Agriculture & Priority Pollutants Laboratories, Inc. (APPL, Inc.)

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Charles Beasley
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1 NELAP-Recognized Laboratory Accreditation is hereby awarded to in accordance with Texas Water Code Chapter 5, Subchapter R, Title 30 Texas Administrative Code Chapter 25, and the National Environmental Laboratory Accreditation Program. The laboratory's scope of accreditation includes the fields of accreditation that accompany this certificate. Continued accreditation depends upon successful ongoing participation in the program. The Texas Commission on urges customers to verify the laboratory's current location(s) and accreditation status for particular methods and analyses ( Accreditation does not imply that a product, process, system or person is approved by the Texas Commission on. Certificate Number: T Effective Date: 12/1/2017 Executive Director Texas Commission on

2 T /2018 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water Method EPA 6010 Analyte AB Analyte 10 Method 10 Antimony UT Arsenic UT Barium UT Beryllium UT Cadmium UT Chromium UT Cobalt UT Copper UT Lead UT Molybdenum UT Nickel UT Selenium UT Silver UT Thallium UT Vanadium UT Zinc UT Method EPA 7470 Analyte AB Analyte 10 Method 10 Mercury UT Method EPA 8081 Analyte AB Analyte 10 Method 10 4,4'-DDD UT ,4'-DDE UT ,4'-DDT UT Aldrin UT alpha-bhc (alpha-hexachlorocyclohexane) UT alpha-chlordane UT beta-bhc (beta-hexachlorocyclohexane) UT Chlordane (tech.) UT Page 1 of 18

3 1211/2017 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water delta-bhc (delta-hexachlorocyclohexane) UT Dieldrin UT Endosulfan I UT Endosulfan II UT Endosulfan sulfate UT Endrin UT Endrin aldehyde UT Endrin ketone UT gamma-bhc (Lindane, gamma-hexachlorocyclohexane) UT Heptachlor UT Heptachlor epoxide UT Methoxychlor UT Toxaphene (Chlorinated camphene) UT Method EPA 8082 Analyte AB Analyte 10 Method ID Aroclor-1016 (PCB-1016) UT Aroclor-1221 (PCB-1221) UT Aroclor-1232 (PCB-1232) UT Aroclor-1242 (PCB-1242) UT Aroclor-1248 (PCB-1248) UT Aroclor-1254 (PCB-1254) UT Aroclor-1260 (PCB-1260) UT PCBs (total) UT Method EPA 8141 Analyte AB Analyte 10 Method ID Azinphos-methyl (Guthion) UT Chlorpyrifos (Dursban) UT Demeton-o UT Demeton-s UT Diazinon UT Dimethoate UT Page 2 of 18

4 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water Disulfoton UT EPN (Phosphonothioic acid, phenyl-, O-ethyl O-(p-nitrophenyl) ester) UT Ethion UT Famphur UT Malathion UT Methyl parathion (Parathion, methyl) UT Mevinphos UT 7850 lo Naled UT 7905 lo Parathion, ethyl UT Phorate UT Ronnel UT 8110 lo Simazine UT 8125 lo Sulfotepp UT Method EPA ,4,5-T UT ,4-D UT 8545 lo ,4-DB UT 8560 lo ,5-Dichlorobenzoic acid UT 8600 lo Acifluorfen UT Bentazon UT 8530 lo Dacthal (DCPA) UT 8550 lo Dalapon UT Dicamba UT 8595 lo Dichloroprop (Dichlorprop, Weedone) UT 8605 lo Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) UT MCPA UT MCPP UT Pentachlorophenol UT 6605 lo Picloram UT Page 3 of 18

5 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water Silvex (2,4,5-TP) UT Method EPA ,1,1,2-Tetrachloroethane UT ,1,1-Trichloroethane UT ,1,2,2-Tetrachloroethane UT ,1,2-Trichloroethane UT ,1-Dichloroethane UT ,1-Dichloroethylene UT ,1-Dichloropropene UT ,2,3-Trichlorobenzene UT ,2,3-Trichloropropane UT ,2,4-Trichlorobenzene UT ,2,4-Trimethylbenzene UT ,2-Dibromo-3-chloropropane (DBCP) UT ,2-Dibromoethane (EDB, Ethylene dibromide) UT ,2-Dichlorobenzene UT ,2-Dichloroethane (Ethylene dichloride) UT ,2-Dichloropropane UT ,3,5-Trimethylbenzene UT ,3-Dichlorobenzene UT ,3-Dichloropropane UT ,4-Dichlorobenzene UT ,2-Dichloropropane UT Butanone (Methyl ethyl ketone, MEK) UT Chloroethyl vinyl ether UT Chlorotoluene UT Hexanone (MBK) UT Chlorotoluene UT Methyl-2-pentanone (MIBK) UT Page 4 of 18

6 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water Acetone (2-Propanone) UT Acrolein (Propenal) UT Acrylonitrile UT Benzene UT Bromobenzene UT Bromochloromethane UT Bromodichloromethane UT Bromoform UT Carbon disulfide UT Carbon tetrachloride UT Chlorobenzene UT Chlorodibromomethane UT Chloroethane (Ethyl chloride) UT Chloroform UT cis-1,2-dichloroethylene UT cis-1,3-dichloropropene UT Dibromomethane (Methylene bromide) UT Dichlorodifluoromethane (Freon-12) UT Ethylbenzene UT Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane) UT Hexachlorobutadiene UT Isopropylbenzene (Cumene) UT Methyl bromide (Bromomethane) UT Methyl chloride (Chloromethane) UT Methyl tert-butyl ether (MTBE) UT Methylene chloride (Dichloromethane) UT Naphthalene UT n-butylbenzene UT n-propylbenzene UT sec-butyl benzene UT Page 5 of 18

7 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water Styrene UT T-amylmethylether (TAME) UT tert-butyl alcohol UT tert-butylbenzene UT Tetrachloroethylene (Perchloroethylene) UT Toluene UT trans-1,2-dichloroethylene UT trans-1,3-dichloropropylene UT Trichloroethene (Trichloroethylene) UT Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) UT Vinyl acetate UT Vinyl chloride UT Xylene (total) UT Method EPA 8270 Analyte AB Analyte 10 Method 10 1,2,4-Trichlorobenzene UT ,2-Dichlorobenzene UT ,3-Dichlorobenzene UT ,4-Dichlorobenzene UT ,2' -Oxybis(1-chloropropane) (bis(2-chloro-1-methylethyl)ether) UT ,4,5-Trichlorophenol UT ,4,6-Trichlorophenol UT ,4-Dichlorophenol UT ,4-Dimethylphenol UT ,4-Dinitrophenol UT ,4-Dinitrotoluene (2,4-DNT) UT ,6-Dichlorophenol UT ,6-Dinitrotoluene (2,6-DNT) UT Chloronaphthalene UT Chlorophenol UT Page 6 of 18

8 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) UT Methylnaphthalene UT Methylphenol (o-cresol) UT Nitroaniline UT Nitrophenol UT ,3' -Dich lorobenzid ine UT Methylphenol (m-cresol) UT Nitroaniline UT Bromophenyl phenyl ether (BDE-3) UT Chloro-3-methylphenol UT Chloroaniline UT Chlorophenyl phenylether UT Methylphenol (p-cresol) UT Nitroaniline UT N itrophenol UT Acenaphthene UT Acenaphthylene UT Aniline UT Anthracene UT Benzo( a)anth racene UT Benzo(a)pyrene UT Benzo(b )fluoranthene UT Benzo(g, h, i)perylene UT Benzo(k)fluoranthene UT Benzoic acid UT Benzyl alcohol UT bis(2-chloroethoxy)methane UT bis(2-chloroethyl) ether UT bis(2-ethylhexyl) phthalate (Di(2-Ethylhexyl) phthalate, DEHP) UT Butyl benzyl phthalate UT Page 7 of 18

9 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water Carbazole UT Chrysene UT Dibenz(a,h) anthracene UT Dibenzofuran UT Diethyl phthalate UT Dimethyl phthalate UT Di-n-butyl phthalate UT Di-n-octyl phthalate UT Fluoranthene UT Fluorene UT Hexach lorobenzene UT Hexach lorobutad iene UT Hexachlorocyclopentadiene UT Hexach loroethane UT Indeno(1,2,3-cd) pyrene UT Isophorone UT Naphthalene UT Nitrobenzene UT n-nitrosodimethylamine UT n-nitrosodi-n-propylamine UT n-nitrosodiphenylamine UT Pentachlorophenol UT Phenanthrene UT Phenol UT Pyrene UT Pyridine UT Method EPA ,3,5-Trinitrobenzene (1,3,5-TN B) UT ,3-Dinitrobenzene (1,3-DNB) UT Page 8 of 18

10 T These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Non-Potable Water 2,4,6-Trinitrotoluene (2,4,6-TNT) UT ,4-Dinitrotoluene (2,4-DNT) UT ,6-Dinitrotoluene (2,6-DNT) UT Amino-4,6-dinitrotoluene (2-am-dnt) UT Nitrotoluene UT Nitrotoluene UT Amino-2,6-dinitrotoluene (4-am-dnt) UT Nitrotoluene UT Methyl-2,4,6-trinitrophenylnitramine (tetryl) UT Nitrobenzene UT Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) UT RDX (hexahydro-1,3,5-trinitro-1,3,5-triazine) UT Method EPA 9040 ph UT Method EPA 9056 Analyte AB Analyte 10 Method ID Chloride UT Fluoride UT Nitrate as N UT Nitrate-nitrite UT Orthophosphate as P UT Sulfate UT Method SM 2320 B Alkalinity as CaC03 UT Method SM 4500-S2- F Sulfide UT Page 9 of 18

11 T /2017 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials Method EPA 1311 Analyte AB Analyte 10 Method 10 TCLP UT Method EPA 6010 Analyte AB Analyte 10 Method 10 Antimony UT Arsenic UT Barium UT Beryllium UT Cadmium UT Chromium UT Cobalt UT Copper UT Lead UT Molybdenum UT Nickel UT Selenium UT Silver UT Thallium UT Vanadium UT Zinc UT Method EPA 7471 Analyte AB Analyte 10 Method 10 Mercury UT Method EPA 8081 Analyte AB Analyte 10 Method 10 4,4'-000 UT ,4'-00E UT ,4'-00T UT Aldrin UT alpha-bhc (alpha-hexachlorocyclohexane) UT Page 10 of 18

12 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials alpha-chlordane UT beta-b HC (beta-hexachlorocyclohexane) UT Chlordane (tech.) UT delta-bhc (delta-hexachlorocyclohexane) UT Dieldrin UT Endosulfan I UT Endosulfan II UT Endosulfan sulfate UT Endrin UT Endrin aldehyde UT Endrin ketone UT gamma-bhc (Lindane, gamma-hexachlorocyclohexane) UT gamma-chlordane UT Heptachlor UT Heptachlor epoxide UT Methoxychlor UT Toxaphene (Chlorinated camphene) UT Method EPA 8082 Aroclor-1016 (PCB-1016) UT Aroclor-1221 (PCB-1221) UT Aroclor-1232 (PCB-1232) UT Aroclor-1242 (PCB-1242) UT Aroclor-1248 (PCB-1248) UT Aroclor-1254 (PCB-1254) UT Aroclor (PCB-1260) UT PCBs (total) UT Method EPA 8141 Azinphos-methyl (Guthion) UT Chlorpyrifos (Dursban) UT Page 11 of 18

13 NElAP - Recognized laboratory Fields of Accreditation T These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials Demeton-o UT Demeton-s UT Diazinon UT Dimethoate UT Disulfoton UT EPN (Phosphonothioic acid, phenyl-, O-ethyl O-(p-nitrophenyl) ester) UT Ethion UT Famphur UT Malathion UT Methyl parathion (Parathion, methyl) UT Mevinphos UT Naled UT Parathion, ethyl UT Phorate UT Ronnel UT Simazine UT Sulfotepp UT Method EPA ,4,5-T UT ,4-D UT ,4-DB UT ,5-Dichlorobenzoic acid UT Acifluorfen UT Bentazon UT Dacthal (DCPA) UT Dalapon UT Dicamba UT Dichloroprop (Dichlorprop, Weedone) UT Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) UT Page 12 of 18

14 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials MCPA UT MCPP UT Pentachlorophenol UT Picloram UT Silvex (2,4,5-TP) UT Method EPA 8260 Analyte AB Analyte 10 Method 10 1,1,1,2-Tetrachloroethane UT ,1,1-Trichloroethane UT ,1,2,2-Tetrachloroethane UT ,1,2-Trichloroethane UT ,1-Dichloroethane UT , 1-Dich loroethylene UT ,1-Dichloropropene UT ,2,3-Trichlorobenzene UT ,2,3-Trichloropropane UT ,2,4-Trichlorobenzene UT ,2,4-Trimethylbenzene UT ,2-Dibromo-3-chloropropane (DBCP) UT ,2-Dibromoethane (EDB, Ethylene dibromide) UT ,2-Dichlorobenzene UT ,2-Dichloroethane (Ethylene dichloride) UT ,2-Dichloropropane UT ,3,5-Trimethylbenzene UT ,3-Dichlorobenzene UT ,3-Dichloropropane UT A-Dichlorobenzene UT ,2-Dichloropropane UT Butanone (Methyl ethyl ketone, MEK) UT Chloroethyl vinyl ether UT Page 13 of 18

15 1211/2017 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials 2-Chlorotoluene UT Hexanone (MBK) UT Chlorotoluene UT Methyl-2-pentanone (MIBK) UT ' Acetone (2-Propanone) UT Acrolein (Propenal) UT Acrylonitrile UT Benzene UT Bromobenzene UT Bromochloromethane UT Bromodichloromethane UT Bromoform UT Carbon disulfide UT Carbon tetrachloride UT Chlorobenzene UT Chlorodibromomethane UT Chloroethane (Ethyl chloride) UT Chloroform UT cis-1,2-dichloroethylene UT cis-1,3-dichloropropene UT Dibromomethane (Methylene bromide) UT Dichlorodifluoromethane (Freon-12) UT Ethylbenzene UT Hexach lorobutad iene UT Isopropylbenzene (Cumene) UT Methyl bromide (Bromomethane) UT Methyl chloride (Chloromethane) UT Methyl tert-butyl ether (MTBE) UT Methylene chloride (Dichloromethane) UT Naphthalene UT Page 14 of 18

16 T These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials n-butylbenzene UT n-propylbenzene UT sec-butyl benzene UT Styrene UT tert-butyl alcohol UT tert-butylbenzene UT Tetrachloroethylene (Perchloroethylene) UT Toluene UT trans-1,2-dichloroethylene UT trans-1,3-dichloropropylene UT Trichloroethene (Trichloroethylene) UT Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) UT Vinyl acetate UT Vinyl chloride UT Xylene (total) UT Method EPA ,2,4-Trichlorobenzene UT ,2-Dichlorobenzene UT ,3-Dichlorobenzene UT ,4-Dichlorobenzene UT ,2' -Oxybis( 1-ch loropropane) (bis(2-chloro-1-methylethyl)ether) UT ,4,5-Trichlorophenol UT ,4,6-Trichlorophenol UT ,4-Dichlorophenol UT ,4-Dimethylphenol UT ,4-Dinitrophenol UT ,4-Dinitrotoluene (2,4-DNT) UT ,6-Dichlorophenol UT ,6-Dinitrotoluene (2,6-DNT) UT Page 15 of 18

17 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials 2-Chloronaphthalene UT Chlorophenol UT Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) UT Methylnaphthalene UT Methylphenol (a-cresol) UT Nitroaniline UT Nitrophenol UT ,3'-Dichlorobenzidine UT Methylphenol (m-cresol) UT Nitroaniline UT Bromophenyl phenyl ether (BDE-3) UT Chloro-3-methylphenol UT Chlorophenyl phenylether. UT Methylphenol (p-cresol) UT Nitroaniline UT Nitrophenol UT Acenaphthene UT Acenaphthylene UT Aniline UT Anthracene UT Benzo(a)anthracene UT Benzo(a)pyrene UT Benzo(b )fluoranthene UT Benzo(g, h, i)perylene UT Benzo(k)fluoranthene UT Benzoic acid UT Benzyl alcohol UT bis(2-chloroethoxy)methane UT bis(2-chloroethyl) ether UT bis(2-ethylhexyl) phthalate (Di(2-Ethylhexyl) phthalate, DEHP) UT Page 16 of 18

18 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials Butyl benzyl phthalate UT Carbazole UT Chrysene UT Dibenz(a,h) anthracene UT Dibenzofuran UT Diethyl phthalate UT Dimethyl phthalate UT Di-n-butyl phthalate UT Di-n-octyl phthalate UT Fluoranthene UT Fluorene UT Hexachlorobenzene UT Hexachlorobutadiene UT Hexachlorocyclopentadiene UT Hexachloroethane UT Indeno(1,2,3-cd) pyrene UT Isophorone UT Naphthalene UT Nitrobenzene UT n-nitrosodimethylamine UT n-nitrosodi-n-propylamine UT n-nitrosodiphenylamine UT Pentachlorophenol UT Phenanthrene UT Phenol UT Pyrene UT Pyridine UT Method EPA ,3,5-Trinitrobenzene (1,3,5-TNB) UT Page 17 of 18

19 These fields of accreditation supercede all previous fields. The Texas Commission on urges customers to Matrix: Solid & Chemical Materials 1,3-Dinitrobenzene (1,3-DNB) UT ,4,6-Trinitrotoluene (2,4,6-TNT) UT ,4-Dinitrotoluene (2,4-DNT) UT ,6-Dinitrotoluene (2,6-DNT) UT Amino-4,6-dinitrotoluene (2-am-dnt) UT Nitrotoluene UT Nitrotoluene UT Amino-2,6-dinitrotoluene (4-am-dnt) UT Nitrotoluene UT Methyl-2,4,6-trinitrophenylnitramine (tetryl) UT Nitrobenzene UT Octahydro-1,3,5,7 -tetranitro-1,3,5,7-tetrazocine (HMX) UT RDX (hexahydro-1,3,5-trinitro-1,3,5-triazine) UT Method EPA 9045 Analyte AB Analyte 10 Method ID ph UT Method EPA 9056 Analyte AB Analyte 10 Method ID Chloride UT Fluoride UT Nitrate as N UT Nitrate-nitrite UT Nitrite as N UT Orthophosphate as P UT Sulfate UT Method TCEQ 1005 Total Petroleum Hydrocarbons (TPH) TX Page 18 of 18

Texas Commission on Environmental Quality

Texas Commission on Environmental Quality Method 40 CFR Part 50 Appendix L AB ID Method ID Fine particulates