboratories. The SPE shows its performance in a wide range of applications: environmental analysis, pharmaceutical analysis, organic chemistry and food analysis. SPE is used for three important tasks: enrichment of the analyte, removal of interfering components and change of the matrix of the analyte. Advantages of the SPE in comparison to classical liquid-liquid extraction: 1. Reduced consumption of solvents 2. Great time-saving 3. Possibility of automation 4. High continuity in individual sample handling CHROMABOND VACCUM CHAMBER AND ACCESSORIES: article art.no. description quantity Complete vacuum chamber for up to 12 columns or cartridges MN Glass 1 Stainless steel connectors MN to avoid cross contamination 12/PAK PTFE-connectors MN to avoid cross contamination 12/PAK CHROMABOND C18 EC POLYPROPYLENE COLUMNS: Base material silica gel, pore diameter 60 angström, particle size 45 µm, ph stability 2-8. Recommended use: aflatoxins, amphetamines, antibioatics, antiepileptics, barbiturates, caffeine, drugs, preservatives, fatty acids, nicotine, PAHs, pestiacides, PCBsa, heavy metals, vitamins. volume filling quantity packaging unit 100 mg 200 mg 500 mg 1 g 2 g 1 ml MN ml MN MN ml MN MN MN ml MN page 7 Please note: Other Dimensions are also available!

9 solid phase extraction (spe) by macherey nagel art.no. article description packing unit MN C18 ec Propylene column, SPE PP, 100 mg, 1 ml 100 MN C18 ec Propylene column, SPE PP, 200 mg, 3 ml 50 MN C18 ec Propylene column, SPE PP, 500 mg, 3 ml 50 MN C18 ec Propylene column, SPE PP, 500 mg, 6 ml 30 MN C18 ec Propylene column, SPE PP, 1000 mg, 6 ml 30 MN C18 ec Propylene column, SPE PP, 2000 mg, 6 ml 30 MN C18 ec Propylene column, SPE PP, 2000 mg, 15 ml 20 KIESELGUHR PHASE FOR LIQUID-LIQUID EXTRACTION Basic material coarse-grained kieselguhr, large pore width, high pore volume, ph range Liquid-liquid extraction of highly viscous and aqueous solutions such as, for example, dyes in textiles or in environmental and food analysis without the use of a separation funnel. Fast, reproducible and cost-saving, high recovery rates. art.no. article description packing unit MN Chromabond XTR PP, 1000 mg, 6 ml 30 MN Chromabond XTR PP, 3000 mg, 15 ml 30 MN Chromabond XTR PP, 4500 mg, 30 ml 30 MN Chromabond XTR PP, 8300 mg, 45 ml 30 MN Chromabond XTR PP, mg, 70 ml 30 Please note: Other Dimensions are also available! page 8

10 thin layer chromatography (tlc) 5. Thin layer chromatography (TLC) The principle of TLC is known for over 100 years. TLC is still a popular technique in the laboratory for reaction, quality and identity control. Advantages of TLC are: High sample throughput possible in a short time No complex sample preparation required Simple method without expensive instruments IMPLEMENTATION OF A TLC SEPARATION SELECTION OF THE SOLVENT: The solvent is selected by elution strength. The most appropriate solvent can be determined very easily. SAMPLE APPLICATION: A common method is to use a glass capillary to place a point or a short line on the TLC plate. The placement of the substance has to be narrow, because, if the point or line is too broad this leads to a poor separation, since the zones become broader while processing. After application, the solvent is allowed to evaporate, this can be accelerated by the use of a heat gun. DEVELOPMENT: A common method is to use a developing chamber. The eluent is filled into the bottom of the chamber. For a reproducible running distance, the saturation of the chamber with the running medium vapor is necessary. Then the TLC plate with the sample is positioned in the chamber. The separation is completed when the eluent has ascended to the upper end of the TLC plate. The TLC plate can now be removed and dried accordingly. EVALUATION: The evaluation depends on the aim of the chromatographic analysis. In the case of qualitative determinations, it must be allowed to run alongside the simplest comparative substances. Quantitative evaluations are possible via appropriate calibration measurements. In this case, the area of the substance spots is used or a photometric evaluation is carried out on the layer. In the case of the latter, however, the complexity of the apparatus is greater. page 9

11 thin layer chromatography (tlc) TLC CONSUMABLES AND PLATES FROM MERCK art.no. description quantity MC TLC silica gel 60 Alu foil 20 x 20 cm 25 MC TLC silica gel 60 F254 Alu foil 20 x 20 cm with fluorescent indicator 25 MC TLC silica gel 60 F254 Alu foil 10 x 20 cm with fluorescent indicator 25 MC TLC cellulose glass plate 20 x 20 cm 25 MC UV-lamp 254 nm for thin layer chromatography 1 TLC CONSUMABLES FROM MACHEREY NAGEL art.no. description quantity MN TLC-developing chamber 10x10 cm 1 MN TLC-developing chamber 20x20 cm 1 MN Glas capillary, 1 μl 150 MN Small rubber hats for capillaries 2 MN Application template 2 TLC PLATES FROM MACHEREY NAGEL Alugram SilG: unmodified standard silica layers for TLC; Silica 60, particle size 5-17 µm art.no. description quantity MN TLC plates ALUGRAM SIL G, 5x7,5 cm 20 MN TLC plates ALUGRAM SIL G, 5x10 cm 50 MN TLC plates ALUGRAM SIL G/UV254, 4x8 cm with fluorescent indicator 50 MN TLC plates ALUGRAM SIL G/UV254, 5x10 cm with fluorescent indicator 50 ALUGRAM XTRA SIL G unmodified standard silica layers on aluminium for TLC; Silica 60; 5-17 µm, outstanding wettability, improved cutting properties art.no. description quantity MN TLC plates ALUGRAM Xtra SIL G, 5x10 cm 50 MN TLC plates ALUGRAM Xtra SIL G/UV254, 5x10 cm with fluorescent indicator 50 MN TLC plates ALUGRAM Xtra SIL G, 20x20 cm 25 MN TLC plates ALUGRAM Xtra SIL G/UV254, 20x20 cm with fluorescent indicator 25 MN TLC plates ALUGRAM Xtra SIL G/UV254, 4x8 cm with fluorescent indicator 50 ADAMANT unmodified standard silica layers for TLC, Silica 60; 5-17 µm, improved binder system; optimized particle size distribution art.no. description quantity MN TLC plates ADAMANT, 0,25 mm, 10x10 cm 25 MN TLC plates ADAMANT UV254, 0,25 mm, 10x10 cm with fluorescent indicator 25 Please note: Other Dimensions are also available! page 10

12 tablet dissolution accessories 6. Tablet Dissolution Accessories CANNULA FILTER: Filters are important to hold back particles of the tablet. All filters are USP compliant. By using cannula filters the hydrodynamics in the vessel may be affected, advantage is the large surface area. If high particulates are present blockage of sample probes can be prevented, due to the high flowrate. There are different porosity ranges available. For different manufacturers different filters are recommended, they are not interchangeable due to the differences in diameter. For some manufacturers also filter discs or filter tips are available. CANNULA FILTER DISTEK Distek baths normally use 1/16 cannula style filters with a large range of porosities. art.no. description pore size pack size oem reference QLFIL10S-DK Cannula Filter, UHMW Polyethylene 10 µm QLFIL10S-DK-a Cannula Filter, UHMW Polyethylene 10 µm QLFIL20S-DK Cannula Filter, UHMW Polyethylene 20 µm QLFIL20S-DK-a Cannula Filter, UHMW Polyethylene 20 µm QLFIL35S-DK Cannula Filter, UHMW Polyethylene 35 µm QLFIL35S-DK-a Cannula Filter, UHMW Polyethylene 35 µm QLFIL45S-DK Cannula Filter, UHMW Polyethylene 45 µm QLFIL45S-DK-a Cannula Filter, UHMW Polyethylene 45 µm QLFIL70S-DK Cannula Filter, UHMW Polyethylene 70 µm QLFIL70S-DK-a Cannula Filter, UHMW Polyethylene 70 µm CANNULA FILTER ERWEKA Erweka baths normally use 1/8 (3.2 mm) cannula style filters with a large range of porosities. art.no. description pore size pack size oem reference QLFIL001-EW Cannula Filter, Erweka, UHMW Polyethylene 1 µm QLFIL001-EW-a Cannula Filter, Erweka, UHMW Polyethylene 1 µm QLFIL004-EW Cannula Filter, Erweka, UHMW Polyethylene 4 µm QLFIL004-EW-a Cannula Filter, Erweka, UHMW Polyethylene 4 µm QLFIL010-EW Cannula Filter, Erweka, UHMW Polyethylene 10 µm QLFIL010-EW-a Cannula Filter, Erweka, UHMW Polyethylene 10 µm QLFIL020-EW Cannula Filter, Erweka, UHMW Polyethylene 20 µm QLFIL020-EW-a Cannula Filter, Erweka, UHMW Polyethylene 20 µm QLFIL035-EW Cannula Filter, Erweka, UHMW Polyethylene 35 µm 1000 QLFIL035-EW-a Cannula Filter, Erweka, UHMW Polyethylene 35 µm 100 QLFIL040-EW Cannula Filter, Erweka, UHMW Polyethylene 40 µm 1000 QLFIL040-EW-a Cannula Filter, Erweka, UHMW Polyethylene 40 µm 100 QLFIL070-EW Cannula Filter, Erweka, UHMW Polyethylene 70 µm 1000 QLFIL070-EW-a Cannula Filter, Erweka, UHMW Polyethylene 70 µm 100 page 11 Further Dissolution articles available on request.

13 tablet dissolution accessories CANNULA FILTER HANSON Hanson Research baths use cannula style filters. The Hanson/Waters Dissolution HPLC interface uses a 1/16 (1.6 mm) narrow bore filterinstead of the normal 1/8 (3.2 mm) diameter. art.no. description pore size pack size oem reference QLFIL001-HR Cannula Filter, Hanson, UHMW Polyethylene 1 µm QLFIL001-HR-a Cannula Filter, Hanson, UHMW Polyethylene 1 µm QLFIL004-HR Cannula Filter, Hanson, UHMW Polyethylene 4 µm QLFIL004-HR-a Cannula Filter, Hanson, UHMW Polyethylene 4 µm QLFIL010-HR Cannula Filter, Hanson, UHMW Polyethylene 10 µm QLFIL010-HR-a Cannula Filter, Hanson, UHMW Polyethylene 10 µm QLFIL020-HR Cannula Filter, Hanson, UHMW Polyethylene 20 µm 1000 QLFIL020-HR-a Cannula Filter, Hanson, UHMW Polyethylene 20 µm 100 QLFIL035-HR Cannula Filter, Hanson, UHMW Polyethylene 35 µm QLFIL035-HR-a Cannula Filter, Hanson, UHMW Polyethylene 35 µm QLFIL045-HR Cannula Filter, Hanson, UHMW Polyethylene 45 µm 1000 QLFIL045-HR-a Cannula Filter, Hanson, UHMW Polyethylene 45 µm QLFIL070-HR Cannula Filter, Hanson, UHMW Polyethylene 70 µm QLFIL070-HR-a Cannula Filter, Hanson, UHMW Polyethylene 70 µm CANNULA FILTER PHARMATEST Pharmtest baths use 1/8 (3.2 mm) cannula style filters with a variety of porosities. art.no. description pore size pack size oem reference QLFIL001-PT Cannula Filter, Pharmatest, UHMW Polyethylene 1 µm 1000 QLFIL001-PT-a Cannula Filter, Pharmatest, UHMW Polyethylene 1 µm 100 QLFIL004-PT Cannula Filter, Pharmatest, UHMW Polyethylene 4 µm 1000 QLFIL004-PT-a Cannula Filter, Pharmatest, UHMW Polyethylene 4 µm 100 QLFIL005-PT Cannula Filter, Pharmatest, UHMW Polyethylene 5 µm 1000 QLFIL005-PT-a Cannula Filter, Pharmatest, UHMW Polyethylene 5 µm QLFIL010-PT Cannula Filter, Pharmatest, UHMW Polyethylene 10 µm 1000 QLFIL010-PT-a Cannula Filter, Pharmatest, UHMW Polyethylene 10 µm QLFIL035-PT Cannula Filter, Pharmatest, UHMW Polyethylene 35 µm 1000 QLFIL035-PT-a Cannula Filter, Pharmatest, UHMW Polyethylene 35 µm 100 QLFIL070-PT Cannula Filter, Pharmatest, UHMW Polyethylene 70 µm 1000 QLFIL070-PT-a Cannula Filter, Pharmatest, UHMW Polyethylene 70 µm 100 Further Dissolution articles available on request. page 12

14 tablet dissolution accessories CANNULA FILTER SOTAX For Sotax 1/8 (3.2 mm) cannula filters are used with different porosities. art.no. description pore size pack size oem reference QLFIL010-ST Cannula Filter, Sotax, UHMW Polyethylene 10 µm QLFIL010-ST-a Cannula Filter, Sotax, UHMW Polyethylene 10 µm QLFIL020-ST Cannula Filter, Sotax, UHMW Polyethylene 20 µm 1000 QLFIL020-ST-a Cannula Filter, Sotax, UHMW Polyethylene 20 µm 100 QLFIL035-ST Cannula Filter, Sotax, UHMW Polyethylene 35 µm QLFIL035-ST-a Cannula Filter, Sotax, UHMW Polyethylene 35 µm QLFIL070-ST Cannula Filter, Sotax, UHMW Polyethylene 70 µm QLFIL070-ST-a Cannula Filter, Sotax, UHMW Polyethylene 70 µm CANNULA FILTER AGILENT/VANKEL For both normally full flow filters or filter tips are used. They fit directly, there is no additional tubing necessary. art.no. description pore size pack size oem reference QLFIL Cannula Filter, Agilent/Vankel, UHMW Polyethylene 10 µm QLFIL a Cannula Filter, Agilent/Vankel, UHMW Polyethylene 10 µm QLFIL Cannula Filter, Agilent/Vankel, UHMW Polyethylene 20 µm 1000 QLFIL a Cannula Filter, Agilent/Vankel, UHMW Polyethylene 20 µm 100 QLFIL Cannula Filter, Agilent/Vankel, UHMW Polyethylene 35 µm QLFIL a Cannula Filter, Agilent/Vankel, UHMW Polyethylene 35 µm QLFIL Cannula Filter, Agilent/Vankel, UHMW Polyethylene 45 µm 100 QLFIL a Cannula Filter, Agilent/Vankel, UHMW Polyethylene 45 µm 1000 QLFIL Cannula Filter, Agilent/Vankel, UHMW Polyethylene 70 µm QLFIL a Cannula Filter, Agilent/Vankel, UHMW Polyethylene 70 µm page 13 Further Dissolution articles available on request.

15 sampling cannulae 7. Sampling Cannulae Sampling position: Cannula length: Cannula Material: Stoppers: Important for test with baskets, it is different for 500 ml and 900 ml tests. The cannula varies in length depending if it is a 500 ml or 900 ml test. They are made from stainless steel or PEEK, in order to guarantee that there is no adsorbtion or interference with the active ingredient. Stoppers can be used to make sure that the sample is always been taken from the same depth. The stoppers are attached to the cannula and they sit in a hole in the vessel cover. SAMPLING CANNULAE DISTEK art.no. description quantity oem reference QLCAN500-DK 500 ml Standard Sampling Probe for Distek Baths QLCAN900-DK 900 ml Standard Sampling Probe for Distek Baths QLCAN01K-DK 1000 ml Standard Sampling Probe for Distek Baths QLCAN02K-DK 2000 ml Standard Sampling Probe for Distek Baths 1 SAMPLING CANNULAE ERWEKA art.no. description quantity oem reference QLCAN475-SH 4.75 inch (120 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with SS luer Lock 1 QLCAN775-SH 7.75 inch (195 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with SS Luer Lock 1 QLCAN475-PH 4.75 inch (120 mm) Bent Peek 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock 1 QLCAN775-PH 7.75 inch (195 mm) Bent PEEK 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock 1 CAN015-PH 15 inch (380 mm) Bent PEEK 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock 1 Further Dissolution articles available on request. page 14

16 sampling cannulae SAMPLING CANNULAE HANSON art.no. description quantity oem reference QLCAN475-HR QLCAN775-HR QLCAN475-SH QLCAN475-SHL QLCAN775-SH QLCAN775-SHL QLCAN015-SH QLCAN475-PH QLCAN775-PH QLCAN015-PH 4.75 inch (120 mm) Bent 316 SS Cannula with SS Luer Lock & Perm SS Tip for Hanson/QLA inchhr inch style 7.75 inch (195 mm) Bent 316 SS Cannula with SS Luer Lock & Perm SS Tip for Hanson/QLA inchhr inch st 4.75 inch (120 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with SS luer Lock 4.75 inch (120 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with Kynar Luer Lock, Low Cost alternative 7.75 inch (195 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with SS Luer Lock 7.75 inch (195 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with Kynar Luer Lock, Low cost alternative 15 inch (380 mm) Bent 316 SS 1/8 (3.2 mm) OD Cannula with SS Luer Lock 4.75 inch (120 mm) Bent Peek 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock 7.75 inch (195 mm) Bent PEEK 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock 15 inch (380 mm) Bent PEEK 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock SAMPLING CANNULAE PHARMATEST art.no. description quantity oem reference QLCAN475-SH 4.75 inch (120 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with SS luer Lock 1 QLCAN775-SH 7.75 inch (195 mm) Bent 316 SS 1/8 inch (3.2 mm) OD Cannula with SS Luer Lock 1 QLCAN475-PH 4.75 inch (120 mm) Bent Peek 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock 1 QLCAN775-PH 7.75 inch (195 mm) Bent PEEK 1/8 inch (3.2 mm) OD Cannula with PEEK Luer Lock 1 SAMPLING CANNULAE SOTAX art.no. description quantity oem reference QLCAN013-ST QLCAN013-ST-5 QLCAN013-ST-5-9 QLCAN013-ST-9 13 inch (330 mm) Bent 316 SS Cannula with SS Luer Lock (thru head mount) 13 inch (330 mm) Bent 316 SS Cannula with SS Luer Lock, Pre-set with stopper for 500mL 13inch (330 mm) Bent 316 SS Cannula with SS Luer Lock and 2 Position Stopper 13 inch (330 mm) Bent 316 SS Cannula with SS Luer Lock, Pre-set with stopper for 900mL page 15 Further Dissolution articles available on request.

17 vessels 8. Vessels High quality vessels are important to obtain reproducible and correct results. They are the key element of the dissolution test. They have to meet the dimensions of the USP, also the bottom should be perfectly rounded without obvious efects of the glass on the inside. The thickness of the wall has to be even and reproducible. Vessels associated for different dissolution baths can vary in dimensions, although the dimensions are specified by the USP. The tolerances are quite wide. In general standard vessels are used, there are also Ultracenter Precision Vessels available. STANDARD GLAS VESSELS AGILENT (VANKEL) art.no. description quantity oem reference QLGLA900-AV 1000 ml Amber Glass Vessel for Agilent/VanKel/Varian, Serialized QLGLA900-AUNP 1000 ml Amber Glass Vessel with Plastic Rim, Serialized 1 QLGLA900-UNP 1000 ml Clear Glass Vessel with Plastic Rim, Serialized 1 QLGLA900-AVK 1000 ml Amber Glass Vessel for TruCenter, No Magnetic Collar, Serialized QLGLA900-VK 1000 ml Clear Glass Vessel for TruCenter, No Magnetic Collar, Serialized QLGLA900-70XDS 1000 ml Clear Glass Vessel with Plastic Rim for Agilent 708/709-DS Baths, Serialized QLGLA900-A70XDS 1000 ml Amber Glass Vessel with Plastic Rim for Agilent 708/709-DS Baths, Serialized QLGLA9PK ml Clear Glass PEAK Vessel for Agilent/VanKel/Varian, Serialized QLGLA9PK-AV 1000 ml Amber Glass PEAK Vessel for Agilent/VanKel/Varian, Serialized QLGLA9PK-UNP 1000 ml Clear Glass PEAK Vessel with Plastic Rim, Serialized 1 QLGLA9PK-AUNP 1000 ml Amber Glass PEAK Vessel with Plastic Rim, Serialized 1 QLGLA9PK-VK 1000 ml Clear Glass PEAK Vessel for TruCenter, No Magnetic Collar, Serialized QLGLA9PK-70XDS 1000 ml Clear Glass PEAK Vessel with Plastic Rim for Agilent 708/709-DS Baths, Serialized QLGLA9PK-A70XDS 1000 ml Amber Glass PEAK Vessel with Plastic Rim for Agilent 708/709-DS Baths, Serialized STANDARD GLAS VESSELS DISTEK art.no. description quantity oem reference QLGLA100-DK 100 ml Clear Glass Vessel for Distek & QLA Small Volume 1 QLGLA200-DK 200 ml Clear Glass Vessel for Distek & QLA Small Volume 1 QLGLA500-DK 500 ml Clear Glass Vessel for Distek, No Ring 1 QLGLA900-DK 1000 ml Clear Glass Vessel for Distek, No Ring, Serialized 1 QLGLA9CR-DK 1000 ml Clear Glass Vessel with Acculign Ring for Distek, Serialized QLGLA02K-DK 2000 ml Clear Glass Vessel for Distek, No Ring, Serialized QLGLA100-AD 100 ml Amber Glass Vessel for Distek & QLA Small Volume 1 QLGLA500-AD 500 ml Amber Glass Vessel for Distek, No Ring 1 QLGLA900-AD 1000 ml Amber Glass Vessel for Distek, No Ring, Serialized 1 QLGLA9CR-AD 1000 ml Amber Glass Vessel with Acculign Ring for Distek, Serialized Further Dissolution articles available on request. page 16

18 vessels STANDARD GLAS VESSELS ERWEKA art.no. description quantity oem reference QLGLA900-EW 1000 ml Clear Glass Vessel for Erweka, Serialized QLGLA02K-EW 2000 ml Clear Glass Vessel for Erweka, Serialized QLGLA900-AEW 1000 ml Amber Glass Vessel for Erweka STANDARD GLAS VESSELS FOR SR8-PLUS HANSON art.no. description quantity oem reference QLGLA500-HR 500 ml Clear Glass Vessel for Hanson SR8-Plus 1 QLGLA900-HR 1000 ml Clear Glass Vessel for Hanson SR8-Plus, Serialized QLGLA9PK-HR 1000 ml Clear Glass PEAK Vessel with Ring for Hanson SR8-Plus, Serialized QLGLA900-AH 1000 ml Amber Glass Vessel for Hanson SR8-Plus, Serialized QLGLA9PK-AH 1000 ml Amber Glass PEAK Vessel with Ring for Hanson SR8-Plus, Serialized QLGLA900-UNP 1000 ml Clear Glass Vessel with Plastic Rim, Serialized 1 QLGLA900-AUNP 1000 ml Amber Glass Vessel with Plastic Rim, Serialized 1 QLGLA9PK-UNP 1000 ml Clear Glass PEAK Vessel with Plastic Rim, Serialized 1 QLGLA9PK-AUNP 1000 ml Amber Glass PEAK Vessel with Plastic Rim, Serialized 1 STANDARD GLAS VESSELS PHARMATEST art.no. description quantity oem reference QLGLA900-PT 1000 ml Clear Glass Vessel for Pharmatest, Serialized QLGLA900-APT 1000 ml Amber Glass Vessel for Pharmatest, Serialized STANDARD GLAS VESSELS SOTAX art.no. description quantity oem reference QLGLA900-ST 1000 ml Clear Glas Vessel, Serialized QLGLA900-AST 1000 ml Amber Glas Vessel, Serialized Glass vessels have the advantage of good thermal conductivity. They have a high resistance to scratching which means they don`t have to be replaced so often. Amber vessels are used if light sensitive analytes are tested. They are available in glass and plastic. There are also Plastic Vessels, Plastic Rim Vessels and Peak Vessels available. UNIVERSAL VESSEL STANDS They are useful for the safe transportation and storage of the vessels. Scratched, chipped or smashed vessels can be avoided. The stands can hold 6 or 8 vessels of any dissolution bath manufacturer. art.no. description quantity oem reference QLVESSTD-06H 6 position Vessel Stand, Universal 1 QLVESSTD-08H 8 position Vessel Stand, Universal 1 page 17 Further Dissolution articles available on request.

19 paddles 9. Paddles Paddles are used for the Apparatus 2, commonly known as the paddle method. If it is important to get consistent results from vessel to vessel the dimensions and tolerances of the paddle can be critical. According to USP the paddle has to rotate smoothly without significant wobble. No sharp edges in the contours of the paddle blade wanted. They could produce a turbulent instead of a laminar flow pattern. Types: Electropolished Stainless Steel they are strong and resistant to bending. Surface impurities are removed by electropolishment, they are resitstant to corrosion. PTFE coated: Paddles are coated according to the suggestion of the USP to enhance inertness. Solid Fluoropolymer: a single piece molded design assures reduced wobble. AGILENT COMPATIBLE PADDLES art.no. description quantity oem reference QLEPD (370 mm) Paddle for V-Series, Electropolished 316 SS, Serialized QLEPD (380 mm) Paddle for VanKel/Varian, Electropolished 316 SS, Serialized QLEPD (480 mm) Paddle for VanKel/Varian, Electropolished 316 SS, Serialized QLEPD (535 mm) Paddle, Electropolished 316 SS, Serialized QLEPD (610 mm) Paddle, Electropolished 316 SS, Serialized QLNPD " (370 mm) Paddle for V-Series, PTFE coated over 316 SS, Serialized QLNPD (380 mm) Paddle for VanKel/Varian, PTFE coated over 316 SS, Serialized QLNPD (480 mm) Paddle for VanKel/Varian, PTFE coated over 316 SS, Serialized QLNPD (535 mm) Paddle, PTFE coated over 316 SS, Serialized QLNPD (610 mm) Paddle, PTFE coated over 316 SS, Serialized Further Dissolution articles available on request. page 18

20 paddles DISTEK COMPATIBLE PADDLES art.no. description quantity oem reference QLEPD QLNPD QLTPD (420 mm) Paddle for Distek 2100, Electropolished 316 SS, Serialized 16.5 (420 mm) Paddle for Distek 2100, PTFE coated over 316 SS, Serialized 16.5" (420 mm) Paddle for Distek 2100, Solid Molded Fluoropolymer, One Piece Design, Serialized HANSON COMPATIBLE PADDLES art.no. description quantity oem reference QLEPD QLTPD QLTPD (405 mm) Paddle for Hanson SR8-Plus, Electropolished 316 SS, Serialized 16" (405 mm) Paddle for Hanson SR8-Plus, Solid Molded Fluoropolymer, One Piece Design, Serialized 18" (457 mm) Paddle for Hanson, Solid Molded Fluoropolymer, One Piece Design, Serialized SOTAX COMPATIBLE PADDLES art.no. description quantity oem reference TPD012-ST (300 mm) Paddle with 10mm OD for Sotax, Solid Molded Fluoropolymer, One Piece Design, Serialized 1 BASKET SHAFT/PADDLE HOLDER Benefits: Prevents benting or scratching Quick and easy transport Non corrosive, quality plastic construction Space saving design art.no. description quantity oem reference QLPADHLD-12A 12 Position Paddle/Shaft holder 1 QLPADHLD-16A 16 Position Paddle/Shaft holder 1 page 19 Further Dissolution articles available on request.

21 baskets 10. Baskets The basket method was the first official method. This method is now named Apparatus 1. The metallic shaft is connected to the cylindrical basket. The basket is positioned inside the vessel, kept at a constant temperature. The vessel solution is stirred smoothly by the rotating basket. Normally the USP method required a 40 mesh screen unless otherwise specified. AGILENT COMPATIBLE BASKETS art.no. description quantity oem reference QLBSK Mesh Clip Style Basket for Agilent/VanKel, 316 SS, Serialized QLBSK Mesh (USP) Clip Style Basket for Agilent/VanKel, 316 SS, Serialized QLBSK Mesh Clip Style Basket for Agilent/VanKel, 316 SS, Serialized QLBSKPTV Mesh Clip Style Basket for Agilent/VanKel, PTFE Coated over 316 SS, Serialized QLBSKSUP-01 Suppository Basket for Agilent/VanKel, Plastic DISTEK COMPATIBLE BASKET art.no. description quantity oem reference QLBSK010-DK 10 Mesh Standard Push-On Style Basket for Distek, 316 SS, Serialized QLBSK010-DKC 10 Mesh Evolution Series Basket for Distek, 316 SS, Serialized QLBSK020-DK 20 Mesh Standard Push-On Style Basket for Distek, 316 SS, Serialized QLBSK020-DKC 20 Mesh Evolution Style Basket for Distek, 316 SS, Serialized QLBSK040-DK 40 Mesh (USP) Standard Push-On Style Basket for Distek, 316 SS, Serialized QLBSK040-DKC 40 Mesh (USP) Evolution Style Basket for Distek, 316 SS, Serialized QLBSK100-DK 100 Mesh Standard Push-On Style Basket for Distek, 316 SS, Serialized QLBSK100-DKC 100 Mesh Evolution Style Basket for Distek, 316 SS, Serialized QLBSKPTD Mesh Standard Push-On Style Basket for Distek, PTFE Coated over 316 SS, Serialized 1 QLBSKSUP-DK Suppository Basket for Distek Standard Push-On Style, Plastic Further Dissolution articles available on request. page 20

22 baskets ERWEKA COMPATIBLE BASKET art.no. description quantity oem reference QLBSK010-EW 10 Mesh Clip Style Basket for Erweka, 316 SS, Serialized QLBSK020-EW 20 Mesh Clip Style Basket for Erweka, 316 SS, Serialized QLBSK040-EW 40 Mesh (USP) Clip Style Basket for Erweka, 316 SS, Serialized QLBSKSUP-EW Suppository Basket for Erweka, Plastic HANSON COMPATIBLE BASKET art.no. description quantity oem reference QLBSK010-HR 10 Mesh Clip Style Basket for Hanson, 316 SS, Serialized QLBSK020-HR 20 Mesh Clip Style Basket for Hanson, 316 SS, Serialized QLBSK040-HRP 40 Mesh (USP) Precision Clip Style Basket for Hanson, 316 SS, Serialized QLBSK100-HR 100 Mesh Clip Style Basket for Hanson, 316 SS, Serialized 1 QLBSKPTH Mesh Clip Style Basket for Hanson, PTFE Coated over 316 SS, Serialized 1 QLBSKSUP-HR Suppository Basket for Hanson, Plastic PHARMATEST COMPATIBLE BASKET art.no. description quantity oem reference QLBSK010-PT 10 Mesh Clip Style Basket for Pharmatest, 316 SS, Serialized QLBSK020-PT 20 Mesh Clip Style Basket for Pharmatest, 316 SS, Serialized 1 QLBSK040-PT 40 Mesh (USP) Clip Style Basket for Pharmatest, 316 SS, Serialized QLBSKPTP Mesh Clip Style Basket for Pharmatest, PTFE Coated over 316 SS, Serialized QLBSKSUP-PT Suppository Basket for Pharmatest, Plastic 1 SOTAX COMPATIBLE BASKET art.no. description quantity oem reference QLBSK010-ST 10 Mesh Clip Style Basket for Sotax, 316 SS, Serialized 1 QLBSK020-ST 20 Mesh Clip Style Basket for Sotax, 316 SS, Serialized 1 QLBSK040-ST 40 Mesh (USP) Clip Style Basket for Sotax, 316 SS, Serialized QLBSK080-ST 80 Mesh Clip Style Basket for Sotax, 316 SS, Serialized 1 QLBSK100-ST 100 Mesh Clip Style Basket for Sotax, 316 SS, Serialized 1 QLBSK140-ST 140 Mesh Clip Style Basket for Sotax, 316 SS, Serialized 1 QLBSKSUP-ST Suppository Basket for Sotax, Plastic 1 page 21 Further Dissolution articles available on request.

23 baskets CARE AND MAINTENANCE Handling: They always should be handled by the upper rim, because they can be easily deformed. Also special tools are available for handling the baskets. Cleaning: Baskets have to clean prior to use. Often the mesh is clogged, therefore carefully cleaning is necessary. Storage: In order to extend their life they should be stored correctly. The suppliers case is recommended, also there are specially designed basket holders available. BASKET STORAGE Basket Holders provide a convenient way to organize and store baskets. The damaging can be reduced with a basket storage. Benefits: Compatible with all popular basket types Avoids deformed or bent baskets Stackable to maximize storage place art.no. description quantity oem reference QLBSKHLD-6 6 Position Basket Holder 1 QLBSKHLD Position Basket Holder 1 Further Dissolution articles available on request. page 22

24 capsule spiral sinkers 11. Capsule Spiral Sinkers Using a sinker helps to enhance reproducibility in the dissolving process. Sinkers also prevent that the tablet stickes to the side of the vessel. It is recommended to stick to the same sinker design, once an application is approved. Basket sinkers: used for coin shaped tablets, clogging of the mesh has to be avoided Spiral Sinkers: Clogging is easily avoided compared to basket sinkers art.no. description quantity oem reference QLCAPWHT-02 QLCAPWHT-04 QLCAPWHT-2S QLCAPWHT-4S QLCAPWHT-LG QLCAPWHT-LGMT QLCAPWHT-XL QLCAPWHT-XLS QLCAPWHT-XLSS QLCAPWHT-XS Spiral Capsule Sinker, PTFE Coated Music Wire,.84" (21.3 mm) L x.37" (9.4 mm) W capacity, 8.5 coils Spiral Coated Capsule Sinker, PTFE Coated Music Wire, L x.84" (21.3 mm) L x.385" (9.8 mm) W capacity, 5 coils Spiral Coated Capsule Sinker, 316 SS,.84" (21.3 mm) L x.37" (9.4 mm) W capacity, 8.5 coils Spiral Coated Capsule Sinker, 316 SS,.84" (21.3 mm) L x.385" (9.8 mm) W capacity, 5 coils Spiral Coated Capsule Sinker, PTFE Coated Music Wire, 1.10" (27.9 mm) L x.41" (10.4 mm) W capacity, 6.5 coils Spiral Capsule Sinker, Orange PTFE Coated Music Wire, 1.10" (27.9 mm) L x.41" (10.4 mm) W capacity, 6.5 coils Spiral Coated Capsule Sinker, PTFE Coated Music Wire, 1.15" (29.2 mm) L x.465" (11.8 mm) W capacity, 5.5 coils Spiral Coated Capsule Sinker, 316 SS, 1.15" (29.2 mm) L x.465" (11.8 mm) W capacity, 5.5 coils Spiral Coated Capsule Sinker, 316 SS,.885" (22.5 mm) L x.465" (11.8 mm) W capacity, 3 coils Spiral Coated Capsule Sinker, 316 SS,.885" (22.5 mm) L x.575" (14.6 mm) W capacity, 8.5 coils page 23 Further Dissolution articles available on request.

25 basket sinkers 12. Basket sinkers art.no. description quantity oem reference QLBSK Mesh Basket Sinker, 316 SS, 1.06" (26.9 mm) L x.62" (15.7 mm) W capacity 1 QLBSK008-01LG 8 Mesh Basket Sinker; 316 SS, Custom Size 1 QLBSK008-JP 8 Mesh Basket Sinker, 316 SS,.90" (22.9 mm) L x.51" (12.9 mm) W capacity 1 QLCUSBSK-JP Japanese Pharmacopeia Basket Sinker, 316 SS (same dimensions as shown in USP) QLCUSBSK-JPMAG Magnetic Japanese Basket Sinker, 316 SS (same dimensions as shown in USP) 1 QLSNK008-VK 8 Mesh Sinker Basket with Lid, 316 SS QLSNK010-VK 10 Mesh Sinker Basket with Lid, 316 SS QLSNK020-VK 20 Mesh Sinker Basket with Lid, 316 SS QLSNK030-VK 30 Mesh Sinker Basket with Lid, 316 SS 1 QLSNK040-VK 40 Mesh Sinker Basket with Lid, 316 SS QLSNK080-VK 80 Mesh Sinker Basket with Lid, 316 SS 1 Further Dissolution articles available on request. page 24

26 sample bottles, micro inserts and closures for hplc 13. Sample bottles, micro inserts and closures for HPLC THREAD BOTTLES ND8, NARROW OPENING 1.hydrolytic class, 1.5 ml, standard bottles for HPLC/GC are preferably used on instruments of the following manufacturers: VWR (Merck)/Hitachi, Beckman, CTC, Gilson, Knauer, Shimadzu, Spark, Varian etc. MICRO INSERTS art.no. AAV AAV AAV AAV AAV AAV AAV AAV description 1,5 ml 32x11, 6 mm Clear glass 1,5 ml 32x11, 6 mm Brown glass 1,5 ml 32x11, 6 mm Clear glass Text box 1,5 ml 32x11, 6 mm Brown glass Text box 0,1 ml Micro insert 31x5 mm, Clear glass 15 mm tip 0,1 ml Micro insert 31x5 mm, Clear glass 9 mm tip 0,2 ml Micro insert 31x6 mm Clear glass with flat bottom 0,1 ml Micro insert 29x5, 7 mm Clear glass with polymer stand quantity POLYPROPYLENE SCREW CAPS ND8 art.no. AAV AAV AAV AAV AAV AAV AAV AAV septum Natural rubber redorange/tef transparent Red Rubber/ PTFE beige Butyl red/ PTFE grey Silicone white/ptfe red Ultra Clean Silicone creme/ptfe red Ultra Clean Silicone blue/ PTFE white PTFE red/ Silicone white/ptfe red Silicone white/ptfe red, slitted durometer 60 shore A 45 shore A 55 shore A 45 shore A 55 shore A 45 shore A 45 shore A 45 shore A thickness 1,3 mm 1,0 mm 1,3 mm 1,3 mm 1,5 mm 1,3 mm 1,0 mm 1,3 mm quantity page 25

27 sample bottles, micro inserts and closures for hplc SHORT THREAD VIALS ND9, WIDE OPENING 1.hydrolytic class, ND9 bottles are preferably used on instruments of the following manufactures: Agilent, Shimadzu, Thermo Scientific, Varian, Waters etc. MICRO INSERTS art.no. AAV AAV AAV AAV AAV AAV AAV description 32x11,6 mm, Clear glass 32x11,6 mm, Clear glass labelling field and filling mark 32x11,6 mm, Brown glass labelling field and filling mark 0,1 ml Micro insert 31x6 mm Clear glass 15 mm Tip 0,1 ml Micro insert 31x6 mm 12 mm Tip 0,2 ml Micro insert 31x6 mm Clear glass Flat bottom 0,1 ml Micro insert 29x5,7 mm Clear glass assembled pastic spring quantity POLYPROPYLENE SHORT THREAD VIAL CAPS ND9 art.no. AAV AAV AAV AAV AAV AAV septum PTFE virginal Natural rubber red-orange/tef transparent Red Rubber/ PTFE beige IH-quality Silicone white/ PTFE red Ultra clean PTFE red/ Silicone white/ PTFE red Silicone white/ PTFE blue, slitted durometer 53 shore D 60 shore A 45 shore A 55 shore A 45 shore A 55 shore A thickness 0,2 mm 1,0 mm 1,0 mm 1,0 mm 1,0 mm 1,0 mm quantity page 26

28 sample bottles, micro inserts and closures for hplc SHORT THREAD VIALS ND10, WIDE OPENING 1.hydrolytic class, ND10 bottles are preferably used on instruments of the following manufacturers: Jasco, Perkin Elmer, Shimadzu, Varian, Waters etc. MICRO INSERTS art.no. AAV AAV AAV AAV AAV AAV AAV description 32x11,6 mm Clear glass wide opening 32x11,6 mm Clear glass wide opening, with labelling box and filling mark 32x11,6 mm Brown glass wide opening, with labelling box and filling mark 0,1 ml Micro insert 31x6 mm Clear glass 15 mm Tip 0,1 ml Micro insert 31x6 mm 12 mm Tip 0,2 ml Micro insert 31x6 mm Clear glass Flat bottom 1.1 ml Micro insert 29x5,7 mm Clear glass with polymer stand quantity POLYPROPYLENE SCREW CAPS ND10, BLACK art.no. AAV AAV AAV AAV AAV septum Natural Rubber red-orange/tef transparent Silicone white/ PTFE red Ultra clean Silicone white/ PTFE beige PTFE red/silicone white/ptfe red Silicone white/ PTFE blue slitted durometer 60 shore A 45 shore A 45 shore A 45 shore A 55 shore A thickness 1,3 mm 1,3 mm 1,5 mm 1,0 mm 1,5 mm quantity page 27

29 sample bottles, micro inserts and closures for hplc CRIMP TOP VIALS ND11 1. hydrolytic class, ND11 bottles are preferably used on instruments of the following manufacturers: Agilent, CTC, Gerstel, Jasco, Perkin Elmer, Shimadzu, Spark, Thermo Scientific, Varian etc. MICRO INSERTS art.no. AAV AAV AAV AAV AAV AAV AAV description 1,5 ml crimp top vial, 32x11 mm, clear glass, wide opening 1,5 ml crimp top vial, 32x11 mm, clear glass, wide opening with labeling box and filling mark 1,5 ml crimp top vial, 32x11 mm, brown glass, wide opening with labeling box and filling mark 0,1 ml micro insert 31x6 mm Clear glass 15 mm Tip 0,1 ml micro insert 31x6 mm 12 mm Tip 0,2 ml micro insert 31x6 mm Clear glass Flat bottom 0.1 ml micro insert 29x5, 7 mm Clear glass With polymer stand quantity ALUMINUM ROLL CRIMP ND11 art.no. AAV AAV AAV AAV AAV AAV septum Natural Rubber red-orange/ Butyl red/tef transparent Red Rubber/PTFE beige Silicon white/ PTFE red Ultra clean Silicon creme/ PTFE red PTFE red/ Silicone white/ PTFE red Silicon white/ PTFE blue, cross slitted durometer 45 shorea 45 shorea 45 shorea 55 shorea 45 shorea 55 shore A thickness 1,0 mm 1,0 mm 1,3 mm 1,5 mm 1,0 mm 1,5 mm quantity page 28

30 sample bottles and closures for gc 14. Sample bottles and closures for GC HEADSPACE VIALS ND20 + ND18: art.no. AAV AAV AAV AAV AAV AAV description ND20/ND18 5 ml Headspace-vial, 38,2x22 mm, clear, rounded bottom ND20/ND18 5 ml Crimp Neck Vial, 38x20 mm, clear, flat bottom ND20/ND18 10 ml Headspace-Vial, 46x22,5 mm, clear, DIN-crimp neck, rounded bottom ND20/ND18 10 ml Crimp Neck Vial, 54.5x20 mm, clear glass, 1st hydrolytic class, flat bottom ND20/ND18 10 ml Headspace- Vial 46x22,5 mm, clear, DIN-crimp neck, long neck, flat bottom ND20/ND18 20 ml Headspace-Vial, 75,5x23 mm, clear, rounded bottom volume 5 ml 5 ml 10 ml 10 ml 10 ml 20 ml quantity art.no. AAV AAV AAV AAV AAV AAV description ND20/ND18 20ml Headspace-Vial, 75,5x23 mm, clear, rounded bottom, label/ filling lines ND20/ND18 20ml Headspace-Vial, 75,5x22,5 mm, clear, DIN-crimp neck, long neck, flat bottom ND20/ND18 20 ml Headspace- Vial 75,5x22,5 mm, clear, DIN-crimp neck, long neck, rounded bottom ND20/ND18 20ml SPME vial, 75,5x22,5mm, clear, special crimp neck,rounded bottom ND18 10ml Precision Thread Vial, 46x22,5 mm, clear glass, rounded bottom ND18 20ml Precision Thread Vial, 75,5x22,5 mm, clear glass, rounded bottom volume 20 ml 20 ml 20 ml 20 ml 10 ml 20 ml quantity page 29

31 sample bottles and closures for gc ALUMINIUM CRIMPSEAL ND20 Butyl: art.-no. AAV AAV AAV AAV AAV AAV description ND20 Butyl Combination Seal: Aluminium Cap, plain, 10mm centre hole, dark grey, 3,0 mm ND20 Butyl Combination Seal: Aluminium Headspace Cap, clear lacquered, centre hole, dark grey ND20 Butyl Combination Seal: Aluminium Centre Tear-Off Cap, clear lacquered, dark grey ND20 Butyl Combination Seal: Aluminium Cap, clear lacquered, complete tear off ND20 Butyl Combination Seal: Magnetic Cap, gold, 5 mm centre hole, 3,0 mm ND20 Butyl Combination Seals: Magnetic Cap, gold, 8 mm centre hole, 3,0 mm, darkgrey durometer 55 shore A 55 shore A 55 shore A 55 shore A 55 shore A 55 shore A thickness 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm temperature range -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C quantity Butyl/PTFE: art.-no. AAV AAV AAV AAV AAV AAV description ND20 Al crimpseal, septum 3,0 mm Butyl/PTFE, grey, blank roll. ND20 Al Headspace crimpseal, septum 3,0 mm, Butyl/PTFE, grey, transp. 20 mm Combination Seal: Aluminium Cap, plain, centre tear off 20 mm Combination Seal: Aluminium Cap, clear lacquered, complete tear off ND20 Magneticcrimpseal, w/5 mm hole, gold, 50 3,0 mm, septum Butyl/ PTFE ND20 Magneticcrimpseal w/8 mm hole, 3,0 mm, septum Butyl/PTFE, grey, gold durometer 50 shore A 50 shore A 50 shore A 50 shore A 50 shore A 50 shore A thickness 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm temperature range -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C quantity page 30

32 sample bottles and closures for gc Pharma-Fix (Butyl/PTFE): art.-no. AAV AAV AAV AAV AAV AAV description ND20 Al crimpseal Pharma-Fix-Sept. 3,0 mm, Butyl/ PTFE, blank roll ND20 Al Headspace crimpseal 3,0 mm Butyl/PTFE, transp., Pharma- Fix-Septa ND20 Al crimpseal Pharma-Fix- Sept. 3,0 mm ND20 Al crimpseal Pharma-Fix- Sept. 3,0 mm, Butyl/PTFE, transp., compl. Tear-off ND20 Magnetic crimpseal, Pharma-Fix- Sept,3,0 mm ND20 Magneticcrimpseal w/8 mm hole, 3,0 mm durometer 50 shore A 50 shore A 50 shore A 50 shore A 50 shore A 50 shore A thickness 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm temperature range -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C -40 C to 120 C quantity Silicon blue transparent/ptfe white: art.-no. AAV AAV AAV AAV AAV AAV description ND20 Al crimpseal, blank roll., 3,0 mm Cap, crimp, headspace, with septa, 20 mm, aluminum cap with safety feature, PTFE/ silicone septa UltraClean Closure: 20 mm Combination Seal: Aluminium Cap, plain, centre tear off UltraClean ND20 Magnetic crimpseal,w/ 5 mm hole, 3,0 mm ND20 magnetic crimpn.cap, gold, 8 mm hole, 3,0 mm Caps/septa, crimp, headspace, 20 mm, bimetal magnetic, PTFE/silicone septa durometer 45 shore A 45 shore A 45 shore A 45 shore A 45 shore A 45 shore A thickness 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm 3,0 mm temperature range -60 C to 200 C -60 C to 200 C -60 C to 200 C -60 C to 200 C -60 C to 200 C -60 C to 200 C quantity page 31

33 sample bottles and closures for gc Silicon white/ptfe beige: art.-no. AAV AAV AAV AAV description Cap, crimp, headspace, with septa, 20 mm, silver aluminum cap with safety feature ND20 Al Headspace crimpseal, 3,2 mm 20 mm Combination Seal: Magnetic Cap, gold lacquered, 8mm centre hole 20 mm Combination Seal: Magnetic Bi-Matall Cap, red lacquered, with 8 mm centre hole durometer 45 shore A 45 shore A 45 shore A 45 shore A thickness 3,2 mm 3,2 mm 3,2 mm 3,2 mm temperature range -60 C to 200 C -60 C to 200 C -60 C to 200 C -60 C to 200 C quantity Silicon/Aluminiumfoil: art.-no. AAV AAV AAV description ND20 Al crimpseal, blank roll., 3,0 mm ND20 Al Headspace crimpseal,transp., 3,0 mm 20 mm Combination Seal: Magnetic Cap, gold lacquered, 5 mm centre hole durometer 50 shore A 50 shore A 50 shore A thickness 3,0 mm 3,0 mm 3,0 mm temperature range -60 C to 200 C -60 C to 200 C -60 C to 200 C quantity page 32

34 sample bottles and closures for gc ND18 THREAD VIALS AND MAGNETIC SCREW CAPS art.no. AAV AAV AAV AAV AAV description ND18 10 ml Precision Thread Vial, 46x22,5 mm, clear glass, rounded bottom ND18 20 ml Precision Thread Vial 75,5x22, 5 mm, clear glass, rounded bottom UltraClean Closure: 18 mm Magnetic Universal Screw Cap, silver, centre hole UltraClean 18mm Magnetic Univer.scr. cap, 1,3 mm ND18 MagneticUniversal screwcap, 1,5 mm volume 10 ml 20 ml septum Silicone white PTFE red Silicone blue transparent/ptfe white Ultra Clean Silicone white/ptfe blue Ultra Clean durometer 45 shore A 45 shore A 55 shore A quantity page 33

35 crimping tools 15. Crimping tools We offer a wide range of pliers for opening and sealing sample bottles. Our range includes both manual, electronic and pneumatic crimpers and decappers for all standard flanging caps. Correct crimping Flat cap surface Flat septum surface Not fitting aluminium circular edges Bulging of the cap Deformation of the cap sides Convex looking sealing disc Rounded cap sides/upwards bulging of the cap/disc Tight fit of the aluminium crimp Planar and intact cap side Adjust the crimping pressure by the adjusting screw in the handlebar + Adjust the crimping height with an Allen key (see below) Adjust the crimping pressure by the adjusting screw in the handlebar + Adjust the crimping height with an Allen key (see below) Adjust the crimping height with an Allen key (see below) Adjust the crimping height with an Allen key (see below) Especially in the case of headspace caps, it is important not to over-crimp these. If the aluminum is pulled too far under the rolling edge, the stops of the breaking lines suffer from too much pressure and break even at a low internal pressure of the cylinder (less than 3 bar). In the worst case, they tear apart even next to the breaking lines. MANUAL FLANGING PLIERS: Easy Handling Chemically resistant surface finish Also available stainless steel flanging pliers for clean room work Adjustable by the use of the adjustment screw ELECTRONIC FLANGING PLIERS: Safe and especially reproducible crimping Fast and easy removal of the caps Ergonomic design and the possibility to process big sample quantities fast and easy page 34

36 crimping tools MANUAL CRIMPING TOOLS art.no. AAV AAV AAV AAV article Crimping tool, 8 mm Caps Crimping tool, 11 mm Caps Crimping tool, 13 mm Caps Crimping tool, 20 mm Caps MANUAL DECAPPERS art.no. AAV AAV AAV AAV article Decapper, 8 mm Caps Decapper, 11 mm Caps Decapper, 13 mm Caps Decapper, 20 mm Caps ELECTRONIC CRIMPING TOOLS art.no. MN MN MN MN MN article 11 mm electronic crimping tool with 6.4 V battery and 7.5 V-DC- power supply, 1 piece 20 mm electronic crimping tool with 6.4 V battery and 7.5 V-DC- power supply, 1 piece 11 mm electronic Decapper with 6.4 V battery and 7.5 V-DC- power supply, 1 piece 20 mm electronic Decapper with 6.4 V battery and 7.5 V-DC-power supply, 1 piece Tripod for electronic flanging tools page 35

37 storage system for hplc and gc columns 16. Storage system for HPLC and GC columns This column cabinet is a cost-effective solution for storing your HPLC or GC columns safely and well organized. Storage of up to 30 HPLC-columns or 5 GC-columns in safe foam pits Stackable and thus optionally extendable For HPLC-Columns of up to 30 cm length - also suitable for 5 cm, 12,5 cm, 15 cm and 25 cm Suitable for all types of End-Fitting Robust and firm casing made from 100 % steel with chromium plated drawer handles Highly versatile - store up to 12 different 12,5 cm columns in one single drawer, or a combination of short, analytical or pre-columns HPLC art.no. article description manufacturer AAColStore30 Storage shelf for 30 HPLC columns Altmann Analytik AAColToolTray Insert for small parts of the column Storage cabinet Altmann Analytik AAMountingKit Metal clip to connect two storage cabinets for HPLC columns Altmann Analytik GC art.no. article description manufacturer AAColStore GC Storage for five GC colums Altmann Analytik page 36

38 guard columns 17. Guard columns by Altmann Analytik If you would like to protect your column by adding a guard column cartridge, you also always need a guard column holder. The following diagrams show the connection possibilities for a guard column to an HPLC column (column connectors have to be ordered separately): a) Direct coupling in case you use a guard column by Altmann and a HPLC-column by Altmann b) Indirect coupling in case you use a guard column by Altmann and a HPLC-column by another manufacturer Guard column holder, direct (and fitting adapter, included) Guard column holder, indirect (and fitting adapter, included) Guard column holder, fitting adapter, pre-column and column Guard column holder, guard column Guard column holder screwed to column Column without guard column (front) Guard column holder, column connector (Not included), column Please pay attention to the fact that you need to order the appropriate guard column holder (see following page)! page 37

39 guard holder EXAMPLES PRECOLUMNS art.no. precolumns material length (mm) diameter (mm) particle size (mm) quantity suitable holder direct suitable holder indirect HYPERSIL AAVHSBC Pre column Hypersil BDS C ,6 3 5 AAHD AAHI AAVHSBC Pre column Hypersil BDS C AAHD AAHI LICHROSPHER AAVLI1R Pre column Lichrospher 100 RP AAHD AAHI AAVLI1R Pre column Lichrospher 100 RP AAHD AAHI AAVLI6RS Pre column Cartridge Lichrospher 60 RP-Select-B 5 5 4,6 5 5 AAHD-0546 AAHI-0546 AAVLI6RS Pre column Lichrospher 60 RP-Select-B AAHD AAHI LICHROSORB AAVLS6S Pre column Lichrosorb 60 Si AAHD AAHI AAVLS6S Pre column Lichrosorb 60 Si, 5 µm AAHD AAHI NUCLEOSIL C18 AAVNS1C Pre column Nucleosil 100 C18, 5µm 10x4 mm, 5 St AAHD AAHI AAVNS1C Pre column Nucleosil 100 C18, 5µm 5x4,6 mm, 5/PAK 5 4,6 5 5 AAHD-0546 AAHI-0546 GUARD HOLDERS Here, we list all available guard column holders for connecting Altmann guard columns with Altmann columns (direct coupling) or columns from other manufacturers (indirect coupling). For the indirect guard column holders, you need a column connector (see following page), as an intermediate piece between column and guard column holder. Make sure that the length (5, 10, 20 mm) matches length of the guard column. In principle, the guard column should not be more than 10 % compared to the column. FOR COLUMNS WE THEREFORE RECOMMEND with a length of 50 mm: guard columns with a length of 5 mm with a length of 60 mm up to 199 mm: guard columns with a length of 10 mm with a length of 200 mm and longer: guard columns with a length of 20 mm length of precolumn cartridge guard column holder for indirect coupling (column connector needed!) 5x4,6 mm AAHI x4,6 mm AAHI x4,6 mm AAHI x4 mm AAHI x4 mm AAHI x4 mm AAHI x3 mm AAHI x2 mm AAHI x2 mm AAHI x2 mm AAHI length of precolumn cartridge guard column holder for direct coupling 5x4,6 mm AAHD x4,6 mm AAHD x4,6 mm AAHD x4 mm 10x4 mm 20x4 mm 5x2 mm 10x2 mm AAHD-0540 AAHD AAHD AAHD-0520 AAHD Other dimensions available on request page 38

40 column connectors COLUMN CONNECTORS, ONE-PIECE FINGERTIGHT (FOR INDIRECT COUPLING) TIP: make sure to pay attention to the correct size and the dead volume. article art.no. pu Column connector, PEEK, universal 0,13 mm Inner diameter, red JR Column connector, PEEK, universal 0,17 mm Inner diameter, yellow JR Column connector, PEEK, universal 0,25 mm Inner diameter, blue JR Column connector, PEEK, universal 0,50 mm Inner diameter, orange JR COLUMN PLUGS art.no. colour pu JR White 10 JR Black 10 JR Red 10 JR Green 10 JR Blue 10 page 39

41 hplc columns by altmann analytik 18. HPLC columns by Altmann Analytik We supply HPLC columns of our own brand with all common filling materials (Hypersil, Nucleosil, Inertsil etc.) in all sizes in the highest quality. Other columns with different dimensions are available upon request. If you are unsure about the HPLC column, please contact our customer service. HYPERSIL BDS C18: Hypersil BDS is a very robust universal applicable column for a huge range of applications. Due to a low silanol activity, therefore reliable results can be expected. The base deactivated material is one of the most popular material. art.no. column length (mm) diameter (mm) particle size (µm) AANHSBC HPLC Column Hypersil BDS C18 3 μm 100x AANHSBC HPLC Column Hypersil BDS C18 3 μm 100x4, ,6 3 AANHSBC HPLC Column Hypersil BDS C18 3 μm 150x4, ,6 3 AANHSBC HPLC Column Hypersil BDS C18 5 μm 150x4, ,6 5 AANHSBC HPLC Column Hypersil BDS C18 5 μm 250x AANHSBC HPLC Column Hypersil BDS C18 5 μm 250x4, ,6 5 HYPERSIL ODS: Universal phase for a huge range of applications. art.no. column length (mm) diameter (mm) particle size (µm) AANHSO HPLC Column Hypersil ODS 3 μm 125x AANHSO HPLC Column Hypersil ODS 3 μm 125x4, ,6 3 AANHSO HPLC Column Hypersil ODS 5 μm 125x AANHSO HPLC Column Hypersil ODS 5 μm 125x4, ,6 5 Other dimensions available on request page 40

42 hplc columns by altmann analytik LICHROSPHER: Lichrospher is a reliable and versatile spherical silica sorbent, available in different modifications. art.no. column length (mm) diameter (mm) particle size (µm) AANLI1D HPLC Column Lichrospher 100 Diol 5 μm 150x AANLI1D HPLC Column Lichrospher 100 Diol 5 μm 250x4, ,6 5 AANLI1R HPLC Column Lichrospher 100 RP18 5 μm 125x AANLI1R HPLC Column Lichrospher 100 RP18 5 μm 250x AANLI1R HPLC Column Lichrospher 100 RP18 5 μm 250x4, ,6 5 AANLI6RS HPLC Column Lichrospher 60 RP-Select-B 5 μm 125x AANLI6RS HPLC Column Lichrospher 60 RP-Select-B 5 μm 125x4, ,6 5 AANLI6RS HPLC Column Lichrospher 60 RP-Select-B 5 μm 250x AANLI6RS HPLC Column Lichrospher 60 RP-Select-B 5 μm 250x4, ,6 5 LICHROSORB: Lichrosorb is one of the most successful and reliable packing material on the market. The totally porous irregular 5 µm particles are available in many different dimensions. art.no. column length (mm) diameter (mm) AANLS1R HPLC Column Lichrosorb 100 RP18 5 μm 250x AANLS1R HPLC Column Lichrosorb 100 RP18 5 μm 250x4, ,6 5 AANLS6S HPLC Column Lichrosorb 60 Si 5 μm 100x4, ,6 5 AANLS6S HPLC Column Lichrosorb 60 Si 5 μm 125x AANLS6S HPLC Column Lichrosorb 60 Si 5 μm 250x particle size (µm) NUCLEOSIL C18: Nonpolar, endcapped phase for RP chromatography. Different pore sizes and particle sizes are available. The separation process is based on hydrophobic interactions and slight residual silanol interactions. art.no. column length (mm) diameter (mm) particle size (µm) AANNS1C HPLC Column Nucleosil 100 C18 5 μm 125x AANNS1C HPLC Column Nucleosil 100 C18 5 μm 125x4, ,6 5 AANNS1C HPLC Column Nucleosil 100 C18 5 μm 150x4, ,6 5 AANNS1C HPLC Column Nucleosil 100 C18 5 μm 250x4, ,6 5 AANNS9C HPLC Column Nucleosil 120 C18 3 μm 100x AANNS9C HPLC Column Nucleosil 120 C18 3 μm 150x page 41 Other dimensions are available on request.

43 akzo nobel kromasil columns 19. Akzo Nobel Kromasil Columns Kromasil is a high-efficiency silica-based packing material for many different applications. Columns can be used for analytical applications and efficient for full scale production. A wide range of separation problems can be covered due to the variety of surface chemistry and pore sizes. The well-known Kromasil Classic 100 Å family is used to separate and purify molecules of up to about Da. In fact, drug candidates for the pharmaceutical, natural products and API industries are separated and purified using Kromasil Classic 100 Å columns and bulk material KROMASIL RP18 COLUMNS: High quality sperical silica gel. All derivatised phases are endcapped. Therefore a huge stability and a high batch to batch reproduceability is assured. art.no. description length (mm) diameter (mm) particle size (µm) pore size quantity ANM05CLD10 Kromasil C , ANM05CLD15 Kromasil C , ANM05CLD25 Kromasil C , ANM05CLC10 Kromasil C ANM05CLC1F Kromasil C ANM05CLC15 Kromasil C ANM05CLC25 Kromasil C ANM05CLC30 Kromasil C ANM05CLJ15 Kromasil C , ANM05CLJ25 Kromasil C , ANM05CLB10 Kromasil C ANM05CLB1F Kromasil C ANM05CLB15 Kromasil C ANM05CLB20 Kromasil C ANM05CLB25 Kromasil C ANM05CLA10 Kromasil C , ANM05CLA1F Kromasil C , ANM05CLA15 Kromasil C , ANM05CLA20 Kromasil C , ANM05CLA25 Kromasil C , Other dimensions available on request page 42

44 akzo nobel kromasil columns KROMASIL C8 COLUMNS High quality sperical silica gel. All derivatised phases are endcapped. Therefore a huge stability and a high batch to batch reproduceability is assured. art.no. description length (mm) diameter (mm) particle size (µm) pore size quantity ANM05CMD10 Kromasil C , ANM05CMD15 Kromasil C , ANM05CMD25 Kromasil C , ANM05CMC10 Kromasil C ANM05CMC1F Kromasil C ANM05CMC15 Kromasil C ANM05CMC25 Kromasil C ANM05CMJ15 Kromasil C , ANM05CMJ25 Kromasil C , ANM05CMB10 Kromasil C ANM05CMB1F Kromasil C ANM05CMB15 Kromasil C ANM05CMB20 Kromasil C ANM05CMB25 Kromasil C ANM05CMA10 Kromasil C , ANM05CMA1F Kromasil C , ANM05CMA15 Kromasil C , ANM05CMA20 Kromasil C , ANM05CMA25 Kromasil C , KROMASIL PHENYL COLUMNS High quality sperical silica gel. Kromasil Pheny is a good alternative to standard RP phases like C18 or C8 due to another selectivity. art.no. description length (mm) diameter (mm) particle size (µm) pore size quantity ANM05PHD10 Kromasil Phenyl 100 2, ANM05PHD15 Kromasil Phenyl 150 2, ANM05PHD25 Kromasil Phenyl 250 2, ANM05PHC10 Kromasil Phenyl ANM05PHC1F Kromasil Phenyl ANM05PHC15 Kromasil Phenyl ANM05PHC25 Kromasil Phenyl ANM05PHB10 Kromasil Phenyl ANM05PHB1F Kromasil Phenyl ANM05PHB15 Kromasil Phenyl ANM05PHB25 Kromasil Phenyl ANM05PHA10 Kromasil Phenyl 100 4, ANM05PHA1F Kromasil Phenyl 125 4, ANM05PHA15 Kromasil Phenyl 150 4, ANM05PHA25 Kromasil Phenyl 250 4, page 43 Other dimensions are available on request.

45 chiral columns by daicel 20. Chiral columns by Daicel IMMOBILIZED TYPE CHIRAL HPLC COLUMNS CHIRALPAK I-SERIES High solvent versality in the selection oft the mobile phase composition High selectivity in the resolution of the enantiomers Robustness and extended durability Easy use of the columns Chiralpak IA: AMYLOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) IMMOBILISED ON A SILICA SUPPORT art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC80323 CHIRALPAK IA 100 4,6 5 1 DAIC80324 CHIRALPAK IA 150 4,6 5 1 DAIC80325 CHIRALPAK IA 250 4,6 5 1 Chiralpak IA-3: AMYLOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) IMMOBILISED ON A SILICA SUPPORT art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC80523 CHIRALPAK IA ,6 3 1 DAIC80524 CHIRALPAK IA ,6 3 1 DAIC80525 CHIRALPAK IA ,6 3 1 Chiralpak IB: CELLULOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) IMMOBILISED ON A SILICA SUPPORT art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC81323 CHIRALPAK IB 100 4,6 5 1 DAIC81324 CHIRALPAK IB 150 4,6 5 1 DAIC81325 CHIRALPAK IB 250 4,6 5 1 Please note: Other Chiral Phases and Dimensions are also available page 44

46 chiral columns by daicel Chiralpak IB-3: CELLULOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) IMMOBILISED ON A SILICA SUPPORT art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC81523 CHIRALPAK IB ,6 3 1 DAIC81524 CHIRALPAK IB ,6 3 1 DAIC81525 CHIRALPAK IB ,6 3 1 Chiralpak IC: CELLULOSE TRIS (3,5-DICHLOROPHENYLCARBAMATE) IMMOBILISED ON A SILICA SUPPORT art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC83324 CHIRALPAK IC 150 4,6 5 1 DAIC83325 CHIRALPAK IC 250 4, Chiralpak IC-3: CELLULOSE TRIS (3,5-DICHLOROPHENYLCARBAMATE) IMMOBILISED ON A SILICA SUPPORT art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC83523 CHIRALPAK IC ,6 3 1 DAIC83524 CHIRALPAK IC ,6 3 1 DAIC83525 CHIRALPAK IC ,6 3 1 Chiralpak ID: AMYLOSE TRIS(3-CHLOROPHENYLCARBAMATE) IMMOBILISED ON 5 µm SILICA GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC84323 CHIRALPAK ID 100 4,6 3 1 DAIC84324 CHIRALPAK ID 150 4,6 3 1 DAIC84325 CHIRALPAK ID 250 4,6 3 1 Chiralpak ID-3: AMYLOSE TRIS(3-CHLOROPHENYLCARBAMATE) IMMOBILISED ON 3µM SILICA GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC84523 CHIRALPAK ID ,6 3 1 DAIC84524 CHIRALPAK ID ,6 3 1 DAIC84525 CHIRALPAK ID ,6 3 1 page 45 Please note: Other Chiral Phases and Dimensions are also available

47 chiral columns by daicel Chiralpak IE: AMYLOSE TRIS (3,5-DICHLOROPHENYLCARBAMATE) IMMOBILISED ON 5 µm SILICA GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC85323 CHIRALPAK IE 100 4,6 5 1 DAIC85324 CHIRALPAK IE 150 4,6 5 1 DAIC85325 CHIRALPAK IE 250 4,6 5 1 Chiralpak IE-3: AMYLOSE TRIS (3,5-DICHLOROPHENYLCARBAMATE) IMMOBILISED ON 3 µm SILICA GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC85523 CHIRALPAK IE ,6 3 1 DAIC85524 CHIRALPAK IE ,6 3 1 DAIC85525 CHIRALPAK IE ,6 3 1 Chiralpak IF: AMYLOSE TRIS (3-CHLORO-4-METHYLPHENYLCARBAMATE) IMMOBILISED ON 5 µm SILICA GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC86323 CHIRALPAK IF 100 4,6 5 1 DAIC86324 CHIRALPAK IF 150 4,6 5 1 DAIC86325 CHIRALPAK IF 250 4,6 5 1 Chiralpak IF-3: AMYLOSE TRIS (3-CHLORO-4-METHYLPHENYLCARBAMATE) IMMOBILISED ON 3 µm SILICA GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC86523 CHIRALPAK IF ,6 3 1 DAIC86524 CHIRALPAK IF ,6 3 1 DAIC86525 CHIRALPAK IF ,6 3 1 Please note: Other Chiral Phases and Dimensions are also available page 46

48 chiral columns by daicel NORMAL PHASE COLUMNS most widely used for chiral separations available from semi-micro to preparative type 3 and 5 µm type available Chiralcel OD-H: CELLULOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 5 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC14323 CHIRALCEL OD-H 100 4,6 5 1 DAIC14324 CHIRALCEL OD-H 150 4,6 5 1 DAIC14325 CHIRALCEL OD-H 250 4,6 5 1 Chiralcel OD-3: CELLULOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 3 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC14523 CHIRALCEL OD ,6 3 1 DAIC14524 CHIRALCEL OD ,6 3 1 DAIC14525 CHIRALCEL OD ,6 3 1 Chiralcel OJ-H: CELLULOSE TRIS (4-METHYLBENZOATE)COATED ON 5 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC17323 CHIRALCEL OJ-H 100 4,6 5 1 DAIC17324 CHIRALCEL OJ-H 150 4,6 5 1 DAIC17325 CHIRALCEL OJ-H 250 4,6 5 1 Chiralcel OJ-3: CELLULOSE TRIS (4-METHYLBENZOATE) COATED ON 3 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC17523 CHIRALCEL OJ ,6 3 1 DAIC17524 CHIRALCEL OJ ,6 3 1 DAIC17525 CHIRALCEL OJ ,6 3 1 page 47 Please note: Other Chiral Phases and Dimensions are also available

49 chiral columns by daicel Chiralpak AD-H: AMYLOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 5 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC19323 CHIRALPAK AD-H 100 4,6 5 1 DAIC19324 CHIRALPAK AD-H 150 4,6 5 1 DAIC19325 CHIRALPAK AD-H 250 4,6 5 1 Chiralpak AD-3: AMYLOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 3 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC19523 CHIRALPAK AD ,6 3 1 DAIC19524 CHIRALPAK AD ,6 3 1 DAIC19525 CHIRALPAK AD ,6 3 1 Chiralpak AS-H: AMYLOSE TRIS [(S)-α-METHYLBENZYLCARBAMATE] COATED ON 5 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC20323 CHIRALPAK AS-H 100 4,6 5 1 DAIC20324 CHIRALPAK AS-H 150 4,6 5 1 DAIC20325 CHIRALPAK AS-H 250 4,6 5 1 Chiralpak AS-3: AMYLOSE TRIS [(S)-α-METHYLBENZYLCARBAMATE] COATED ON 3 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC20523 CHIRALPAK AS ,6 3 1 DAIC20524 CHIRALPAK AS ,6 3 1 DAIC20525 CHIRALPAK AS ,6 3 1 REVERSED PHASE COLUMNS for reverse phase use available for LC-MS 3 and 5 µm type available usable for aqeous organic phases high ph flexibility Please note: Other Chiral Phases and Dimensions are also available page 48

50 chiral columns by daicel Chiralpak AD-RH: AMYLOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 5 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC19724 CHIRALPAK AD-RH 150 4,6 5 1 DAIC CHIRALPAK AD-RH 150 2,1 5 1 Chiralpak AD-3R: AMYLOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 3 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC19824 CHIRALPAK AD-3R 150 4,6 3 1 DAIC19894 CHIRALPAK AD-3R 150 2,1 3 1 Chiralpak AS-RH: AMYLOSE TRIS [(S)-α-METHYLBENZYLCARBAMATE] COATED ON 5 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC CHIRALPAK AS-RH 150 4,6 5 1 DAIC CHIRALPAK AS-RH 150 2,1 5 1 Chiralpak AS-3R: AMYLOSE TRIS [(S)-α-METHYLBENZYLCARBAMATE] COATED ON 3 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC CHIRALPAK AS-3R 150 4,6 3 1 DAIC CHIRALPAK AS-3R 150 2,1 3 1 Chiralpak OD-RH: CELLULOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 5 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC CHIRALCEL OD-RH 150 4,6 5 1 DAIC CHIRALCEL OD-RH 150 2,1 5 1 Chiralpak OD-3R CELLULOSE TRIS (3,5-DIMETHYLPHENYLCARBAMATE) COATED ON 3 µm SILICA-GEL art.no. description length (mm) diameter (mm) particle size (µm) quantity DAIC CHIRALCEL OD-3R 150 4,6 3 1 DAIC CHIRALCEL OD-3R 150 2,1 3 1 page 49 Please note: Other Chiral Phases and Dimensions are also available

51 hplc columns by grace 21. HPLC columns by Grace Previously these HPLC columns were supplied by Grace. The column division of Grace has been taken over by different manufacturers. With Altmann Analytik, you can get all the columns from one source as usual. Vydac TP columns are used as standard for the analysis of peptides and proteins. A pore size of 300 angstroms ensures that the polypeptides can be taken up unrestrictedly by the pores of the silica gel. GENERAL CHARACTERISTICS OF VYDAC COLUMNS: Long lifetime Reliable protein purification, easy upscaling from analytical to preparative scale vydac tp phase functional group particle size chromatographic properties application usp code Vydac 218TP C18 3, 5, 10 First generation of polymer C18 phase with unique selectivity Vydac 238TP C18 5 First generation of monomeric C18 phase Small polypeptides 4-5K MW, enzymatic digestion, synthetic peptide Same application as 218 TP, different selectivity Vydac 208TP C8 5 Phase with lower hydrophobicity compared to C18TP Polypeptides 10-20K MW L7 Vydac 214TP C4 5,10 First generation C4 phase Glycoproteins, histons, insuline, membrane proteins L26 Vydac 214ATP C4 5 C4 phase with less endcapping Ideal for the analysis of Human Growth Hormones L26 Vydac 219TP Diphenyl 5,10 First generation diphenyl phase Polypeptides with aromatic sidechains, big hydrophobic proteins, L11 lipid peptides, fusionproteins Vydac 201TP C18 5, 10 Not endcapped C18 phase Separation of PAHs L1 Vydac 202TP C18 5 Higher carbon content than 201 TP Separation of PAHs L1 L1 L1 art.no. description length (mm) diameter (mm) particle size (µm) quantity GR Vydac 201TP C18 Column GR Vydac 201TP C18 Column GR Vydac 208TP C8 Column GR Vydac 208TP C8 Column GR Vydac 214MS C4 Column GR Vydac 214MS C4 Column GR Vydac 214TP C4 Column GR Vydac 214TP C4 Column GR Vydac 218MS C18 Column GR Vydac 218MS C18 Column Additional dimensions and phases are available on request page 50

52 hplc columns by grace art.no. description length (mm) diameter (mm) particle size (µm) quantity GR Vydac 218TP C GR Vydac 218TP C GR Vydac 219TP Diphenyl Column GR Vydac 219TP Diphenyl Column GR Vydac 238TP C18 Column GR Vydac 238TP C18 Column ALLTIMA HP Alltima HP columns offer a superior product range of low-flow, low-metal, and specific selectivity variants of reverse-phase packing materials. art.no. description length (mm) diameter (mm) particle size (µm) quantity GR AlltimaHP C18 Column GR AlltimaHP C18 Column GR AlltimaHP C8 Column GR AlltimaHP C8 Column GR Alltima Phenyl Column GR Alltima Phenyl Column ALLTIMA COLUMNS Alltima columns offer a wide range of column formats, which are high-quality all-purpose columns. art.no. description length (mm) diameter (mm) particle size (µm) quantity GR Alltima C18 Column GR Alltima C18 Column GR Alltima C8 Column GR Alltima C8 Column GR Alltima Phenyl Column GR Alltima Phenyl Column VISION Broad selectivity range, unique complementary phase chemistries. Separation of complex samples with excellent resolution art.no. description length (mm) diameter (mm) particle size (µm) quantity GR VisionHT C18 Polar GR VisionHT C18 Polar ECONOSPHERE Econosphere columns are used for simple, general chromatographic applications and offer a cost-effective alternative to other columns. art.no. description length (mm) diameter (mm) particle size (µm) quantity GR Econosphere C18 Column GR Econosphere C18 Column GR Econosphere C8 Column GR Econosphere C8 Column page 51 Additional dimensions and phases are available on request

53 hplc columns by macherey-nagel 22. HPLC columns by Macherey-Nagel GUARD COLUMN NUCLEODUR PI 2 art.-no. description MN EC 4/2 NUCLEODUR Pi2, 5 µm MN EC 4/3 NUCLEODUR Pi2, 5 µm MN Column-Protection-System guard column holder NUCLEODUR PI 2 Biphenylpropyl modification with multi-end capping Hydrophobic phase with alternative selectivities to classical C18 phases Separation is based on 2 mechanisms: π-π and hydrophobic interactions Better retention of aromatic molecules Good performance even at 100 % aqueous conditions art.-no. description length (mm) diameter (mm) particle size (µm) quantity MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI Additional dimensions and phases are available on request page 52

54 hplc columns by macherey-nagel art.-no. description length (mm) diameter (mm) particle size (µm) quantity MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI MN EC Nucleodur PI NUCLEODUR High-purity silica phase for HPLC Suitable for routine analysis or upscaling available in pore sizes of 100 and 300 angstroms art.-no. description length (mm) diameter (mm) particle size (µm) quantity MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec MN EC Nucleodur C18 ec page 53 Additional dimensions and phases are available on request

55 sielc columns 23. SIELC columns Primesep columns are specifically designed for mixed-mode separations and capable of separating a huge range of compounds by different separation modes based only upon mobile phase selection. Primesep A (strongest acidic phase) are columns with negatively charged funcional groups due to the embedded anionic ion-pairing reagent. Primesep A: REVERSE-PHASE ANALYTICAL COLUMN WITH EMBEDDED STRONG ACIDIC ION PAIRING GROUPS improves retention of weak basic compounds by cation-exchange mechanism separates acid by ion-exclusion mechanism retains neutral compounds by RP-mechanism art.no. description length (mm) diameter (mm) particle size (µm) quantity SLA Primesep A 100 4,6 5 1 SLA Primesep A 150 4,6 5 1 SLA Primesep A 250 4,6 5 1 Primesep 100 (strong acidic phase): COLUMNS WITH NEGATIVELY CHARGED FUNCTIONAL GROUPS DUE TO THE EMBEDDED ANIONIC ION-PAIRING GROUPS most versatile column of primesep family for separation of a broad range of compounds improves retention of basic compounds by cation-exchange mechanism separates acid by ion-exclusion mechanism retaines neutral compounds by RP-mechanism art.no. description length (mm) diameter (mm) particle size (µm) quantity SL Primesep ,6 3 1 SL Primesep ,6 3 1 SL Primesep ,6 3 1 SL Primesep ,6 5 1 SL Primesep ,6 5 1 SL Primesep ,6 5 1 Primesep B: PRIMESEP B IS A RP COLUMN WITH EMBEDDED BASIC ION-PAIRING GROUP improves retention of acidic compounds by anion exchange mechanism separates bases by ion-exclusion mechanism retains neutral compounds by RP mechanism art.no. description length (mm) diameter (mm) particle size (µm) quantity SLB Primesep B 100 4,6 5 1 SLB Primesep B 150 4,6 5 1 SLB Primesep B 250 4,6 5 1 Additional dimensions and phases are available on request page 54

56 sielc columns Primesep P: PRIMESEP P IS A RP PHASE WITH EMBEDDED AROMATIC AND ACIDIC ION PAIRING GROUPS improves retention of basic compounds by cation-exchange mechanism separates aromatic compounds by pi-pi interaction retains neutral compounds by RP-mechanism art.no. description length (mm) diameter (mm) particle size (µm) quantity SLP Primesep P 100 4,6 5 1 SLP Primesep P 150 4,6 5 1 SLP Primesep P 250 4,6 5 1 Obelisc R: OBELISC R IS A RP COLUMN AND CAN BE USED IN TRADITIONAL, RP-TYPE APPLICATIONS due to presence of ionic groups and a long hydrophobic chain the column offers additional retention and separation that is not available with traditional RP-columns multiple separation modes (RP, NP, IE) art.no. description length (mm) diameter (mm) particle size (µm) quantity SLOR Obelisc R 100 4,6 5 1 SLOR Obelisc R 150 4,6 5 1 SLOR Obelisc R 250 4,6 5 1 Obelisc N: OBELISC N IS A COLUMN WITH VERY POLAR CHARACTERISTICA AND WORKS WELL FOR POLAR AND CHARGED ANALYTES offers both positively and negatively charged goups to interact with positively or negatively charged analytes multiple separation modes (HILIC, NP, IE) In Hilic mode, Obelisc offers different selectivity from other Hilic columns art.no. description length (mm) diameter (mm) particle size (µm) quantity SLON Obelisc N 100 4,6 5 1 SLON Obelisc N 150 4,6 5 1 SLON Obelisc N 250 4,6 5 1 page 55 Additional dimensions and phases are available on request

57 tubing and fitting by upchurch 24. Tubing and Fitting by Upchurch PEEK TUBING UP1531: Peek Tubing natural, biocompatible and optimized for use in high-pressure application. High inertness. art.-no. description tubing od (in) tubing id (in) length pressure limit (psi) UP1531 Tubing natural 1/16 0,010 5 ft 7000 UP1531L Tubing natural 1/16 0, ft 7000 UP1531XL Tubing natural 1/16 0, ft 7000 UP1536: Biocompatible, PEEK Tubing is optimized for use in high-pressure applications. Its distinct materials make it inert to most solvents and give it a smooth internal surface that improves the resolution of sample bands. A variety of color options for easy coding and identification is available. It comes in yellow. art.-no. description tubing od (in) tubing id (in) length pressure limit (psi) UP1536 Tubing yellow 1/16 0,007 5 ft 7000 UP1536L Tubing yellow 1/16 0, ft 7000 UP1536XL Tubing yellow 1/16 0, ft 7000 UP1577: Biocompatible, PEEK Tubing is optimized for use in high-pressure applications. Its distinct materials make it inert to most solvents and give it a smooth internal surface that improves the resolution of sample bands. A variety of color options for easy coding and identification is available. It comes in yellow. art.-no. description tubing od (in) tubing id (in) length pressure limit (psi) UP1577 Tubing yellow 1/32 0,007 5 ft 5000 UP1577L Tubing yellow 1/32 0, ft 5000 UP1577XL Tubing yellow 1/32 0, ft 5000 UP1581: Biocompatible, PEEK Tubing is optimized for use in high-pressure applications. Its distinct materials make it inert to most solvents and give it a smooth internal surface that improves the resolution of sample bands. A variety of color options for easy coding and identification is available. It comes in blue. art.-no. description tubing od (in) tubing id (in) length pressure limit (psi) UP1581 Tubing yellow 1/32 0,010 5 ft 5000 UP1581L Tubing yellow 1/32 0, ft 5000 UP1581XL Tubing yellow 1/32 0, ft 5000 page 56

58 upchurch STAINLESS STEEL TUBING Stainless Steel Tubing is specifically designed to meet the exacting requirements of today's analyses. The pre-cut tubing is put through rigorous preparation that leave it ready to use with flat, burr free ends and a clean finish. This thorough process results in zero dead volume connections and excellent chromatographic results. art.-no. description tubing od (in) tubing id (in) length (cm) pressure limit (psi) UPU-115 Stainless Steel Tubing 1/16 0, UPU-116 Stainless Steel Tubing 1/16 0, UPU-117 Stainless Steel Tubing 1/16 0, UPU-138 Stainless Steel Tubing 1/16 0, UPU-139 Stainless Steel Tubing 1/16 0, UPU-140 Stainless Steel Tubing 1/16 0, CAPILLARY POLYMER TUBING CUTTER art.-no. description tubing od (in) quantity UPA-327 Plastic Tubing cutter 1/8 or 1/16 1/Pkg UPA-328 Tubing cutter Blade 5/Pkg UPA-329 Polymer Tubing Cutter Large bore 3/16 or 3/16 1/Pkg UPA-350 Tube Cutter Capillary Polymer 1/32 1/Pkg ONE PIECE FINGERTIGHT FITTING The original One-Piece Fingertight Fittings offer the convenience of making a tubing connection without the need for wrenches or specialized tools when tightening the fitting into place. Simply use your fingers to tighten the fitting into the receiving port! It has a Coned thread port configuration and is for 1/16" tubing OD. art.-no. description tubing od (in) thread port pressure limit (psi) quantity F-100x F-120x One Piece Fingertight Male nut One Piece Fingertight Male nut 1/ / STAINLESS STEEL FITTINGS The Two-Piece Stainless Steel Fitting and Ferrule is specifically designed for the rigid requirements of our high pressure rated valves. art.-no. description tubing od (in) thread port pressure limit (psi) quantity RY Rheodyne SST Fitting 1/16 coned, 5/16" RY Two Piece SST Fitting 1/ RY Rheodyne SST Ferrule 1/ page 57

59 upchurch TWO-PIECE FINGERTIGHT FITTINGS AND FERRULE This PEEK Double Winged Fingertight Fitting offers the convenience of making a tubing connection without the need for wrenches or specialized tools when tightening the fitting into place. Simply use your fingers to tighten the fitting into the receiving port! The fitting is designed for easy connecting to 1/6"OD tubing. The ferrule is part number F-142 and can be ordered separately. art.-no. description tubing od (in) thread port pressure limit (psi) quantity UPF-300x Two-Piece Fingertight Fitting 1/ UPF-330x Two-Piece Fingertight Fitting long 1/ UPF-142 Fingertight Ferrule 1/ MARVELX Easy-to-use MarvelX Biocompatible PEEK-Lined UHPLC Connection Systems from IDEX Health & Science eliminates dead volume and provides higher repeat uses without sacrificing from consistent performance. The biocompatible PEEK-lined connection system has been specially designed to allow for easier routing and superior re-usability throughout your instrument. Built with a convenient, removable fitting and changeable precision-cut flexible tubing, MarvelX can be used up to 200 times! It is compatible with coned receiving ports for easy and repeatable finger-tight connections no tool required. Innovative design makes it possible to replace tubing independent of fittings. Similar to Viper Capillary Steel Fingertight Fittings. art.-no. description tubing od (in) tubing id (in) length (mm) thread port pressure limit (psi) quantity UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends 0, UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends 0, UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends UPUPFP Peek-Lined Stainless Steel 1/32"OD Flexible 316 Stainless Steel with 1/16" OD rigid tube ends page 58

60 upchurch UNIONS: The PEEK ZDV Union Assembly ensures a reliable connection for tubing. It effectively addresses this need in the high pressure region of a system where a dependable connection is imperative. Our assembly includes (2) F-300 Fingertight Fittings. art.-no. description tubing od (in) thread port thru hole (in) pressure limit (psi) UPP-704 Peek ZDV Union Assembly (union and 2 fingertight fittings) 1/ coned UPP-742 Peek ZDV Union Assembly (union and 2 fingertight fittings) 1/ coned UPP-760 Peek ZDV Union Assembly (union and 2 fingertight fittings) 1/ coned quantity TIGHTENING TOOLS: art.-no. description fitting material torque delivered head style UPP-1000 Standard Knurl Torque Tool VHP Fitting PCTFE 0.45 Nm Standard Knurl 1 UPVHP-1000 VHP Wrench VHP Fitting PCTFE 1.3 Nm ¼ Hex 1 UPVHP-2000 VHP Wrench VHP Fitting PCTFE 1.58 Nm ¼ Hex 1 quantity page 59

61 storage system consumables 25. Storage System Consumables STORAGE SYSTEM PORTABLE Our storage systems in a portable und in a lab bench version helps to keep small consumable parts well arranged. art.no. description dimensions AAOBP18F Portable Storage case for consumables, with 18 compartments 350x200x465 STORAGE SYSTEM FOR LAB BENCH art.no. AAOB655 AAOB5669 AAOB99666 description Case for consumables 3 Levels 16 compartments Case for consumables 4 Levels 26 compartments Case for consumables 5 Levels 36 compartments page 60

62 degasser 26. Degasser INSTRUMENTAL ANALYTICS AND GENERAL CHROMATOGRAPHY Due to the high permeability Systec AF membrane the internal volume is excellent for degassing efficiency for flow rates up to 3 ml/min. High degassing efficiency Suitable for all systems Long Lifetime Biocompatible special offer: when ordering a degasser device, the tubing & fitting is included for free! art.-no. description channels volume BT A 2-channel Biotech DEGASI Plus Classic Degasser, 480 µl Systec AF µl BT A 3-channel Biotech DEGASI Plus Classic Degasser, 480 µl Systec AF µl BT A 4-channel Biotech DEGASI Plus Classic Degasser, 480 µl Systec AF µl BT A 5-channel Biotech DEGASI Plus Classic Degasser, 480 µl Systec AF µl FITTINGS AND TUBINGS art.-no. description BT0704 BT1608 FEP Tubing 1/8 OD x 1/16 ID, 5 meter One-piece Superflangeless Fittings, 10 pcs PEEK Nuts 1/4-28 with integrated PEEK ferrules 1/8 ID GPC AND NORMAL PHASE CHROMATOGRAPHY art.-no. channels volume BT Hohe Entgasungseffizienz µl BT Passend für alle Systeme µl BT Lange Lebensdauer µl Biokompatibel BT µl page 61

63 safety caps/waste cap accessories 27. Safety caps/waste cap accessories The release of solvents is prevented, and no contamination of the mobile phase from the room air is possible. GL45 thread for Schott and Duran. Smart Healthy Caps are a cost-effective alternative to SCAT-Europe products. article description art.-no. oem scat europe Smart Healthy Cap1 1 Port and 1 Air check ventile AISHC Smart Healthy Cap2 2 Ports Outlet and 1 Air check ventile AISHC Smart Healthy Cap3 3 Ports Outlet and 1 Air check ventile AISHC Smart Healthy Cap with lock valve Safe collection system for HPLC solvents with aeration valve and shut-off valve. More flexibility and no air bubbles in the tubing. GL45 thread for Schott and Duran. article description art.-no. oem scat europe Smart Healthy Cap V1 1 connection with shut-off valve and 1 air check valve AISHC-V Smart Healthy Cap V2 2 connections with shut-off valve and 1 air check valve AISHC-V Smart Healthy Cap3 3 connections with shut-off valve and 1 air check valve AISHC-V Spare Air Check Valve article description art.-no. oem scat europe Air Check valve 10 Air Check valves AISHC-SV Air Check valve 50 Air Check valves AISHC-SV Smart Healthy Cap Adapter for other thread sizes article description art.-no. oem scat europe GL40 PTFE Adapter for GL40 thread AIAD-40-T GL38 PTFE Adapter for GL38 thread AIAD-38-T GL32 PTFE Adapter for GL32 thread AIAD-32-T Activated carbon filter cartridge for Smart Waste Caps Each cartridge is supplied with a label for the date and change date of the filter. The shelf life of the filter depends on the size. article description art.-no. oem scat europe Charcoal cartridge filter 25 gram AIFC Charcoal cartridge filter 50 gram AIFC Charcoal cartridge filter 100 gram AIFC Further sizes and specifications on request. page 62

64 deuterium lamps 28. Deuterium lamps for the HPLC laboratory Deuterium lamps provide an almost continuous light spectrum from the UV wavelength range ( nm) to the visible spectral range ( nm) and burn very stable, which is why they are particularly suitable for spectroscopic investigations. The high-quality deuterium lamps we offer have a lifetime of 1000 to 2000 hours. All lamps also have quartz glass or UV glass flasks. We offer lamps (e.g. D2 deuterium lamps) for the devices of all current manufacturers. For example: Agilent lamps, Perkin Elmer lamps, Varian lamps, Waters lamps and much more. art.-no. description for devices of KILD-AGI-104LL Deuterium (D2) lamp long life for Agilent 1100, 1200, 1260 VWD Agilent KILD-AGI-108LL Deuterium (D2) lamp long life for Agilent 1260, 1290 Infinity DAD (8 Pin) Agilent KILD-AGI-105LL Deuterium (D2) lamp long life for Agilent 1100, 1200, 1260 DAD Agilent HN Deuterium lamp (D2) for Waters 486 Waters KILD-WAT-105LL Deuterium (D2) lamp long life for Waters 2487, 2488 Waters KILD-WAT-104LL Deuterium (D2) lamp long life for Waters 996, 2996 PDA Waters HN Deuterium lamp (D2) for Waters 2996/996 Waters HN Deuterium lamp (D2) for Waters 2487 dual wave- length, 2488 dual wavelength, Acquity UPLC TUV Waters HN Deuterium lamp (D2) for Dionex AD-25/PDA-100/UltiMate PDA-3000 Dionex HN Deuterium lampe (D2) for Alpkem, Biorad, Biotronic, Dionex, GAT, Spectra, Dionex HN Deuterium lamp (D2) for Dionex UltiMate DAD/MWD/VWD Dionex HN Deuterium lamp (D2) for Dionex UltiMate UVD-3000 Dionex HN Deuterium lamp (D2) for Dionex UV-Vis Spectrometer UVD Dionex HN Deuterium lamp (D2) for Hitachi Hitachi HN Deuterium lamp (D2) for Shimadzu SPD Shimadzu HN Deuterium lamp (D2) for Shimadzu SPD-M10x Shimadzu HN Deuterium lamp (D2) for Shimadzu SPD-6/7 Shimadzu HN Deuterium lamp (D2) for Shimadzu LC 2010x Shimadzu HN Deuterium Lampe (D2) for Varian Varian HN Deuterium lamp (D2) for Perkin Elmer, Hitachi Perkin Elmer, Hitachi page 63

65 tungsten lamps for hplc-laboratory 29. Tungsten lamps for the HPLC laboratory The series of tungsten halogen lamps are specifically for use in analytical applications. Special quartz envelopes enable high transmission below 380 nm and the position of the tungsten filament is closely controlled through precise alignment. The lamps offer high colour temperature, luminous efficacy and long life. Tungsten lamps are filled with a halogen gas mixture specific to their final application and range from 5 W 200 W, with typical lifetimes of more than 2,000 hours. art.-no. description for devices of HN Tungsten (VIS) Lamp for Beckman, Pharmacia, Shimadzu Shimadzu HN Tungsten (VIS) Lamp for Shimadzu SPD-10x/20x Shimadzu HN Tungsten (VIS) Lamp for PerkinElmer Perkin Elmer HN Tungsten (VIS) Lamp for PerkinElmer Lambda series Perkin Elmer HN Tungsten (VIS) Lamp for Dionex AD-25/PDA-100/UltiMate PDA-3000 Dionex HN Tungsten (VIS) Lamp for Dionex UltiMate DAD/MWD/UVD/VWD Dionex HN Tungsten (VIS) Lamp for Thermo Spectronic, Unicam Helios Thermo, Unicam 30. Lamps for Atom Absorption Spectroscopy (AAS) Hollow cathode lamps (HCL) are discharge lamps designed for use in Atomic Absorption (AA) instruments. They consist of a cathode made from the element of interest, an anode and an inert filler gas contained in a glass envelope. Heraeus offers the widest selection of single- and multielement coded / non-coded in low and high-current, 37 mm and 50 mm lamps in the industry. 37 MM STANDARD 50 MM STANDARD art.-no. description size art.-no. description size element quantity element quantity HN HCL single element Al 37 mm 1 HN HCL single element Co 37 mm 1 HN HCL single element Fe 37 mm 1 HN HCL single element Pb 37 mm 1 HN HCL single element Mg 37 mm 1 HN HCL single element Hg 37 mm 1 HN HCL single element Ni 37 mm 1 HN HCL single element Al 50 mm 1 HN HCL single element Co 50 mm 1 HN HCL single element Fe 50 mm 1 HN HCL single element Pb 50 mm 1 HN HCL single element Mg 50 mm 1 HN HCL single element Hg 50 mm 1 HN HCL single element Ni 50 mm 1 page 64

66 lamps for aas AGILENT/VARIAN art.-no. description element size quantity HN HCL single element Al 37 mm 1 HN HCL single element Co 37 mm 1 HN HCL single element Fe 37 mm 1 HN HCL single element Pb 37 mm 1 HN HCL single element Mg 37 mm 1 HN HCL single element Hg 37 mm 1 HN HCL single element Ni 37 mm 1 PERKINELMER art.-no. description element size quantity HN HCL single element Al 50 mm 1 HN HCL single element Co 50 mm 1 HN HCL single element Fe 50 mm 1 HN HCL single element Pb 50 mm 1 HN HCL single element Mg 50 mm 1 HN HCL single element Hg 50 mm 1 HN HCL single element Ni 50 mm 1 UNICAM/THERMO art.-no. description element size quantity HN HCL single element Al 37 mm 1 HN HCL single element Co 37 mm 1 HN HCL single element Fe 37 mm 1 HN HCL single element Pb 37 mm 1 HN HCL single element Mg 37 mm 1 HN HCL single element Hg 37 mm 1 HN HCL single element Ni 37 mm 1 page 65 Further elements as well as multi-element lamps are available on request!

67 graphite tubes by altmann analytik 31. Graphite Tubes by Altmann Analytik GBC art.-no. description quantity ASP Shroud for GBC ASP Standard tube, pyrocoated, with rings for GBC EL-ASP Standard tube, coated, longlife for GBC ASP Standard tube, uncoated, for GBC ASP Electrode/Contact for GBC ASP Standard tube, pyrocoated, Omega platform for GBC 10 HITACHI art.-no. description quantity ASP Zeeman Contact, OD 18 mm for Hitachi ASP Zeeman Contact, OD 18 mm for Hitachi ASP Standard tube, uncoated, with segment for Hitachi ASP Electrode / Contact, OD 20 mm for Hitachi ASP Platform, L vov type for Hitachi ASP Standard tube, pyrocoated, with segment for Hitachi ASP Tube, pyrocoated, with Omega platform for Hitachi 10 PERKIN ELMER art.-no. description quantity B ASP Tube, pyrocoated, with L vov platform for PerkinElmer 10 B ASP Contact set for Z-AASfor PerkinElmer 1 B ASP Platform, L vov type, Pyro graphite for PerkinElmer, 10 B ASP Tube, coated, for L vov platform for PerkinElmer 10 B ASP Tube, uncoated, for L vov platform for PerkinElmer 10 B ASP Contact set, with sensor hole for PerkinElmer, HGA 400/500 1 B ASP Contact set, w/o sensor hole for PerkinElmer, HGA 300/600/700/800 1 B ASP Tube, pyrocoated, with grooves for PerkinElmer 10 B ASP Tube, uncoated,with grooves for PerkinElmer 10 B ASP Central pr. Insert for PerkinElmer 10 B ASP Graphitpipe for central prob, coated for PerkinElmer 10 page 66

68 graphite tubes by altmann analytik SHIMADZU art.-no. description quantity ASP Tube, uncoated, plane 60 for Shimadzu ASP Tube, pyrocoated, plane 60 for Shimadzu ASP Left contact, 90 for Shimadzu ASP Right contact, 90 for Shimadzu ASP Tube, coated, with forked platform for Shimadzu ASP Right contact, 60 for Shimadzu ASP Left contact, 60 for Shimadzu ASP Tube, coated, with forked platform for Shimadzu 10 THERMO ELECTRON art.-no. description quantity ASP Standard tube plain, uncoated Thermo Electron ASP Standard tube plain, coated Thermo Electron ASP Partridged tube plain, uncoated Thermo Electron ASP Contacts, standard Electrode for Thermo Electron ASP Tube, uncoated, halfrings for Thermo Electron ASP Tube, pyrocoated, longlife for Thermo Electron ASP Tube, pyrocoated, halfrings for Thermo Electron ASP Tube, pyrocoated for Thermo Electron ASP Contacts, Zeeman Electrode for Thermo Electron 2 VARIAN art.-no. description quantity ASP Plateau-tube, coated for Varian ASP Tube, pyrocoated, with rings for Varian EL-ASP Tube, pyro coated, with rings, Longlife for Varian ASP Bone-Platform, Pyro graphite for Varian ASP Electrodes/contacts for SpectrAA for Varian ASP Zeeman Electrode for Varian ASP Shroud for SpectrAA for Varian ASP Zeeman Shroud for Varian ASP Tube, coated, with Omega-Platform for Varian 10 page 67

69 cuvettes 32. Cuvettes It is particularly important for a problem-free operation with cuvettes that the light can only penetrate the interior. Therefore, the light beam cross-section should always be selected appropriately and the cuvette must be exactly aligned in the holder. The light beam cross-section must be selected to be smaller than the inner width. This ensures that neither the side walls nor the ground are touched by the light beam. In photometry, the macrocuvette has largely established itself as a standard. It is defined as follows: The designation macro cuvette applies according to DIN58963, if the inner space is wider than 5 mm in a stretch cuvette. For a cylinder cuvette, the inside diameter must be over 8mm, so that it can be counted in this category. MACRO CUVETTES art.no. description layer thickness size inner width (mm) volume (µl) quantity HL Macro cuvette 100-OS 5 45x12,5x7,5 9, HL Macro cuvette 100-OS 10 45x12,5x12,5 9, HL Macro cuvette 100-OS 20 45x12,5x22,5 9, HL Macro cuvette 100-OS 40 45x12,5x42,5 9, art.no. description layer thickness size inner width (mm) volume (µl) quantity HL Macro cuvette 100-QS 5 45x12,5x7,5 9, HL Macro cuvette 100-QS 10 45x12,5x12,5 9, HL Macro cuvette 100-QS 20 45x12,5x22,5 9, HL Macro cuvette 100-QS 40 45x12,5x42,5 9, The micro cuvette has a smaller volume. It is either a rectangle cuvette with an inside space up to 2mm or a cylinder cuvette with an inner diameter up to 5 mm. MIKRO CUVETTES Die Bezeichnung Makro-Küvette trifft nach DIN58963 zu, art.no. description layer thickness size inner width (mm) volume (µl) quantity HL Mikro Cuvette 104 OS 10 45x12,5x12, HL Mikro Cuvette 104 QS 10 45x12,5x12, HL Mikro Cuvette 105 QS 10 25x12,5x12, QS: QS is the identification logo which indicates that Quartz of the highest purity and homogeneity has been used for the window. Because it is produced from a silicon compound, it is also called synthetic Quartz. Hellma use Quartz SUPRASIL from Heraeus Quarzglas GmbH, with which gives transmission values of more than 80 % over a spectral range of between 200 nm and 2500 nm for an empty cell. OS: OS indicates that SCHOTT type UK 5 is used for cells referred to in the catalogue as manufactured from Special Optical Glass. This crown glass is made from exceptionally pure raw materials, which gives an improved transmission in the near ultraviolet range. An empty cell will give a transmission of more than 80 % over a spectral range of between 320 nm and 2500 nm. Further dimensions and materials are available. page 68

70 agilent alternative replacement parts 33. Agilent alternative replacement parts PUMP Model 1260/1200/1100 art.-no. art.-no. original description model ASP Plunger Pump Model 1260/1200/ ASP Black Piston Seals Pump Model 1260/1200/ ASP Gold Piston Seals Pump Model 1260/1200/ ASP Wash Seal Pump Model 1260/1200/ ASP Seal Cap Assembly Pump Model 1260/1200/ ASP Glass Solvent Filter Pump Model 1260/1200/ ASP Active Inlet Valve Pump Model 1100/1200 G ASP G Outlet Ball Valve Pump Model 1100/1200 AUTOSAMPLER Model 1260/1200/1100 art.-no. art.-no. original description model G ASP G Needle Assembly Autosampler Model 1260/1200/1100 G ASP G Needle Seat, std Autosampler Model 1260/1200/1100 G ASP G Needle Assembly Autosampler Model 1100/1200 G ASP G Needle Seat, Std., Autosampler Model 1100/ ASP Rotor Seal, Vespel Autosampler Model 1100/ ASP Stator Face Assembly Autosampler Model 1100/ ASP Manual Injection Valve Autosampler Model 1100/ ASP Stator Face Assembly Autosampler Model 1100/1200 page 69

71 shimadzu/waters alternative replacement parts 34. Shimadzu alternative replacement parts PUMP art.-no. art.-no. original description ASP Plunger Holder ASP Plunger Seal ASP Plunger Seal ASP Plunger Seal ASP Inlet Check Valve ASP Outlet Check Valve ASP Inlet Check Valve, Primary ASP Syringe 500 µl 35. Waters alternative replacement parts INLET art.-no. art.-no. original description WAT033325ASP WAT Inlet Check Valve, #4, #5 Heads Model M45, 501, 510, 515, 1515, 1525, 590, 600 WAT025203ASP WAT Inlet Check Valve Housing M6KA, 510, 515, 600, 610, LC Module 1 WAT060307ASP WAT Inlet Check Valve Assembly - Extended Flow, 225 μl WAT033679ASP WAT Inlet Check Valve Assembly (Ball and Seat) 510, 515, 600, 610, 1525EF, LC Module 1, Prep LC-4000 M6KA, 510, 515, 600, 610, LC Module 1 page 70

72 waters alternative replacement parts OUTLET art.-no. art.-no. original description model WAT033326ASP WAT Outlet Check Valve Model M45, 501, 510, 515, 1515, 1525, 590, ASP Check Valve Cartridge, 2/pk 510, 515, 600, 610, 1515, 1525, 2690, 2690D, 2695, 2695D, 2795 WAT025028ASP WAT Outlet Check Valve Assembly - Actuator Style WAT025212ASP WAT Outlet Housing - Actuator Style WAT026016ASP WAT Outlet Check Valve Rebuild Kit - Actuator Style (rebuilds 2 valves) WAT025216ASP WAT Outlet Check Valve Assembly - Ball & Seat WAT025207ASP WAT Outlet Check Valve Housing - Ball & Seat M6KA, 510 M6KA, 510 M6KA, , 515, 600, 610, 1525EF, LC Module 1 510, 515, 600, 610, 1525EF, LC Module 1 PLUNGER art.-no. art.-no. original description model WAT022934ASP WAT Plunger Seal M6KA, 510, 515, 600, 610, 1515, 1525, LC Module 1 WAT026613ASP WAT Black GFP Plunger Seal 510, 515, 600, 610, 1515, 1525, LC Module 1 WAT026644ASP WAT Black Plunger Seal, EF Heads 510, 515, 590, 600, 610, LC Module 1 WAT060304ASP WAT Sapphire Plunger, Extended Flow 510, 515, 590, 600, 610, 1525EF, LC Module 1 WAT025656ASP; WAT069511ASP WAT025656, WAT Sapphire Plunger/Performance Plus Oriented Plunger WAS207069, ASP WAS Sapphire Plunger Assembly 515, 1515, 1525 M6KA, 510, 590, 600, 610, LC Module 1 page 71

73 waters replacement parts PUMP/AUTOSAMPLER ACQUITY H-CLASS art.-no. art.-no. original description model ASP Needle Seat ACQUITY H-Class SM-FTN, ACQUITY I-Class SM-FTN ASP Needle Guide ACQUITY H-Class SM-FTN, ACQUITY I-Class SM-FTN ASP Sample Needle Kit, 15µL ACQUITY H-Class SM-FTN WAT076152ASP WAT O-Ring, PTFE ACQUITY H-Class QSM, ACQUITY I-Class BSM, ACQUITY UPLC I2V BSM, ACQUITY UPLC BSM, Prep LC-2000, nanoacquity UPLC BSM/ASM ASP Plunger, 2/pk ACQUITY H-Class Bio QSM; ACQUITY H-Class QSM; ACQUITY I-Class BSM; ACQUITY UPLC I2V BSM; ACQUITY UPLC BSM; nanoacquity UPLC BSM/ ASM ASP Head Plunger Seal, 2/pk ACQUITY H-Class QSM, ACQUITY UPLC I2V BSM, ACQUITY UPLC BSM, nanoacquity UPLC BSM/ASM ASP Wash Seal, 2/pk ACQUITY H-Class QSM; ACQUITY UPLC I2V BSM; ACQUITY UPLC BSM; nanoacquity UPLC BSM/ASM ASP Acquity H-Class QSM Performance Maintenance Kit ACQUITY H-Class QSM ASP Filter, Air, Door ACQUITY H-Class Bio QSM, ACQUITY H-Class QSM ASP Check Valve, Double Ball & Seat ASP μl Sample Metering Syringe, HP ASP Cartridge, Intelligent Valve ASP Tube Assembly, Transducer to Check Valve ACQUITY H-Class QSM ACQUITY H-Class SM-FTN, ACQUITY I-Class SM-FTN, ACQUITY UPLC Sample Mgr, nanoacquity UPLC Sample Mgr ACQUITY H-Class QSM ACQUITY H-Class QSM ASP Filter, GPV, 4/pk ACQUITY H-Class QSM page 72

74 waters replacement parts PUMP/AUTOSAMPLER ACQUITY I-CLASS BSM art.-no. art.-no. original description model ASP SS Filter Frit Replacement Cartridge, 2/pk ACQUITY I-Class BSM ASP Solvent Bottle Filter, 7/pk ACQUITY I-Class BSM ASP UPLC Primary Check Valve Assy, 2/pk ACQUITY I-Class BSM ASP UPLC Check Valve, Double Ball & Seat, 2/pk ACQUITY I-Class BSM ASP SS Primary Inlet Check Valve Filter Kit, 2/pk ACQUITY I-Class BSM ASP Cartridge, Intelligent Valve, 2/pk ACQUITY I-Class BSM page 73

75 gc/hplc-syringes by hamilton 36. GC/HPLC-Syringes by Hamilton GAUGE INDEX When selecting a needle gauge it is important to keep in mind the volume of the syringe and the dead volume of the needle. For example, it will be very difficult to prime a 10 µl syringe if the dead volume in the needle is greater than 10 µl. Refer to the gauge index to choose a needle gauge with an appropriate µl/inch before selecting a needle. Select the minimum length that allows you to carry out your application comfortably. nominal o.d. nominal i.d. wall thickness volume gauge inch mm inch mm inch mm µl/inch s s s NEEDLE POINT STYLE: Several different needle point styles are offered on Hamilton syringe and needle products depending on the application. The correct point style varies depending on the intended application. Below are a few examples of common applications. Manual GC Injections: Historically a Point Style 2 was required to achieve efficient septum penetration with minimized coring. With Hamilton s new line of GC septa there is evidence that indicates the Point Style AS will consistently extend septa life by as much as 10-fold. Manual HPLC Injections: Most manual injection valves are designed to be used with a 22 gauge Point Style 3 needle. Drawing Sample: Any point style will efficiently draw a sample, but when it is important to get the last drop out of a vial use Point Style 3 or AS to reach all the way to the bottom. Animal Injections: Animal injections require the sharpest needle possible. The recommended needle point style for this application is a Point Style 4 at a 12 bevel. For applications where injection site depth is critical or the target is small, a more vertical bevel as shown below, such as a 30 or 45, is suggested. Point Style 2: Point Style 3: Sharp, beveled, curved, non-coring needle point, recommended for septum penetration Blunt needle point for use with HPLC injection valves and for sample pipetting Point Style 3T: Blunt needle point for thin layer chromatography (TLC) applications. Needles are coated with PTFE ¾ up from the needle tip. Point Style 4: Point Style 5: AS: Standard 12 beveled needle point is recommended for life science applications. Conical needle with side port for penetration of septa, thin-gauged vinyls and plastics without coring. Special conical style needle point used on autosampler syringes the non-coring needle point is recommended for septum penetration. page 74

76 gc/hplc-syringes by hamilton CTC LEAP COMBIPAL HD HEADSPACE SYRINGES: Hamilton s NEW headspace syringe with its unique, high-temperature plunger tip, is specifically designed for the CTC CobiPAL autosampler system. The High Dynamic (HD) plunger has been optimized for higher throughput in headspace techniques. The HD design by Hamilton sets a new standard for headspace syringe performance. art.-no. model volume gauge point style needle HT Model 1001 LTN CTC Syringe 1 ml 23 5 fixed HT Model 1002 LTN CTC Syringe 2,5 ml 23 5 fixed HT Model 1005 LTN CTC Syringe 5 ml 23 5 fixed HT Model 1001 LTN CTC Syringe 1 ml 26 5 fixed HT Model 1002 LTN CTC Syringe 2,5 ml 26 5 fixed HT Model 1005 LTN CTC Syringe 5 ml 26 5 fixed C-LINE SYRINGES: C-Line syringes incorporate several unique design features that ensure superior performance. An improperly installed syringe can cause mis-injections or bent needles due to poor alignment. The unique flange alignment design aids in installation and results in fewer bent needles while the plunger button can be adjusted to prevent plunger tip damage. An innovative direct attachment design of the needle to the barrel minimizes sample carryover. art.-no. model volume gauge point style needle HT C-Line Model 701 FN CTC Syringe (6.6 mm) 10 µl 26 2 fixed HT C-Line Model 1702 FN CTC Syringe (7.9 mm) 25 µl 26 AS fixed HT C-Line Model 1710 FN CTC Syringe (6.6 mm) 100 µl 26 AS fixed HT C-Line Model 1725 FN CTC Syringe (7.9 mm) 250 µl 26 AS fixed HT C-Line Model 701 FN CTC Syringe (6.6 mm) 10 µl 22 3 fixed HT C-Line Model 1702 FN CTC Syringe (7.9 mm) 25 µl 22 3 fixed HT C-Line Model 1710 FN CTC Syringe (6.6 mm) 100 µl 22 3 fixed HT C-Line Model 1725 FN CTC Syringe (7.9 mm) 250 µl 22 3 fixed HT C-Line Model 1001 LTN CTC Syringe (7.6 mm) 1 ml 22 3 fixed HT C-Line Model 1002 LTN CTC Syringe (9.65 mm) 2,5 ml 22 3 fixed HT C-Line Model 1005 LTN CTC Syringe (13.6 mm) 5 ml 22 3 fixed HT C-Line Model 1701 FN CTC Syringe (6.6 mm) 10 µl 22 3 fixed HT C-Line Model 1710 FN CTC Syringe (6.6 mm) 100 µl 22 3 fixed HT C-Line Model 1750 FN CTC Syringe (7.9 mm) 500 µl 22 3 fixed page 75

77 AGILENT 7693A SYRINGES: The 7693A builds on the proven Agilent Autosampler technologies that have worked reliably for customers in the past, including dual simultaneous injection and patented fast injection. The 7693A takes it one step further, adding basic sample preparation capabilities such as dilution, internal standard addition, heating and more. art.-no. model volume gauge point style needle HT87987 Model 75 N Agilent Syringe 5 µl 23 s AS fixed HT87993 Model 75 N Agilent Syringe 5 µl 23-26s AS fixed HT80387 Model 701 N Agilent Syringe 10 µl 23 s AS fixed HT80388 Model 701 N Agilent Syringe 10 µl 26 s AS fixed HT80079 Model 1701 N Agilent Syringe 10 µl 23-26s AS fixed HT80080 Model 1701 N Agilent Syringe 10 µl 23s AS fixed page 76

78 manual syringes 37. Manual Syringes GASTIGHT 1700 SERIES SYRINGES: The 1700 series syringes are the Gastight version of the original 700 series syringes. This series of syringes is ideal for dispensing volumes from 1 μl up to 500 μl. A variety of different terminations and needle options are available in this series. N: Cemented needle SN: Cemented Special Needle LTN: Luer Tip Cemented Needle RN: Removeable needle SL: Sample Lock MODEL 1701 art.-no. model volume gauge point style needle HT80000 Model 1701 N Syringe, 2 inch 10 µl 26s 2 fixed HT80030 Model 1701 RN Syringe, Small, 2 inch 10 µl 26s 2 changeable HT80039 Model 1701 N Syringe, 2 inch 10 µl 26s 5 fixed HT80050 Model 1701 N Syringe, 2 inch 10 µl 26s 3T fixed HT80065 Model 1701 RN Syringe, Small, 2 inch 10 µl 22s 3 changeable HT80075 Model 1701 N Syringe, 2 inch 10 µl 26s 3 fixed HT80087 Model 1701 RN Agilent Syringe, Small inch 10 µl 23s AS changeable HT80088 Model 1701 RN Agilent Syringe, Small, inch 10 µl 26s AS changeable HT80089 Model 1701 RN Agilent Syringe, Small, inch 10 µl 23s-26s AS changeable MODEL 1702 art.-no. model volume gauge point style needle HT80200 Model 1702 N Syringe, 2 inch 25 µl 22s 2 fixed HT80230 Model 1702 RN Syringe, 2 inch 25 µl 22s 2 changeable HT80239 Model 1702 N Syringe, 2 inch 25 µl 22s 5 fixed HT80250 Model 1702 N Syringe, 2 inch 25 µl 22s 3T fixed HT80265 Model 1702 RN Syringe, 2 inch 25 µl 22s 3 changeable HT80200 Model 1702 N Syringe, 2 inch 25 µl 22s 2 fixed MODEL 1705 art.-no. model volume gauge point style needle HT µl, Model 1705 N Syringe, 2 inch 50 µl 22 2 fixed HT µl, Model 1705 RN Syringe, Small, 2 inch 50 µl 22 2 changeable HT µl, Model 1705 N Syringe, 2 inch 50 µl 22 3t fixed HT µl, Model 1705 SL Syringe, Large, 2 inch 50 µl 22 2 changeable HT µl, Model 1705 RN Syringe, Small, 2 inch 50 µl 22 3 changeable page 77

79 manual syringes MODEL 1710 art.-no. model volume gauge point style needle HT µl, Model 1710 N Syringe, 2 inch 100 µl 22s 2 fixed HT µl, Model 1710 RN Syringe, Small, 2 inch 100 µl 22s 2 changeable HT µl, Model 1710 N Syringe, 2 inch 100 µl 22s 3t fixed HT µl, Model 1710 SL Syringe, Large, 2 inch 100 µl 22s 2 changeable HT µl, Model 1710 RN Syringe, Small, 2 inch 100 µl 22s 3 changeable HT µl, Model 1710 N Syringe, 2 inch 100 µl 22s 2 fixed MODEL 1725 art.-no. model volume gauge point style needle HT µl, Model 1725 LTN Syringe, 2 inch 250 µl 22s 2 fixed HT µl, Model 1725 RN Syringe, 2 inch 250 µl 22s 2 changeable HT µl, Model 1725 N Syringe, 2 inch 250 µl 22s 5 fixed HT µl, Model 1725 SL Syringe, 2 inch 250 µl 22s 2 changeable HT µl, Model 1725 RN Syringe, 2 inch 250 µl 22 3 changeable MODEL 1750 art.-no. model volume gauge point style needle HT µl, Model 1750 LTN Syringe, 2 inch 500 µl 22 2 fixed HT µl, Model 1750 RN Syringe, 2 inch 500 µl 22 2 changeable HT µl, Model 1750 LTN Syringe, 2 inch5 500 µl 22 5 fixed HT µl, Model 1750 SL Syringe, 2 inch 500 µl 22 2 changeable HT µl, Model 1750 RN Syringe, 2 inch 500 µl 22 3 changeable MICROLITER 700 SERIES SYRINGES: The 700 series syringe is the original hand-fitted Hamilton syringe. This series of syringes is ideal for dispensing volumes from 0.5 μl up to 500 μl. A variety of different terminations and needle options are available in this series. MODEL 701 art.-no. model volume gauge point style needle HT µl, Model 701 RN Syringe, 6 Pack, Small, 2 inch 10 µl 26s 2 changeable HT µl, Model 701 N Syringe, 2 inch 10 µl 26s 5 fixed HT µl, Model 701 RN Agilent Syringe, 1.71 inch 10 µl 23s AS changeable HT µl, Model 701 RN Agilent Syringe, 1.71 inch 10 µl 26s AS changeable HT µl, Model 701 RN Agilent Syringe, 23s-26s ga, 1.71 inch 10 µl 23s-26s AS changeable page 78

80 manual syringes art.-no. model volume gauge point style needle HT µl, Model 701 N Syringe, 2 inch 10 µl 22s 3 fixed HT µl, Model 701 N Syringe, 2 inch 10 µl 26s 3 fixed HT µl, Model 701 N Syringe, 3 inch 10 µl 26s 2 fixed HT µl, Model 701 N Agilent Syringe, 1.71 inch 10 µl 23s 2 fixed HT µl, Model 701 N Agilent Syringe, 1.71 inch 10 µl 26s 2 fixed MODEL 702 art.-no. model volume gauge point style needle HT µl, Model 702 N Syringe,fixed Needle, 22s ga, 2 in 25 µl 22s 2 fixed HT µl, Model 702 RN Syringe, Small el, 22s ga, 2 in 25 µl 22s 2 changeable HT µl, Model 702 N Syringe, fixed Needle, 22s ga, 2 in 25 µl 22s 3 fixed MODEL 705 art.-no. model volume gauge point style needle HT µl, Model 705 N Syringe, fixed Needle, 22s ga, 2 in 50 µl 22s 2 fixed HT µl, Model 705 RN Syringe, Small Au Needle, 22s ga, 2 in 50 µl 22s 2 changeable HT µl, Model 705 N Syringe, fixed Needle, 22s ga, 2 in 50 µl 22s 3 fixed MODEL 710 art.-no. model volume gauge point style needle HT µl, Model 710 N Syringe, fixed Needle, 22s ga, 2 in 100 µl 22s 2 fixed HT µl, Model 710 RN Syringe, Small, 22s ga, 2 in 100 µl 22s 3 changeable HT µl, Model 710 N Syringe, fixed Needle, 22s ga, 2 in 100 µl 22s 4 fixed MODEL 725 art.-no. model volume gauge point style needle HT µl, Model 725 N Syringe, fixed Needle, 22s ga, 2 in 250 µl 22s 2 fixed HT µl, Model 725 RN Syringe, Large, 22s ga, 2 in 250 µl 22s 2 changeable HT µl, Model 725 N Syringe, fixed Needle, 22 ga, 2 in 250 µl 22 3 fixed MODEL 750 art.-no. model volume gauge point style needle HT µl, Model 750 N Syringe, 2 inch 500 µl 22 2 fixed HT µl, Model 750 RN Syringe, Large Needle 2 inch 500 µl 22 2 changeable HT µl, Model 750 N Syringe, fixed Needle, 2 inch 500 µl 22 5 fixed HT µl, Model 750 N Syringe, fixed Needle, 2 inch 500 µl 22 3 fixed page 79

81 manual syringes GASTIGHT 1000 SERIES SYRINGES: The 1000 series syringes are a mid volume gastight syringe. This series of syringes is ideal for dispensing volumes from 100 μl up to 100 ml. A variety of different terminations and needle options are available in this series. MODEL 1001 art.-no. model volume gauge point style needle HT81317 Model 1001 LTN Syringe, 2 inch 1 ml 22 2 Fixed HT81330 Model 1001 RN Syringe, Large, 2 inch 1 ml 22 2 changeable HT81343 Model 1001 LTN Syringe, 2 inch 1 ml 22 5 fixed HT81356 Model 1001 SL Syringe, Large, 2 inch 1 ml 22 2 changeable HT81365 Model 1001 RN Syringe, Large, 2 inch 1 ml 22 3 changeable MODEL 1002 art.-no. model volume gauge point style needle HT81417 Model 1002 LTN Syringe, 2 inch 2,5 ml 22 2 fixed HT81430 Model 1002 RN Syringe, 2 inch 2,5 ml 22 2 changeable HT81443 Model 1002 LTN Syringe, 2 inch 2,5 ml 22 5 fixed HT81456 Model 1002 SL Syringe, Large, 2 inch 2,5 ml 22 2 changeable MODEL 1005 art.-no. model volume gauge point style needle HT81517 Model 1005 LTN Syringe, 2 inch 5 ml 22 2 fixed HT81530 Model 1005 RN Syringe, Large, 2 inch 5 ml 22 2 changeable HT81543 Model 1005 LTN Syringe, 2 inch 5 ml 22 5 fixed HT81556 Model 1005 SL Syringe, 2 inch 5 ml 22 2 changeable MODEL 1010 art.-no. model volume gauge point style needle HT81617 Model 1010 LTN Syringe, 2 inch 10 ml 22 2 fixed HT81630 Model 1010 RN Syringe, Large, 2 inch 10 ml 22 2 changeable HT81643 Model 1010 LTN Syringe, 2 inch 10 ml 22 5 fixed HT81656 Model 1010 SL Syringe, Large, 2 inch 10 ml 22 2 changeable Please note: a lot of other models/dimensions of syringes are available! page 80

82 gc syringes by sge 38. GC syringes by SGE MANUAL OR AUTOSAMPLER SYRINGES: If the syringe is used manually, then a manual syringe is sufficient if it is to be installed in an instrument. Make sure that the selected syringe matches the instrument. Syringe size: For good reproducibility and accuracy, no more than 10 % of total injection capacity should be injected. PERMANENT OR REPLACABLE NEEDLES: Fixed needles are the first choice for experienced users or analyzes in the trace area. Fixed needles are suitable for autosamplers where there is little risk that the needle will bend. Solid needles are very easy to handle. Interchangeable needles can save costs over time because, with bent needles, the needles can be replaced separately. The needles can also be exchanged for different applications. DIFFERENT TYPES OF NEEDLES: Beveled: Is the first choice when manually inserted into a septum. Beveled tips are also known as Point Style 2. Cone: This type of tip is specifically designed for multiple injections or when the lifetime of the septum in the autosampler is to be extended. The conical shape effectively perforates the septum during the piercing process without cutting it in. Conical needles are also known as Point Syle AS. HPLC: These straight needles are used in HPLC and are also known as Point Style 3. Side Hole: The samples are injected through the side hole to prevent clogging of the needle. This shape is ideal for large-volume gas injections and is also known as Point Style 5 needles. Sheathed bevelled needle: This needle corresponds to the chamfered needle, except that the needle is still strengthened by a sheath. These needles are also known as Point Style 4 needles. KINDS OF PLUNGERS: Metal Plunger: These plungers can not be exchanged, stainless steel plungers with special fitting into the injection body. Standard for chromatographic applications. Used for injection volume between 5 and 500 μl. Plunger with PTFE Tip: Can be used for gaseous and liquid injections. The plunger is interchangeable, easy to remove. Used for injection volumes between 10 μl and 100 ml. Conical needles are also known as Point Syle AS. Flexibler Plunger: Very robust plunger, ideal for student use. Used for injection volumes between 5 and 10 μl. page 81

83 gc syringes by sge MANUAL SYRINGES: art.-no. description type volume alternative hamilton SG μl Removable Needle Syringe with 5 cm 0.47 mm OD Bevel Tipped Needle Removable Needle Syringe 5 µl HT87930 SG μl Fixed Needle Syringe with 5 cm 0.47 mm OD Bevel Tipped Needle Cemented Needle Syringe 5 µl HT87900 art.-no. description type volume alternative hamilton SG μl Fixed Needle Syringe with 5 cm 0.47 mm OD Bevel Tipped Needle Cemented Needle Syringe 10 µl HT80300 SG μl Fixed Needle Syringe with 5 cm 0.47 mm OD Bevel Tipped Needle PK6 Cemented Needle Syringe 10 µl HT80366 SG μl Removable Needle Syringe with 5 cm 0.47 mm OD Bevel Tipped Needle Removable Needle Syringe 10 µl HT80330 art.-no. description type volume alternative hamilton SG μl Fixed Needle Syringe with 5 cm 0.5 mm OD Bevel Tipped Needle Cemented Needle Syringe 25 µl HT80400 SG μl Fixed Needle Syringe with GT Plunger & 5 cm 0.5 mm OD Bevel Tipped Needle Cemented Needle Syringe 25 µl HT80200 SG μl Removable Needle Syringe with GT Plunger & 5 cm 0.5 mm OD Bevel Tipped Needle Removable Needle Syringe 25 µl HT80230 page 82

84 gc syringes by sge art.-no. description type volume alternative hamilton SG μl Fixed Needle Syringe with 5 cm 0.5 mm OD, Bevel Tipped Needle Cemented Needle Syringe 50 µl HT80500 SG μl Fixed Needle Syringe with GT Plunger & 5 cm 0.5 mm, OD Bevel Tipped Needle Cemented Needle Syringe 50 µl HT80900 SG μl Removable Needle Syringe with GT Plunger & 5 cm 0.5 mm OD Bevel Tipped Needle Removable Needle Syringe 50 µl HT80930 art.-no. description type volume alternative hamilton SG μl Fixed Needle Syringe with 5 cm 0.5 mm OD, Bevel Tipped Needle Cemented Needle Syringe 100 µl HT80600 SG μl Fixed Needle Syringe with GT Plunger & 5 cm 0.5 mm OD Bevel Tipped Needle Cemented Needle Syringe 100 µl HT81000 SG μl Removable Needle Syringe with GT Plunger & 5 cm 0.5 mm OD Bevel Tipped Needle Removable Needle Syringe 100 µl HT81030 art.-no. description type volume alternative hamilton SG μl Fixed Needle Syringe with 5 cm 0.5 mm OD, Bevel Tipped Needle Cemented Needle Syringe 250 µl HT80700 SG μl Removable Needle Syringe with 5 cm 0.5 mm OD, Bevel Tipped Needle Removable Needle Syringe 250 µl HT80730 page 83

85 syringes for agilent-devices SYRINGES FOR AGILENT-DEVICES: art.-no. description type volume alternative hamilton SG μl NanoVolume Agilent Syringe with 4.2 cm 0.63 mm OD Cone Tipped Needle Needle: Replaceable, 23 gauge, Length 42 mm, Tip style: AS, conical 1 µl HT80176 SG μl Fixed Needle Agilent Syringe with GT Plunger & 4.2 cm 0.63 mm OD Cone Tipped Needle Needle: Fixed, 23 gauge, Length 42 mm, Style of tip: AS, conical 10 µl HT80176 SG μl Fixed Needle Agilent Syringe with 4.2 cm 0.63/0.47 mm OD Cone Tipped Dual Gauge Needle Fixed Tapered Needle Syringe 5 µl HT87959 SG μl Fixed Needle Agilent Syringe with 4.2 cm 0.63/0.47 mm OD Cone Tipped Dual Gauge Needle Fixed Tapered Needle Syringe 10 µl HT80393 SG μl Fixed Needle Agilent Syringe with 4.2 cm 0.63 mm OD Cone Tipped Needle Fixed Straight Needle 10 µl HT80393 SG μl Fixed Needle Agilent Syringe with 4.2 cm 0.63 mm OD Cone Tipped Needle PK6 Needle: Fixed, 23 gauge, Length 42 mm, Style of tip: AS, conical 10 µl HT80390 SG μl Removable Needle Varian (8035, 8100, 8200) Syringe with GT Plunger & 5.3 cm 0.5 mm OD Needle Removable Needle Syringe 10 µl HT page 84

86 syringes for ctc/thermo scientific-devices SYRINGES FOR CTC/THERMO SCIENTIFIC-DEVICES: art.-no. description type volume alternative hamilton SG Thermo Scientific Autosampler Syringes 10 µl HT SG μl Fixed Needle CTC/Thermo Syringe with 5 cm 0.47 mm OD Cone Tipped Needle Fixed Needle Syringe 5 µl HT SG μl Fixed Needle CTC/Thermo (Classic Button) Syringe with 5 cm 0.47 mm OD Cone Tipped Needle 5 µl HT SG μl Removable Needle CTC/Thermo Syringe with GT Plunger & 5 cm 0.47 mm OD Cone Tipped Needle Needle: Replaceable, 26 gauge, Length 50 mm, Style of tip: AS, conical 10 µl SG μl Fixed Needle CTC/Thermo Syringe with 5 cm 0.63 mm OD Cone Tipped Needle Needle: Fixed, 23 gauge, Length 50 mm, Style of tip: AS, conical 10 µl HT SG μl Fixed Needle CTC/Thermo (Classic Button) Syringe with 5 cm 0.47 mm OD Cone Tipped Needle 10 µl HT SG μl Fixed Needle CTC/Thermo Syringe with 5 cm 0.47 mm OD Cone Tipped Needle Needle: Fixed, 26 gauge, Length 50 mm, Style of tip: AS, conical 10 µl HT SG μl Fixed Needle CTC Syringe with 5 cm 0.47 mm OD Cone Tipped Needle Fixed Needle Syringe 10 µl HT SG μl Fixed Needle CTC Syringe with GT Plunger & 5 cm 0.47 mm OD Cone Tipped Needle Fixed Needle Syringe 25 µl HT SG μl Fixed Needle CTC/Thermo Syringe with GT Plunger & 5 cm 0.63 mm OD Cone Tipped Needle Needle: Fixed, 23 gauge, Length 50 mm, Style of tip: AS, conical 25 µl SG μl Fixed Needle CTC Syringe with GT Plunger & 5 cm 0.47 mm OD Cone Tipped Needle Fixed Needle Syringe 100 µl HT SG μl Fixed Needle CTC Syringe with GT Plunger & 5 cm 0.47 mm OD Cone Tipped Needle Fixed Needle Syringe 250 µl HT page 85

87 syringes for perkinelmer-devices/shimadzu-devices SYRINGES FOR PERKIN ELMER-DEVICES: art.-no. description type volume alternative hamilton SG μl NanoVolume PerkinElmer Syringe with 7 cm 0.47 mm OD Cone Tipped Needle Needle: Replaceable, 26 gauge, Length 70 mm, Style of tip: AS, conical 0,5 µl SG μl NanoVolume PerkinElmer Syringe with 7 cm 0.63 mm OD Cone Tipped Needle Needle: Replaceable, 23 gauge, Length 70 mm, Style of tip: AS, conical 0,5 µl SG SG μl Fixed Needle PerkinElmer Syringe with GT Plunger & 7 cm 0.63 mm OD Cone Tipped Needle 5 μl Fixed Needle PerkinElmer Syringe with 7 cm 0.47 mm OD Cone Tipped Needle Needle: Replaceable, 23 gauge, Length 70 mm, Style of tip: AS, conical 5 µl Fixed Needle Syringe 5 µl HT88040 SYRINGES FOR SHIMADZU-DEVICES: art.-no. description type volume alternative hamilton SG Metal Syringes AOC20i Needle: Fixed, 23 gauge, Length 42 mm, Style of tip: AS, conical 5 µl SG μl Removable Needle Shimadzu Syringe with 4.2 cm 0.63 mm OD Cone Tipped Needle Removable Needle 10 µl HT88040 page 86

88 ferrule by sge 39. Ferrules by SGE The ferrule is a small, sealing connector within the GC system. Often underestimated, however, the ferrule is of central importance. On the other hand, the ferrule ensures that the GC column is held securely and correctly positioned in the GC apparatus. Ferrules are available in different sizes, materials and shapes and can thus be optimally adapted to the respective GC-Column. Which material suits best for the application? What type of connection is desired? material graphite graphite/vespel siltite metal Advantages Simple Handling High tightness Soft Material Reusable Robust Hard Material, Long Lifetime Specially designed to avoid the disadvantages of graphite ferrules Strong connection/high tightness Tightness immediately after installation, no tightening required Disadvantages Must be retightened after the first temperature cycle, otherwise air can enter the detector Can leave residues in the column Not reusable with another capillary column Too strong tightening can lead to leaks Application possibilities Connection from column to injector FID/ECD/TCD/NPD Detectors MS Interface Ideal for MS Interface Temperature limit 450 C 325 C No temperature limit page 87

89 ferrules by sge GRAPHITE/VESPEL: compatible with material description column id (mm) Ferrule id (mm) art.-no. quantity Agilent Agilent Agilent Agilent Agilent Agilent 15% Graphite/ 85% Vespel 15% Graphite/ 85% Vespel 15% Graphite/ 85% Vespel 15% Graphite/ 85% Vespel 15% Graphite/ 85% Vespel 15% Graphite/ 85% Vespel For Injectors&Detectors at atmospheric pressure SG For Injectors&Detectors at atmospheric pressure SG For Injectors&Detectors at atmospheric pressure SG For GC-MS Interface Connection SG For GC-MS Interface Connectionnection SG For GC-MS Interface Connection SG compatible with material description column id (mm) Ferrule id (mm) art.-no. quantity Shimadzu Shimadzu Shimadzu Shimadzu 15 % Graphite/ 85 % Vespel 15 % Graphite/ 85 % Vespel 15 % Graphite/ 85 % Vespel 15 % Graphite/ 85 % Vespel QP5000/50050 Standard MS Interface SG QP5000/50050 Standard MS Interface 0.32 SG QP5000-II & QP5050 MS Interface 0.53 SG QP5000-II & QP5050 MS Interface SG Shimadzu 15 % Graphite/ 85 % Vespel QP5000/50050 Wide Bore MS Interface, QP2010Injector and QP2010 Standard MS Interface SG Shimadzu 15 % Graphite/ 85 % Vespel QP5000/50050 Wide Bore MS Interface, QP2010Injector and QP2010 Standard MS Interface 0.32 SG Shimadzu 15 % Graphite/ 85 % Vespel QP5000/50050 Wide Bore MS Interface, QP2010Injector and QP2010 Standard MS Interface 0.53 SG page 88

90 ferrules by sge compatible with material description column id (mm) Ferrule id (mm) art.-no. quantity Perkin Elmer 15 % Graphite/ 85 % Vespel For Injectors& Detectors at atmospheric pressure SG Perkin Elmer 15 % Graphite/ 85 % Vespel For Injectors& Detectors at atmospheric pressure SG Perkin Elmer 15 % Graphite/ 85 % Vespel For Injectors& Detectors at atmospheric pressure SG compatible with material description column id (mm) Ferrule id (mm) art.-no. quantity Thermo Scientific 15 % Graphite/ 85 % Vespel for all Injectors & Detectors (not for 8000 Series, Focus, Trace/Ultra GC) SG Thermo Scientific 15 % Graphite/ 85 % Vespel for all Injectors & Detectors (not for 8000 Series, Focus, Trace/Ultra GC) SG Thermo Scientific 15 % Graphite/ 85 % Vespel for all Injectors & Detectors (not for 8000 Series, Focus, Trace/Ultra GC) SG Thermo Scientific 15 % Graphite/ 85 % Vespel For all Focus, Trace/Ultra injectors and detectors at atmospheric pressure (not for GCMS) SG Thermo Scientific 15 % Graphite/ 85 % Vespel For all Focus, Trace/Ultra injectors and detectors at atmospheric pressure (not for GCMS) SG Thermo Scientific 15 % Graphite/ 85 % Vespel For all Focus, Trace/Ultra injectors and detectors at atmospheric pressure (not for GCMS) SG page 89

91 ferrules by sge compatible with material description column id (mm) Ferrule id (mm) art.-no. quantity Varian/ Bruker 15 % Graphite/ 85 % Vespel For GCMS & Detectors at atmospheric pressure - column IDs mm SG Varian/ Bruker 15 % Graphite/ 85 % Vespel For GCMS & Detectors at atmospheric pressure - column IDs 0.32 mm SG Varian/ Bruker 15 % Graphite/ 85 % Vespel For GCMS & Detectors at atmospheric pressure - column IDs 0.53 mm SG % GRAPHITE: compatible with description column id (mm) Ferrule id (mm) art.-nr. Quantity Perkin Elmer 100 % Graphite Ferrules SG Perkin Elmer 100 % Graphite Ferrules SG Shimadzu 100 % Graphite Ferrules SG Shimadzu 100 % Graphite Ferrules SG Thermo Scientific 100 % Graphite Ferrules SG Thermo Scientific 100 % Graphite Ferrules SG Varian / Bruker 100 % Graphite Ferrules SG Varian / Bruker 100 % Graphite Ferrules , SG page 90

92 ferrules by sge SILTITE METAL: compatible with description column id (mm) ferrule id (mm) art.-no. quantity Agilent Injector/FID Starter Kit SG Agilent Injector/FID Starter Kit SG compatible with description column id (mm) ferrule id (mm) art.-no. quantity Perkin Elmer Injector/FID Starter Kit 0.4 SG Perkin Elmer Injector/MS Starter Kit 0.4 SG compatible with description column id (mm) ferrule id (mm) art.-no. quantity Shimadzu Shimadzu Shimadzu GC14A, GC17A, GC2010/2014 (Not for MS or QP2010 Injector) Starter kit GC14A, GC17A, GC2010/2014 (Not for MS or QP2010 Injector) Starter kit GC14A, GC17A, GC2014 (Not for MS or QP2010 Injector) Starter kit SG SG SG Shimadzu 2010 Injector/FID Starter Kit SG Shimadzu 2010 Injector/MS Starter Kit SG Shimadzu Shimadzu Shimadzu Shimadzu Shimadzu QP5000/50050 Standard MS Interface Starter Kit QP5000/50050 Standard MS Interface Starter Kit QP5000/50050 Wide Bore MS Interface, QP2010Injector and QP2010 Standard MS Interface Starter Kit QP5000/50050 Wide Bore MS Interface, QP2010Injector and QP2010 Standard MS Interface Starter Kit QP5000/50050 Wide Bore MS Interface, QP2010Injector and QP2010 Standard MS Interface Starter Kit SG SG SG SG SG page 91

93 ferrules by sge compatible with description column id (mm) ferrule id (mm) art.-no. quantity Thermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific For GC-MC Interface Connections (Starter Kit) For GC-MC Interface Connections (Starter Kit) For GC-MC Interface Connections (Starter Kit) Injector/MS (non-isq) Starter Kit SG SG SG SG Thermo Scientific Injector/MS ISQ Starter Kit SG Thermo Scientific Injector/FID Starter Kit SG compatible with description column id (mm) ferrule id (mm) art.-no. quantity Varian/Bruker For GCMS connections Starter Kit - column IDs mm SG Varian/Bruker For GCMS connections Starter Kit - column IDs 0.32 mm Varian/Bruker For GCMS connections Starter Kit - column IDs 0.53 mm SG SG Varian/Bruker Injector/GCMS Starter Kit (not for 220, 1200, 2000, or 4000 MS systems) SG Varian/Bruker Injector/FID Starter Kit SG Varian/Bruker Injector/FID Starter Kit SG Varian/Bruker Injector/MS Starter Kit SG Varian/Bruker Injector/FID Starter Kit 0.4 SG page 92

94 gc columns by sge 40. GC columns by SGE BP1 (DIMETHYLPOLYSILOXANE): USP G1/G2/G38 Classic crosslinked dimethyl polysiloxane technology Excellent general purpose column Low bleed Non-polar Suitable for routine analyses 320 C-340 C upper temperature limit- depentent on film thickness Suitable replacement for: DB-1, HP-1, RTX-1, Ultra-1, CP-Sil 5 CB, VB -1, ZB-1, VF-1ms art.-no. description length (mm) id film thickness quantity SG BP1 Dimethylpolysiloxane 30 0,25 0,25 1 SG BP1 Dimethylpolysiloxane 30 0,32 0,25 1 SG BP1 Dimethylpolysiloxane 30 0, SG BP1 Dimethylpolysiloxane 60 0,25 0,25 1 SG BP1 Dimethylpolysiloxane 60 0,32 0,25 1 SG BP1 Dimethylpolysiloxane 60 0, SG BP1 Dimethylpolysiloxane 60 0, page 93 Other column materials and dimensions are available!

95 BP5 (5 %PHENYL/95 % DIMETHYLPOLYSILOXANE): USP G27/G36 Excellent general purpose column Low bleed Non-polar High temperature 320 C-340 upper temperature limit- depentent on film thickness Suitable Replacement for DB-5, Rtx-5, HP-5, Ultra-2, PTE-5, MDN-5, CP-Sil8CB, VB-5, ZB-5 art.-no. description length (mm) id film thickness quantity SG BP5 (5 %Phenyl/95 %Dimethylpolysiloxane) 30 0,25 0,25 1 SG BP5 (5 %Phenyl/95 %Dimethylpolysiloxane) 30 0,32 0,25 1 SG BP5 (5 %Phenyl/95 %Dimethylpolysiloxane) 30 0, SG BP5 (5 %Phenyl/95 %Dimethylpolysiloxane) 60 0,25 0,25 1 SG BP5 (5 %Phenyl/95 %Dimethylpolysiloxane) 60 0,32 0,25 1 SG BP5 (5 %Phenyl/95 %Dimethylpolysiloxane) 60 0, SG BP5 (5 %Phenyl/95 %Dimethylpolysiloxane) 60 0,53 1,5 1 BPX5 (5 % PHENYL/POLYSILPHENYLENE-SILOXANE): USP G27/G36 High temperature General purpose GC column Very low bleed, ideal for trace analysis Non-polar Extremely inert Ideal for GC-MS 360 C-370 C upper temperature limit- dependent on film thickness Suitable replacement for: DB-5, DB-5ms, Rtx-5ms, HP-5, Hp-5MS, CP-Sil8CB, Rxt-Sil 5 MS, VB-5, ZB-5, VF-5ms art.-no. description length (mm) id film thickness quantity SG BPX5 (5 %Phenyl/Polysilphenylene-siloxane) 30 0,25 0,25 1 SG BPX5 (5 %Phenyl/Polysilphenylene-siloxane) 30 0,32 0,25 1 SG BPX5 (5 %Phenyl/Polysilphenylene-siloxane) 30 0, SG BPX5 (5 %Phenyl/Polysilphenylene-siloxane) 60 0,25 0,25 1 SG BPX5 (5 %Phenyl/Polysilphenylene-siloxane) 60 0,32 0,25 1 SG BPX5 (5 %Phenyl/Polysilphenylene-siloxane) 60 0, SG BPX5 (5 %Phenyl/Polysilphenylene-siloxane) 60 0, Other column materials and dimensions are available! page 94

96 gc columns by sge BP20 (WAX) POLETHYLENE GLYCOL: USP G16 Industry standard wax column Polar phase 240 C-280 C upper temperature limit- dependent on film thickness Bonded and cross-linked Able to be solvent rinsed Suitable replacement for: DB-Wax, HP-20M, Supelcowax 10, CB-Wax, Stabilwax, Carbowax, HP-Innowax, RTX.WAX, RH-WAX, ZB-WAX, TRWAX art.-no. description length (mm) id film thickness quantity SG BP20 (WAX) Polethylene Glycol 30 0,25 0,25 1 SG BP20 (WAX) Polethylene Glycol 30 0,32 0,25 1 SG BP20 (WAX) Polethylene Glycol 30 0, SG BP20 (WAX) Polethylene Glycol 60 0,25 0,25 1 SG BP20 (WAX) Polethylene Glycol 60 0,32 0,25 1 SG BP20 (WAX) Polethylene Glycol 60 0, SG BP20 (WAX) Polethylene Glycol 60 0, page 95 Other column materials and dimensions are available!

97 gc columns by macherey-nagel 41. GC columns by Macherey-Nagel GUARD COLUMN: art.-no. MN MN MN description Pre-column: deactivated capillary column without cage Methyl-Sil deactivated ID: 0,25 mm, Length: 10 m Pre-column: deactivated capillary column without cage Methyl-Sil deactivated ID: 0,32 mm, Length: 10 m Pre-column: deactivated capillary column without cage Methyl-Sil deactivated ID: 0,53 mm, Length: 10 m OPTIMA-1 (100% DIMETHYLPOLYSILOXANE): USP G1/G2/G38 Nonpolar Phase Low bleed column Excellent general purpose column 300 C-340 C upper temperature limit- dependent on film thickness Suitable replacement for: DB-1, HP-1, RTX-1, Ultra-1, CP-Sil 5 CB, VB -1, ZB-1, VF-1ms, AT-1, OV-1 art.-no. description length (mm) id film thickness quantity MN Optima-1 (100 % Dimethylpolysiloxane) 30 0,25 0,25 1 MN Optima-1 (100 % Dimethylpolysiloxane) 30 0,32 0,25 1 MN Optima-1 (100 % Dimethylpolysiloxane) 30 0, MN Optima-1 (100 % Dimethylpolysiloxane) 60 0,25 0,25 1 MN Optima-1 (100 % Dimethylpolysiloxane) 60 0,32 0,25 1 MN Optima-1 (100 % Dimethylpolysiloxane) 60 0, Other column materials and dimensions are available! page 96

98 gc columns by macherey-nagel OPTIMA-1MS (100 % DIMETHYLPOLYSILOXANE): USP G1/G2/G38 Nonpolar Phase Extreme low bleeding Suited for GC-MS and trace level analysis Max.temperature for isothermal operation 340 C, max. temperature for short isotherms in a temperature program 360 C Suitable replacement for: Ultra-1, DB-1MS, HP-1MS, Rtx-1MS, Rxi-1MS, Equity 1, AT-1MS, VF-1MS, CP-Sil 5 CB MS art.-no. description length (mm) id film thickness quantity MN Optima-1MS (100 % Dimethylpolysiloxane) 30 0,25 0,25 1 MN Optima-1MS (100 % Dimethylpolysiloxane) 30 0,32 0,25 1 MN Optima-1MS (100 % Dimethylpolysiloxane) 60 0,25 0,25 1 MN Optima-1MS (100 % Dimethylpolysiloxane) 60 0,32 0,25 1 OPTIMA-5 (5 % PHENYL-95 % METHYLPOLYSILOXANE): USP G27/G36 Low bleed Nonpolar phase Large range of applications Columns with mm ID and films < 3 μm: max. temperature for isothermal operation 340 C, max. temperature for short isotherms in a temperature program 360 C; 0.53 mm ID columns with films < 3 μm: max. temperatures 320 C and 340 C, resp. Suitable replacement for: SE-54, SE-52, HP-5, SPB-5, CP Sil 8, Rtx 5, 007-5, BP5, MDN 5, AT 5, ZB 5 art.-no. description length (mm) id film thickness quantity MN Optima-5 (5 % Phenyl-95 % Methylpolysiloxane) 30 0,25 0,25 1 MN Optima-5 (5 % Phenyl-95 % Methylpolysiloxane) 30 0,32 0,25 1 MN Optima-5 (5 % Phenyl-95 % Methylpolysiloxane) 30 0, MN Optima-5 (5 % Phenyl-95 % Methylpolysiloxane) 60 0,25 0,25 1 MN Optima-5 (5 % Phenyl-95 % Methylpolysiloxane) 60 0,32 0,25 1 MN Optima-5 (5 % Phenyl-95 % Methylpolysiloxane) 60 0, MN Optima-5 (5 % Phenyl-95 % Methylpolysiloxane) 60 0, page 97 Other column materials and dimensions are available!

99 OPTIMA WAX (POLYETHYLENEGLYCOL): USP G16 Polar Phase Recommended for solvent analysis and alcohols, suitable for aqueous solutions Columns with mm ID: max. temperature for isothermal operation 240 C, max. temperature for short isotherms in a temperature program 250 C; 0.53 mm ID columns: max. temperatures 220 C and 240 C, resp. Suitable replacement for : DB-Wax, Supelcowax, HP Wax, HP-INNOWAX, Rtx Wax, CP-Wax 52 CB, Stabilwax, 007-CW, BP20, AT-Wax, ZB-Wax art.-no. description length (mm) id film thikness quantity MN Optima WAX (Polyethyleneglycol) 30 0,25 0,25 1 MN Optima WAX (Polyethyleneglycol) 30 0,32 0,25 1 MN Optima WAX (Polyethyleneglycol) 30 0, MN Optima WAX (Polyethyleneglycol) 60 0,25 0,25 1 MN Optima WAX (Polyethyleneglycol) 60 0,32 0,25 1 MN Optima WAX (Polyethyleneglycol) 60 0,32 0,5 1 Other column materials and dimensions are available! page 98

100 chromatogaphy offers Supply for Chromatography & Spectroscopy laboratories All brands from one source YOUR LOCAL DISTRIBUTOR Valid until All offers may be subject to printing errors and price changes.