TOCOBIOL SF C. Natural Antioxidant made up of mixed Tocopherols concentrate from natural NONGMO origin. Helianthus Annuus Seed Oil

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1 TOCOBIOL SF C Natural Antioxidant made up of mixed Tocopherols concentrate from natural NONGMO origin. TOCOBIOL, E % INCI NAME Tocopherol (mixed), Beta-Sitosterol, Squalene CAS NUMBER / / / / / EINECS / / / / / CARRIER: Helianthus Annuus Seed Oil STEROLS Campsterol % Stigmasterol % B-Sitosterol %

2 Appearance: Solubility: Heavy Metals Arsenic Pesticides Oily liquid. Colour amber-yellowish to dark amber. It is possible the presence of cereous components in microcrystalline form. Insoluble in water. Soluble in fats and oils. Not more than 10 ppm Not more than 3 ppm Absence E.coli: Negative Salmonella: Negative Natural antioxidant especially appropriate for edible fats and oils, meat products, snacks, essential oils and natural flavourings. 0,02-0,03% regarding the fat contents. 1, 2 5 and 5 Kg white polypropylene carafes in 20 Kg boxes, 10 kg carafes packaging. We recommend storing the product in tightly closed containers under room temperature

3 conditions away from oxygen, heat and light. Once open, use immediately. Shelf-life: 2 years under the above mentioned storage conditions. NON-GMO Certificate. KOSHER Certificate. Detailed data upon request.

4 LABORATORY REPORT ANTIOXIDANT ACTIVITY OF TOCOBIOL IN COCONUT OIL PROCEDURE RANCIMAT METHOD at 98ºC and 120ºC ANTIOXIDANTS TESTED TOCOBIOL BHA 200 ppm 200 ppm Horas Ranci mat Sin antioxidante BHA 120ºC 98ºC RESULTS Comparison of induction times determined by Rancimat The results obtained indicate that TOCOBIOL is the antioxidant that provides a greater stability for Coconut Oil. Assays performed at 98ºC show that TOCOBIOL increases this oil stability in 75% while BHA samples show an increase of stability of 25%. At 120ºC the induction time of the sample which contains TOCOBIOL is 32,8 hours. That means an increase of the Coconut Oil stability of 6 test hours. The sample containing BHA shows an induction time increase of 0,7 hours.

5 LABORATORY REPORT COMPARATIVE STABILITY STUDY OF BULK S STABILIZED WITH TOCOBIOL Lab report #: 290 B Date: September 3 rd 2008 AIM Samples of lip stick mass containing different doses of TOCOBIOL will be tested using the Rancimat method to determinate the protection against oxidation provided by the mentioned Tocobiol doses. Initial oxidation level of every sample will be tested measuring its Peroxide Value Index. S TESTED Samples with the remarked doses of Tocobiol are received on August 13 th. follows. They are named as TOCOBIOL amount 1A TOC A A TOC B A TOC C B TOC D B TOC E B TOC F C TOC G C TOC H C TOC I

6 ANALYTICAL METHOD: 1. PEROXIDE INDEX Peroxide value index determination is done under UNE regulations PEROXIDE INDEX (meq O 2 / kg fat) 1A TOC A 78 (without antioxidant) 8.7 2A TOC B A TOC C B TOC D 78 (without antioxidant) 3.1 2B TOC E B TOC F C TOC G 78 (without antioxidant) 8.0 2C TOC H C TOC I RANCIMAT METHOD Rancimat test has been carried out over every sample to determinate the protection level provided by Tocobiol at the used dosage.

7 RANCIMAT METHOD FOR A RANGE S TEMPERATURE: 120º C AIR FLOW: 20 l/ h CONDUCTIVITY RANGE : 200 µs FAT MEDIUM: 1A, 2A, 3A S RESULTS: Rancimat hours Stability increasing 1.- 1A TOC A 78 (WITHOUT ANTIOXIDANT) 5,15 h A TOC B 78 14,3 h 177,7% 3.- 3A TOC C 78 20,9 h 305,8% Shown graphically: "A" RANGE S 25 Rancimat Hours A TOC A 78 (W.A.) 2A TOC B 78 3A TOC C 78

8 RANCIMAT METHOD FOR B RANGE S TEMPERATURE: 120º C AIR FLOW: 20 l/ h CONDUCTIVITY RANGE: 200 µs FAT MEDIUM: 1B, 2B, 3B S RESULTS: Rancimat hours Stability increasing 1.- 1B TOC D 78 (W.A.) 10,4 h B TOC E 78 30,1 h 189,4% 3.- 3B TOC F 78 51,0 h 390,0% Shown graphically:

9 "B" RANGE S Rancimat hours B TOC D 78 (W.A.) 2B TOC E 78 3B TOC F 78 RANCIMAT METHOD FOR C RANGE S TEMPERATURE: 120º C AIR FLOW: 20 l/ h CONDUCTIVITY RANGE: 200 µs FAT MEDIUM: 1C, 2C, 3C S RESULTS: Rancimat Hours Stability increasing 1.- 1C TOC G 78 (W.A.) 27,5 h C TOC H 78 41,2 h 49,8% 3.- 3C TOC I 78 51,2 h 86,2% Shown graphically:

10 "C" RANGE S Rancimat Hours C TOC G 78 (W.A.) 2C TOC H 78 3C TOC I ORGANOLEPTIC CHARACTERISTICS The samples sent by the customer show the following organoletic properties: ORGANOLEPTIC PROPERTIES 1A TOC A 78 Pasty cream / 2A TOC B 78 3A TOC C 78 Light green colored 1B TOC D 78 Pasty cream / 2B TOC E 78 Yellow - grey colored 3B TOC F 78 1C TOC G 78 Greasy cream / 2C TOC H 78 Light yellow colored

11 3C TOC I 78 CONCLUSIONS Looking at the initial Peroxide Value index of the samples, we find that all mixes containing TOCOBIOL, get better results than the one without it. That means that even from the manufacturing time, Tocobiol provides a high level of protection against oxidation. No difference in organoleptic properties are reported in the samples containing TOCOBIOL regarding the ones without it. Natural antioxidant TOCOBIOL gets better results when used over the most unstable samples (A and B range) getting a stability increasing up to 300 % for A and 390% for B. The stability improvement for C sample is lower (86%) because the Peroxide Value Index shows that its oxidation level is lower. Sample C seems to be the more stable mix. The adition of TOCOBIOL to every sample tested produces high increasings in the product s stability (up to 390% for B samples) without any organoleptical change.