July 23, Ms. Shanna Schmitt, Project Manager Minnesota Pollution Control Agency VIC Program 520 Lafayette Road St. Paul, Minnesota

Transcription

1 Wenck Associates, Inc Wooddale Drive Suite 100 Woodbury, MN (651) Fax (651) July 23, 2014 Ms. Shanna Schmitt, Project Manager Minnesota Pollution Control Agency VIC Program 520 Lafayette Road St. Paul, Minnesota Ms. Amy Hadiaris, Technical Analyst Minnesota Pollution Control Agency VIC Program 520 Lafayette Road St. Paul, Minnesota RE: Response Action Plan (RAP) Amendment (IRP Site K / Building 102, Former Twin Cities Army Ammunition Plant) Project Name: TCAAP Redevelopment #2 Site (427-Acre Portion of Former Twin Cities Army Ammunition Plant) MPCA ID #: VP22891 Wenck Proj. #: Dear Ms. Schmitt and Ms. Hadiaris: The purpose of this correspondence is to request an amendment of the Site K Response Action Plan (RAP) and Building 102 RAP, previously approved by the MPCA in letters dated April 30, 2014, and June 4, 2014, respectively. In general, the approved RAPs provide for excavation of approximately 11,400 cubic yards of media impacted with volatile organic compound (VOCs) present above the groundwater table at the two sites and mechanically venting the excavated media for a period of approximately one year. Subsequent to treatment, the approved RAPs allow on-site disposition of the treated media if it meets cleanup criteria as stated in the RAPs as initially submitted and approved, or off-site disposal in a lined landfill in the event that the treated media does not meet cleanup criteria. The original volumes of impacted media were calculated based on an historical average groundwater table depth of 7 to 8 feet below grade. Current groundwater levels at the Building 102 and Site K are higher (approximately 4 feet below grade) than in the past, thus reducing the media requiring removal. Based on the anticipated change in site conditions, it is more economical to excavate the VOC-impacted media and dispose of the media off-site in a lined landfill. Additionally, based on the results of sub-slab VOC soil sample analysis, the proposed area of remediation for the Building 102 RAP has been modified slightly (see attached figure). Wenck acknowledges that proposed excavation areas for both Site K and Building 102 are subject to further expansion should confirmation sampling results fail to achieve the applicable cleanup criteria for those sites. Based upon the foregoing, Wenck requests that the MPCA provide written approval of this request for amendment of the Site K and Building 102 RAPs to allow excavation and off-site disposal, without treatment, of VOC impacted media exceeding the cleanup criteria. Given the current project schedule, we request approval of this request on or before Friday, July 28, 2014, if at all possible. N:\Technical\0979 Bolander\03 Field Investigation\Site K_Bldg 102 RAP Amendment\Site K_Bldg 102 RAP Amendment.docx

2 Shanna Schmitt and Amy Hadiaris Minnesota Pollution Control Agency July 23, 2014 In addition, per comment #2 in the RAP approval letter related to Building 102 dated June 4, 2014, Wenck is providing documentation related to the Building 102 floor penetration sampling activities. Attached please find a figure showing the sample locations and revised proposed remedial excavation limits based on the findings, a data table summarizing the floor penetration soil analytical results, and a copy of the soil analytical laboratory reports. If you have any questions, please contact me at (651) , or Joe Otte at (651) Thank you. Sincerely, WENCK ASSOCIATES, INC. Shane Waterman, PG Principal J. Joseph Otte Principal Enclosures C: Mr. Jay Biedny, Ramsey County Mr. Rick Van Allen, Bay West Mr. Rick Kubler, Gray Plant Mooty Attachments: Attachment 1 Revised Figure 3-1 (Building Proposed Excavation Limits) from Building 102 RAP dated February 2014 Attachment 2 Table 1 - Summary of Floor Penetration Soil Analytical Results Attachment 3 Soil Analytical Laboratory Reports and Chain-of-Custody Documentation 2 N:\Technical\0979 Bolander\03 Field Investigation\Site K_Bldg 102 RAP Amendment\Site K_Bldg 102 RAP Amendment.docx

3 Attachment 1 Revised Figure 3-1 (Building Proposed Excavation Limits) from the Building 102 Response Action Plan dated February 2014

4 01L582 01U582 SS SB SB Tetrachloroethene 01U581 RI SS Tetrachloroethene RI SS RI L583 01L581 01U583 01L584 01U VOC VOC-07 RI SS SS VOC-08 RI SS SS Copper SS Lead SS Total PCBs RI U580 RI SS SB VOC-01 RI VOC-02 SS SB RI SS SS U579 SS VOC-13 Trichloroethene RI SS 1003VOC-21 RI RI SS 1003VOC VOC VOC-11 SS SB RI VOC-16 Methylene Chloride 1003VOC VOC VOC-39 Former Building VOC VOC VOC VOC VOC VOC VOC VOC-28 SS VOC-33 SS Diesel Range Organics (DRO) 1003VOC VOC VOC VOC VOC VOC VOC VOC-43 RI SS RI SS SB SS VOC VOC VOC VOC-05 RI SS 1003VOC-30 RI RI SS SS RI Copper RI SS 1003VOC-31 SS VOC VOC VOC-29 SS SS Total PCBs SS VOC-15 01U578 Methylene Chloride 1003VOC-24 SS SB VOC-03 RI RI SS 1003VOC VOC-49 RI SS RI RI SS 1003VOC VOC VOC VOC-48 RI RI SS Legend " ) " ) ( 2012 Aerial Photograph (Source: ESRI) Path: N:\GIS\KEM\Working Docs\Proposed Excavation Limits.mxd Date: 7/23/2014 Time: 4:33:27 PM User: MilKE0481 ( 100 Feet ± ESA Section 1003 VOC Sample Locations (VOC Sample Results below Tier 1 SRV and/or Tier 1 SLV) Extraction Well Monitoring Well Sample result below MPCA Tier I SRV and Screening SLV Hot Spot Location (Sample result above Source: Esri, DigitalGlobe, GeoEye, i-cubed, USDA, USGS, AEX, and/or Getmapping, Aerogrid, IGN, IGP, MPCA Tier I SRV Tier 1 SLV) swisstopo, and the GIS User Community ( RAMSEY COUNTY Building Proposed Excavation Limits Proposed Excavation Engineers - Scientists Business Professionals Wenck 1800 Pioneer Creek Center Maple Plain, MN JULY 2014 Figure 3-1

5 Attachment 2 Table 1 Summary of Floor Penetration Soil Analytical Results

6 Table 1 Summary of Floor Penetration Soil Analytical Results Building 102, Plexus Section 1003 TCAAP Redevelopment #2 Site Arden Hills, Minnesota Sample ID Map ID 1003VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC-12 Sample Collection Date 19-Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun-14 Detected Parameter Method Units Tier I SRV Tier I SLV Acetone EPA 8260 ug/kg 340,000 8,400 <21.5 <21.1 <22.3 <21.7 <22.4 <21.6 <22.5 <24.0 <20.9 <20.7 <21.9 <22.8 Methylene Chloride EPA 8260 ug/kg 97, <21.5 <21.1 <22.3 <21.7 <22.4 <21.6 <22.5 <24.0 <20.9 <20.7 <21.9 <22.8 Tetrachloroethene EPA 8260 ug/kg 72, < <4.5 <4.3 <4.5 <4.3 <4.5 <4.8 <4.2 <4.1 <4.4 <4.6 Trichloroethene EPA 8260 ug/kg 29, <4.3 <4.2 <4.5 <4.3 <4.5 <4.3 <4.5 <4.8 <4.2 <4.1 <4.4 <4.6 Sample ID MS/MSD Map ID 1003VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC-24 Sample Collection Date 19-Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun-14 Detected Parameter Method Units Tier I SRV Tier I SLV Acetone EPA 8260 ug/kg 340,000 8,400 <22.1 <23.7 <22.7 < <22.1 <21.0 <24.2 <21.3 <20.8 <21.3 <21.8 Methylene Chloride EPA 8260 ug/kg 97, <22.1 < <22.4 <22.1 <21.0 <24.2 <21.3 <20.8 <21.3 <21.8 Tetrachloroethene EPA 8260 ug/kg 72, <4.4 <4.7 <4.5 <4.4 <4.5 <4.4 <4.2 <4.8 <4.3 <4.2 <4.3 <4.4 Trichloroethene EPA 8260 ug/kg 29, <4.7 <4.5 <4.4 <4.5 <4.4 <4.2 <4.8 <4.3 <4.2 <4.3 <4.4 Sample ID Map ID 1003VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC-36 Sample Collection Date 16-Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun-14 Detected Parameter Method Units Tier I SRV Tier I SLV Acetone EPA 8260 ug/kg 340,000 8,400 <21.8 <21.8 <23.6 <21.2 <22.6 <21.4 <22.0 <21.2 <21.2 <21.1 <22.5 <20.8 Methylene Chloride EPA 8260 ug/kg 97, <21.8 <21.8 <23.6 <21.2 <22.6 <21.4 <22.0 <21.2 <21.2 <21.1 <22.5 <20.8 Tetrachloroethene EPA 8260 ug/kg 72, <4.4 <4.4 <4.7 <4.2 <4.5 <4.3 <4.4 <4.2 <4.2 <4.2 <4.5 <4.2 Trichloroethene EPA 8260 ug/kg 29, <4.4 <4.4 <4.7 <4.2 <4.5 <4.3 <4.4 <4.2 <4.2 <4.2 <4.5 <4.2 Sample ID Map ID 1003VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC-48 Sample Collection Date 16-Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun Jun-14 Detected Parameter Method Units Tier I SRV Tier I SLV Acetone EPA 8260 ug/kg 340,000 8,400 <20.7 <21.1 <22.4 <22.5 <22.8 <23.1 <21.6 <21.5 <21.1 <20.4 <21.5 <22.4 Methylene Chloride EPA 8260 ug/kg 97, <20.7 <21.1 <22.4 <22.5 <22.8 <23.1 <21.6 <21.5 <21.1 <20.4 <21.5 <22.4 Tetrachloroethene EPA 8260 ug/kg 72, <4.1 <4.2 <4.5 <4.5 <4.6 <4.6 <4.3 <4.3 <4.2 <4.1 <4.3 <4.5 Trichloroethene EPA 8260 ug/kg 29, <4.1 <4.2 <4.5 <4.5 <4.6 <4.6 <4.3 <4.3 <4.2 <4.1 <4.3 < Sample ID MS/MSD Map ID 1003VOC-49 Sample Collection Date 16-Jun-14 Detected Parameter Method Units Tier I SRV Tier I SLV Acetone EPA 8260 ug/kg 340,000 8,400 <21.8 Methylene Chloride EPA 8260 ug/kg 97, <21.8 Tetrachloroethene EPA 8260 ug/kg 72, <4.4 Trichloroethene EPA 8260 ug/kg 29, <4.4 Notes: µg/kg = milligrams per kilogram (parts per billion) 30.6 = Analyte detected above the lab reporting limit but less than regulatory limit 38.6 = Analyte detected above Tier I SRV and/or Tier I SLV Tier I SRV = Minnesota Department of Health Tier I Soil Reference Value Screening SLVs = MPCA May 2013 Screening Soil Leaching Values. N:\Technical\0979 Bolander\03 Field Investigation\Site K_Bldg 102 RAP Amendment\Floor Penetration Soil Sample Results.xlsx.xls

7 Attachment 3 Soil Analytical Laboratory Reports and Chain-of-Custody Documentation

8 #=CL# LIMS USE: FR - SHANE WATERMAN LIMS OBJECT ID: July 02, 2014 Shane Waterman Wenck Associates Inc 1802 Wooddale Drive Suite 100 Saint Paul, MN RE: Dear Shane Waterman: Enclosed are the analytical results for sample(s) received by the laboratory on June 19, The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kabor Xiong kabor.xiong@pacelabs.com Project Manager Enclosures cc: Matt Bowers, Wenck Associate Inc without the written consent of. Page 1 of 67

9 #=CP# CERTIFICATIONS Minnesota Certification IDs 1700 Elm Street SE Suite 200, A2LA Certification #: Alabama Certification #40770 Alabama Certification #40770 Alaska Certification #: UST-078 Alaska Certification #MN00064 Arizona Certification #: AZ-0014 Arkansas Certification #: California Certification #: 01155CA Colorado Certification #Pace Connecticut Certification #: PH-0256 EPA Region 8 Certification #: 8TMS-L Florida/NELAP Certification #: E87605 Guam Certification #: Pace Georgia Certification #: 959 Idaho Certification #: MN00064 Hawaii Certification #MN00064 Illinois Certification #: Indiana Certification#C-MN-01 Iowa Certification #: 368 Kansas Certification #: E Kentucky Dept of Envi. Protection - DW #90062 Kentucky Dept of Envi. Protection - WW #:90062 Louisiana DEQ Certification #: 3086 Louisiana DHH #: LA Maine Certification #: Maryland Certification #: 322 Michigan DEPH Certification #: 9909 Minnesota Certification #: Mississippi Certification #: Pace Montana Certification #: MT0092 Nebraska Certification #: Pace New Jersey Certification #: MN-002 New Jersey Certification #: MN-002 New York Certification #: North Carolina Certification #: 530 North Carolina State Public Health #: North Dakota Certification #: R-036 Ohio EPA #: 4150 Ohio VAP Certification #: CL101 Oklahoma Certification #: 9507 Oregon Certification #: MN Oregon Certification #: MN Pennsylvania Certification #: Puerto Rico Certification Saipan (CNMI) #:MP0003 South Carolina #: Texas Certification #: T Tennessee Certification #: Utah Certification #: MN Virginia DGS Certification #: 251 Virginia/VELAP Certification #: Pace Washington Certification #: C486 Wisconsin Certification #: West Virginia Certification #: 382 West Virginia TO-15 Approval West Virginia DHHR #:9952C without the written consent of. Page 2 of 67

10 #=SS# SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received Solid 06/19/14 09:10 06/19/14 10: Solid 06/19/14 09:12 06/19/14 10: Solid 06/19/14 09:14 06/19/14 10: Solid 06/19/14 09:16 06/19/14 10: Solid 06/19/14 09:18 06/19/14 10: Solid 06/19/14 09:20 06/19/14 10: Solid 06/19/14 09:22 06/19/14 10: Solid 06/19/14 09:24 06/19/14 10: Solid 06/19/14 09:26 06/19/14 10: Solid 06/19/14 09:28 06/19/14 10: DUP-1 Solid 06/19/14 00:00 06/19/14 10: Solid 06/19/14 09:30 06/19/14 10: Solid 06/19/14 09:32 06/19/14 10: Solid 06/19/14 09:34 06/19/14 10: Solid 06/19/14 09:36 06/19/14 10: Solid 06/19/14 09:38 06/19/14 10: Solid 06/19/14 09:40 06/19/14 10: Solid 06/19/14 09:42 06/19/14 10: Solid 06/19/14 09:44 06/19/14 10: Solid 06/19/14 09:46 06/19/14 10: DUP-4 Solid 06/19/14 00:00 06/19/14 10:27 without the written consent of. Page 3 of 67

11 #=SA# SAMPLE ANALYTE COUNT Lab ID Sample ID Method Analysts Analytes Reported Laboratory ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M DUP-1 ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M without the written consent of. Page 4 of 67

12 #=SA# SAMPLE ANALYTE COUNT Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M DUP-4 ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M without the written consent of. Page 5 of 67

13 #=NA# PROJECT NARRATIVE Method: EPA 8260 Description: Client: Wenck Associates, Inc. Date: July 02, 2014 General Information: 21 samples were analyzed for EPA All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 5035A with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. QC Batch: MSV/27507 IS: The internal standard recovery associated with this result exceeds the lower control limit. The reported result should be considered an estimated value (Lab ID: ) Acetone Tetrahydrofuran QC Batch: MSV/27518 IS: The internal standard recovery associated with this result exceeds the lower control limit. The reported result should be considered an estimated value. MS (Lab ID: ) Acetone Tetrahydrofuran MSD (Lab ID: ) Acetone Tetrahydrofuran Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. without the written consent of. Page 6 of 67

14 #=NA# PROJECT NARRATIVE Method: EPA 8260 Description: Client: Wenck Associates, Inc. Date: July 02, 2014 Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. QC Batch: MSV/27518 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MS (Lab ID: ) Bromomethane MSD (Lab ID: ) Bromomethane QC Batch: MSV/27523 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MS (Lab ID: ) Acetone R1: RPD value was outside control limits. MSD (Lab ID: ) 2-Butanone (MEK) Acetone Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. without the written consent of. Page 7 of 67

15 Sample: Lab ID: Collected: 06/19/14 09:10 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 14.1 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 15: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Benzene ND ug/kg /20/14 07:40 06/21/14 15: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 15: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromoform ND ug/kg /20/14 07:40 06/21/14 15: Bromomethane ND ug/kg /20/14 07:40 06/21/14 15: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 15: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 15: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Chloroethane ND ug/kg /20/14 07:40 06/21/14 15: Chloroform ND ug/kg /20/14 07:40 06/21/14 15: Chloromethane ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 15: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 15: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 15: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 15: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 8 of 67

16 Sample: Lab ID: Collected: 06/19/14 09:10 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 15: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 15: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 15: Naphthalene ND ug/kg /20/14 07:40 06/21/14 15: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Styrene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 15: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 15: Toluene ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 99 % /20/14 07:40 06/21/14 15: Toluene-d8 (S) 106 % /20/14 07:40 06/21/14 15: Bromofluorobenzene (S) 104 % /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 9 of 67

17 Sample: Lab ID: Collected: 06/19/14 09:12 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.0 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 15: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Benzene ND ug/kg /20/14 07:40 06/21/14 15: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 15: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromoform ND ug/kg /20/14 07:40 06/21/14 15: Bromomethane ND ug/kg /20/14 07:40 06/21/14 15: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 15: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 15: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Chloroethane ND ug/kg /20/14 07:40 06/21/14 15: Chloroform ND ug/kg /20/14 07:40 06/21/14 15: Chloromethane ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 15: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 15: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 15: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 15: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 10 of 67

18 Sample: Lab ID: Collected: 06/19/14 09:12 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 15: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 15: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 15: Naphthalene ND ug/kg /20/14 07:40 06/21/14 15: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Styrene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: Tetrachloroethene 41.3 ug/kg /20/14 07:40 06/21/14 15: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 15: Toluene ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 98 % /20/14 07:40 06/21/14 15: Toluene-d8 (S) 106 % /20/14 07:40 06/21/14 15: Bromofluorobenzene (S) 106 % /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 11 of 67

19 Sample: Lab ID: Collected: 06/19/14 09:14 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.9 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 15: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Benzene ND ug/kg /20/14 07:40 06/21/14 15: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 15: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromoform ND ug/kg /20/14 07:40 06/21/14 15: Bromomethane ND ug/kg /20/14 07:40 06/21/14 15: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 15: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 15: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Chloroethane ND ug/kg /20/14 07:40 06/21/14 15: Chloroform ND ug/kg /20/14 07:40 06/21/14 15: Chloromethane ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 15: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 15: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 15: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 15: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 12 of 67

20 Sample: Lab ID: Collected: 06/19/14 09:14 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 15: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 15: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 15: Naphthalene ND ug/kg /20/14 07:40 06/21/14 15: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Styrene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 15: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 15: Toluene ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 99 % /20/14 07:40 06/21/14 15: Toluene-d8 (S) 106 % /20/14 07:40 06/21/14 15: Bromofluorobenzene (S) 108 % /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 13 of 67

21 Sample: Lab ID: Collected: 06/19/14 09:16 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 10.9 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 15: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Benzene ND ug/kg /20/14 07:40 06/21/14 15: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 15: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 15: Bromoform ND ug/kg /20/14 07:40 06/21/14 15: Bromomethane ND ug/kg /20/14 07:40 06/21/14 15: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 15: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 15: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Chloroethane ND ug/kg /20/14 07:40 06/21/14 15: Chloroform ND ug/kg /20/14 07:40 06/21/14 15: Chloromethane ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 15: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 15: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 15: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 15: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 15: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 14 of 67

22 Sample: Lab ID: Collected: 06/19/14 09:16 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 15: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 15: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 15: Naphthalene ND ug/kg /20/14 07:40 06/21/14 15: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Styrene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 15: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 15: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 15: Toluene ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 15: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 15: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 15: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 15: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 15: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 15: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 100 % /20/14 07:40 06/21/14 15: Toluene-d8 (S) 104 % /20/14 07:40 06/21/14 15: Bromofluorobenzene (S) 114 % /20/14 07:40 06/21/14 15: Date: 07/02/ :09 PM without the written consent of. Page 15 of 67

23 Sample: Lab ID: Collected: 06/19/14 09:18 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 11.5 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 16: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 16: Benzene ND ug/kg /20/14 07:40 06/21/14 16: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 16: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 16: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 16: Bromoform ND ug/kg /20/14 07:40 06/21/14 16: Bromomethane ND ug/kg /20/14 07:40 06/21/14 16: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 16: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 16: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: Chloroethane ND ug/kg /20/14 07:40 06/21/14 16: Chloroform ND ug/kg /20/14 07:40 06/21/14 16: Chloromethane ND ug/kg /20/14 07:40 06/21/14 16: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 16: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 16: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 16: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 16: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 16: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 16: Date: 07/02/ :09 PM without the written consent of. Page 16 of 67

24 Sample: Lab ID: Collected: 06/19/14 09:18 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 16: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 16: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 16: Naphthalene ND ug/kg /20/14 07:40 06/21/14 16: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Styrene ND ug/kg /20/14 07:40 06/21/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 16: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 16: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 16: Toluene ND ug/kg /20/14 07:40 06/21/14 16: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 16: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 16: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 16: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 16: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /20/14 07:40 06/21/14 16: Toluene-d8 (S) 108 % /20/14 07:40 06/21/14 16: Bromofluorobenzene (S) 106 % /20/14 07:40 06/21/14 16: Date: 07/02/ :09 PM without the written consent of. Page 17 of 67

25 Sample: Lab ID: Collected: 06/19/14 09:20 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.0 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 16: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 16: Benzene ND ug/kg /20/14 07:40 06/21/14 16: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 16: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 16: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 16: Bromoform ND ug/kg /20/14 07:40 06/21/14 16: Bromomethane ND ug/kg /20/14 07:40 06/21/14 16: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 16: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 16: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: Chloroethane ND ug/kg /20/14 07:40 06/21/14 16: Chloroform ND ug/kg /20/14 07:40 06/21/14 16: Chloromethane ND ug/kg /20/14 07:40 06/21/14 16: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 16: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 16: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 16: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 16: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 16: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 16: Date: 07/02/ :09 PM without the written consent of. Page 18 of 67

26 Sample: Lab ID: Collected: 06/19/14 09:20 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 16: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 16: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 16: Naphthalene ND ug/kg /20/14 07:40 06/21/14 16: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Styrene ND ug/kg /20/14 07:40 06/21/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 16: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 16: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 16: Toluene ND ug/kg /20/14 07:40 06/21/14 16: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 16: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 16: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 16: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 16: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 101 % /20/14 07:40 06/21/14 16: Toluene-d8 (S) 102 % /20/14 07:40 06/21/14 16: Bromofluorobenzene (S) 102 % /20/14 07:40 06/21/14 16: Date: 07/02/ :09 PM without the written consent of. Page 19 of 67

27 Sample: Lab ID: Collected: 06/19/14 09:22 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 15.5 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 16: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 16: Benzene ND ug/kg /20/14 07:40 06/21/14 16: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 16: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 16: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 16: Bromoform ND ug/kg /20/14 07:40 06/21/14 16: Bromomethane ND ug/kg /20/14 07:40 06/21/14 16: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 16: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 16: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: Chloroethane ND ug/kg /20/14 07:40 06/21/14 16: Chloroform ND ug/kg /20/14 07:40 06/21/14 16: Chloromethane ND ug/kg /20/14 07:40 06/21/14 16: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 16: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 16: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 16: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 16: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 16: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 16: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 16: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 16: Date: 07/02/ :09 PM without the written consent of. Page 20 of 67

28 Sample: Lab ID: Collected: 06/19/14 09:22 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 16: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 16: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 16: Naphthalene ND ug/kg /20/14 07:40 06/21/14 16: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Styrene ND ug/kg /20/14 07:40 06/21/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 16: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 16: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 16: Toluene ND ug/kg /20/14 07:40 06/21/14 16: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 16: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 16: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 16: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 16: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 16: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 16: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 16: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 101 % /20/14 07:40 06/21/14 16: Toluene-d8 (S) 111 % /20/14 07:40 06/21/14 16: Bromofluorobenzene (S) 109 % /20/14 07:40 06/21/14 16: Date: 07/02/ :09 PM without the written consent of. Page 21 of 67

29 Sample: Lab ID: Collected: 06/19/14 09:24 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 16.9 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 17: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 17: Benzene ND ug/kg /20/14 07:40 06/21/14 17: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 17: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 17: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 17: Bromoform ND ug/kg /20/14 07:40 06/21/14 17: Bromomethane ND ug/kg /20/14 07:40 06/21/14 17: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 17: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 17: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: Chloroethane ND ug/kg /20/14 07:40 06/21/14 17: Chloroform ND ug/kg /20/14 07:40 06/21/14 17: Chloromethane ND ug/kg /20/14 07:40 06/21/14 17: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 17: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 17: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 17: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 17: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 17: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 17: Date: 07/02/ :09 PM without the written consent of. Page 22 of 67

30 Sample: Lab ID: Collected: 06/19/14 09:24 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 17: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 17: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 17: Naphthalene ND ug/kg /20/14 07:40 06/21/14 17: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Styrene ND ug/kg /20/14 07:40 06/21/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 17: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 17: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 17: Toluene ND ug/kg /20/14 07:40 06/21/14 17: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 17: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 17: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 17: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 17: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 105 % /20/14 07:40 06/21/14 17: Toluene-d8 (S) 103 % /20/14 07:40 06/21/14 17: Bromofluorobenzene (S) 110 % /20/14 07:40 06/21/14 17: Date: 07/02/ :09 PM without the written consent of. Page 23 of 67

31 Sample: Lab ID: Collected: 06/19/14 09:26 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.2 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 17: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 17: Benzene ND ug/kg /20/14 07:40 06/21/14 17: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 17: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 17: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 17: Bromoform ND ug/kg /20/14 07:40 06/21/14 17: Bromomethane ND ug/kg /20/14 07:40 06/21/14 17: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 17: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 17: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: Chloroethane ND ug/kg /20/14 07:40 06/21/14 17: Chloroform ND ug/kg /20/14 07:40 06/21/14 17: Chloromethane ND ug/kg /20/14 07:40 06/21/14 17: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 17: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 17: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 17: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 17: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 17: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 17: Date: 07/02/ :09 PM without the written consent of. Page 24 of 67

32 Sample: Lab ID: Collected: 06/19/14 09:26 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 17: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 17: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 17: Naphthalene ND ug/kg /20/14 07:40 06/21/14 17: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Styrene ND ug/kg /20/14 07:40 06/21/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 17: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 17: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 17: Toluene ND ug/kg /20/14 07:40 06/21/14 17: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 17: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 17: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 17: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 17: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /20/14 07:40 06/21/14 17: Toluene-d8 (S) 90 % /20/14 07:40 06/21/14 17: Bromofluorobenzene (S) 130 % /20/14 07:40 06/21/14 17: Date: 07/02/ :09 PM without the written consent of. Page 25 of 67

33 Sample: Lab ID: Collected: 06/19/14 09:28 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 11.8 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 17: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 17: Benzene ND ug/kg /20/14 07:40 06/21/14 17: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 17: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 17: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 17: Bromoform ND ug/kg /20/14 07:40 06/21/14 17: Bromomethane ND ug/kg /20/14 07:40 06/21/14 17: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 17: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 17: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: Chloroethane ND ug/kg /20/14 07:40 06/21/14 17: Chloroform ND ug/kg /20/14 07:40 06/21/14 17: Chloromethane ND ug/kg /20/14 07:40 06/21/14 17: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 17: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 17: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 17: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 17: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 17: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 17: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 17: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 17: Date: 07/02/ :09 PM without the written consent of. Page 26 of 67

34 Sample: Lab ID: Collected: 06/19/14 09:28 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 17: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 17: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 17: Naphthalene ND ug/kg /20/14 07:40 06/21/14 17: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Styrene ND ug/kg /20/14 07:40 06/21/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 17: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 17: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 17: Toluene ND ug/kg /20/14 07:40 06/21/14 17: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 17: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 17: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 17: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 17: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 17: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 17: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 17: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 107 % /20/14 07:40 06/21/14 17: Toluene-d8 (S) 103 % /20/14 07:40 06/21/14 17: Bromofluorobenzene (S) 111 % /20/14 07:40 06/21/14 17: Date: 07/02/ :09 PM without the written consent of. Page 27 of 67

35 Sample: DUP-1 Lab ID: Collected: 06/19/14 00:00 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 8.2 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 18: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 18: Benzene ND ug/kg /20/14 07:40 06/21/14 18: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 18: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 18: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 18: Bromoform ND ug/kg /20/14 07:40 06/21/14 18: Bromomethane ND ug/kg /20/14 07:40 06/21/14 18: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 18: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 18: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: Chloroethane ND ug/kg /20/14 07:40 06/21/14 18: Chloroform ND ug/kg /20/14 07:40 06/21/14 18: Chloromethane ND ug/kg /20/14 07:40 06/21/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 18: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 18: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 18: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 18: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 18: Date: 07/02/ :09 PM without the written consent of. Page 28 of 67

36 Sample: DUP-1 Lab ID: Collected: 06/19/14 00:00 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 18: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 18: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 18: Naphthalene ND ug/kg /20/14 07:40 06/21/14 18: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Styrene ND ug/kg /20/14 07:40 06/21/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 18: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 18: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 18: Toluene ND ug/kg /20/14 07:40 06/21/14 18: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 18: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 18: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 18: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 18: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 106 % /20/14 07:40 06/21/14 18: Toluene-d8 (S) 103 % /20/14 07:40 06/21/14 18: Bromofluorobenzene (S) 106 % /20/14 07:40 06/21/14 18: Date: 07/02/ :09 PM without the written consent of. Page 29 of 67

37 Sample: Lab ID: Collected: 06/19/14 09:30 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 15.1 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 18: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 18: Benzene ND ug/kg /20/14 07:40 06/21/14 18: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 18: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 18: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 18: Bromoform ND ug/kg /20/14 07:40 06/21/14 18: Bromomethane ND ug/kg /20/14 07:40 06/21/14 18: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 18: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 18: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: Chloroethane ND ug/kg /20/14 07:40 06/21/14 18: Chloroform ND ug/kg /20/14 07:40 06/21/14 18: Chloromethane ND ug/kg /20/14 07:40 06/21/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 18: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 18: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 18: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 18: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 18: Date: 07/02/ :09 PM without the written consent of. Page 30 of 67

38 Sample: Lab ID: Collected: 06/19/14 09:30 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 18: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 18: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 18: Naphthalene ND ug/kg /20/14 07:40 06/21/14 18: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Styrene ND ug/kg /20/14 07:40 06/21/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 18: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 18: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 18: Toluene ND ug/kg /20/14 07:40 06/21/14 18: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 18: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 18: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 18: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 18: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /20/14 07:40 06/21/14 18: Toluene-d8 (S) 103 % /20/14 07:40 06/21/14 18: Bromofluorobenzene (S) 92 % /20/14 07:40 06/21/14 18: Date: 07/02/ :09 PM without the written consent of. Page 31 of 67

39 Sample: Lab ID: Collected: 06/19/14 09:32 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 17.7 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 18: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 18: Benzene ND ug/kg /20/14 07:40 06/21/14 18: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 18: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 18: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 18: Bromoform ND ug/kg /20/14 07:40 06/21/14 18: Bromomethane ND ug/kg /20/14 07:40 06/21/14 18: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 18: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 18: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: Chloroethane ND ug/kg /20/14 07:40 06/21/14 18: Chloroform ND ug/kg /20/14 07:40 06/21/14 18: Chloromethane ND ug/kg /20/14 07:40 06/21/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 18: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 18: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 18: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 18: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 18: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 18: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 18: Date: 07/02/ :09 PM without the written consent of. Page 32 of 67

40 Sample: Lab ID: Collected: 06/19/14 09:32 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 18: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 18: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 18: Naphthalene ND ug/kg /20/14 07:40 06/21/14 18: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Styrene ND ug/kg /20/14 07:40 06/21/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 18: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 18: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 18: Toluene ND ug/kg /20/14 07:40 06/21/14 18: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 18: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 18: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 18: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 18: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 18: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 18: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 18: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 105 % /20/14 07:40 06/21/14 18: Toluene-d8 (S) 103 % /20/14 07:40 06/21/14 18: Bromofluorobenzene (S) 105 % /20/14 07:40 06/21/14 18: Date: 07/02/ :09 PM without the written consent of. Page 33 of 67

41 Sample: Lab ID: Collected: 06/19/14 09:34 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 16.4 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 19: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Benzene ND ug/kg /20/14 07:40 06/21/14 19: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 19: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromoform ND ug/kg /20/14 07:40 06/21/14 19: Bromomethane ND ug/kg /20/14 07:40 06/21/14 19: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 19: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 19: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Chloroethane ND ug/kg /20/14 07:40 06/21/14 19: Chloroform ND ug/kg /20/14 07:40 06/21/14 19: Chloromethane ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 19: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 19: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 19: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 19: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 34 of 67

42 Sample: Lab ID: Collected: 06/19/14 09:34 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 19: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 19: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 19: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 19: Naphthalene ND ug/kg /20/14 07:40 06/21/14 19: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Styrene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 19: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 19: Toluene ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: Trichloroethene 10.4 ug/kg /20/14 07:40 06/21/14 19: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 19: Surrogates 1,2-Dichloroethane-d4 (S) 108 % /20/14 07:40 06/21/14 19: Toluene-d8 (S) 100 % /20/14 07:40 06/21/14 19: Bromofluorobenzene (S) 114 % /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 35 of 67

43 Sample: Lab ID: Collected: 06/19/14 09:36 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 17.7 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 19: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Benzene ND ug/kg /20/14 07:40 06/21/14 19: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 19: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromoform ND ug/kg /20/14 07:40 06/21/14 19: Bromomethane ND ug/kg /20/14 07:40 06/21/14 19: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 19: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 19: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Chloroethane ND ug/kg /20/14 07:40 06/21/14 19: Chloroform ND ug/kg /20/14 07:40 06/21/14 19: Chloromethane ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 19: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 19: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 19: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 19: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 36 of 67

44 Sample: Lab ID: Collected: 06/19/14 09:36 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 19: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 19: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 19: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 19: Naphthalene ND ug/kg /20/14 07:40 06/21/14 19: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Styrene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 19: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 19: Toluene ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 19: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 19: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /20/14 07:40 06/21/14 19: Toluene-d8 (S) 103 % /20/14 07:40 06/21/14 19: Bromofluorobenzene (S) 117 % /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 37 of 67

45 Sample: Lab ID: Collected: 06/19/14 09:38 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 16.5 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 19: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Benzene ND ug/kg /20/14 07:40 06/21/14 19: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 19: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromoform ND ug/kg /20/14 07:40 06/21/14 19: Bromomethane ND ug/kg /20/14 07:40 06/21/14 19: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 19: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 19: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Chloroethane ND ug/kg /20/14 07:40 06/21/14 19: Chloroform ND ug/kg /20/14 07:40 06/21/14 19: Chloromethane ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 19: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 19: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 19: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 19: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 38 of 67

46 Sample: Lab ID: Collected: 06/19/14 09:38 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 19: Methylene Chloride 38.6 ug/kg /20/14 07:40 06/21/14 19: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 19: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 19: Naphthalene ND ug/kg /20/14 07:40 06/21/14 19: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Styrene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 19: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 19: Toluene ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 19: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 19: Surrogates 1,2-Dichloroethane-d4 (S) 111 % /20/14 07:40 06/21/14 19: Toluene-d8 (S) 111 % /20/14 07:40 06/21/14 19: Bromofluorobenzene (S) 110 % /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 39 of 67

47 Sample: Lab ID: Collected: 06/19/14 09:40 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 11.1 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/21/14 19: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Benzene ND ug/kg /20/14 07:40 06/21/14 19: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 19: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 19: Bromoform ND ug/kg /20/14 07:40 06/21/14 19: Bromomethane ND ug/kg /20/14 07:40 06/21/14 19: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 19: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 19: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Chloroethane ND ug/kg /20/14 07:40 06/21/14 19: Chloroform ND ug/kg /20/14 07:40 06/21/14 19: Chloromethane ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 19: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 19: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 19: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 19: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 19: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 19: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 40 of 67

48 Sample: Lab ID: Collected: 06/19/14 09:40 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 19: Methylene Chloride 25.9 ug/kg /20/14 07:40 06/21/14 19: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 19: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 19: Naphthalene ND ug/kg /20/14 07:40 06/21/14 19: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Styrene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 19: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 19: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 19: Toluene ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 19: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 19: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 19: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 19: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 19: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 19: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 19: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 19: Surrogates 1,2-Dichloroethane-d4 (S) 111 % /20/14 07:40 06/21/14 19: Toluene-d8 (S) 98 % /20/14 07:40 06/21/14 19: Bromofluorobenzene (S) 104 % /20/14 07:40 06/21/14 19: Date: 07/02/ :09 PM without the written consent of. Page 41 of 67

49 Sample: Lab ID: Collected: 06/19/14 09:42 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 14.3 % /20/14 00:00 Acetone 30.6 ug/kg /20/14 07:40 06/21/14 20: Allyl chloride ND ug/kg /20/14 07:40 06/21/14 20: Benzene ND ug/kg /20/14 07:40 06/21/14 20: Bromobenzene ND ug/kg /20/14 07:40 06/21/14 20: Bromochloromethane ND ug/kg /20/14 07:40 06/21/14 20: Bromodichloromethane ND ug/kg /20/14 07:40 06/21/14 20: Bromoform ND ug/kg /20/14 07:40 06/21/14 20: Bromomethane ND ug/kg /20/14 07:40 06/21/14 20: Butanone (MEK) ND ug/kg /20/14 07:40 06/21/14 20: n-butylbenzene ND ug/kg /20/14 07:40 06/21/14 20: sec-butylbenzene ND ug/kg /20/14 07:40 06/21/14 20: tert-butylbenzene ND ug/kg /20/14 07:40 06/21/14 20: Carbon tetrachloride ND ug/kg /20/14 07:40 06/21/14 20: Chlorobenzene ND ug/kg /20/14 07:40 06/21/14 20: Chloroethane ND ug/kg /20/14 07:40 06/21/14 20: Chloroform ND ug/kg /20/14 07:40 06/21/14 20: Chloromethane ND ug/kg /20/14 07:40 06/21/14 20: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 20: Chlorotoluene ND ug/kg /20/14 07:40 06/21/14 20: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/21/14 20: Dibromochloromethane ND ug/kg /20/14 07:40 06/21/14 20: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/21/14 20: Dibromomethane ND ug/kg /20/14 07:40 06/21/14 20: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 20: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 20: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/21/14 20: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/21/14 20: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 20: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/21/14 20: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/21/14 20: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 20: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/21/14 20: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 20: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 20: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 20: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/21/14 20: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/21/14 20: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 20: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/21/14 20: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/21/14 20: Ethylbenzene ND ug/kg /20/14 07:40 06/21/14 20: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/21/14 20: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/21/14 20: Date: 07/02/ :09 PM without the written consent of. Page 42 of 67

50 Sample: Lab ID: Collected: 06/19/14 09:42 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/21/14 20: Methylene Chloride ND ug/kg /20/14 07:40 06/21/14 20: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/21/14 20: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/21/14 20: Naphthalene ND ug/kg /20/14 07:40 06/21/14 20: n-propylbenzene ND ug/kg /20/14 07:40 06/21/14 20: Styrene ND ug/kg /20/14 07:40 06/21/14 20: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 20: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/21/14 20: Tetrachloroethene ND ug/kg /20/14 07:40 06/21/14 20: Tetrahydrofuran ND ug/kg /20/14 07:40 06/21/14 20: Toluene ND ug/kg /20/14 07:40 06/21/14 20: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 20: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/21/14 20: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 20: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/21/14 20: Trichloroethene ND ug/kg /20/14 07:40 06/21/14 20: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/21/14 20: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/21/14 20: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/21/14 20: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 20: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/21/14 20: Vinyl chloride ND ug/kg /20/14 07:40 06/21/14 20: Xylene (Total) ND ug/kg /20/14 07:40 06/21/14 20: Surrogates 1,2-Dichloroethane-d4 (S) 112 % /20/14 07:40 06/21/14 20: Toluene-d8 (S) 90 % /20/14 07:40 06/21/14 20: Bromofluorobenzene (S) 120 % /20/14 07:40 06/21/14 20: Date: 07/02/ :09 PM without the written consent of. Page 43 of 67

51 Sample: Lab ID: Collected: 06/19/14 09:44 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 14.1 % /20/14 00:00 Acetone ND ug/kg /20/14 07:39 06/21/14 20: Allyl chloride ND ug/kg /20/14 07:39 06/21/14 20: Benzene ND ug/kg /20/14 07:39 06/21/14 20: Bromobenzene ND ug/kg /20/14 07:39 06/21/14 20: Bromochloromethane ND ug/kg /20/14 07:39 06/21/14 20: Bromodichloromethane ND ug/kg /20/14 07:39 06/21/14 20: Bromoform ND ug/kg /20/14 07:39 06/21/14 20: Bromomethane ND ug/kg /20/14 07:39 06/21/14 20: Butanone (MEK) ND ug/kg /20/14 07:39 06/21/14 20: n-butylbenzene ND ug/kg /20/14 07:39 06/21/14 20: sec-butylbenzene ND ug/kg /20/14 07:39 06/21/14 20: tert-butylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Carbon tetrachloride ND ug/kg /20/14 07:39 06/21/14 20: Chlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: Chloroethane ND ug/kg /20/14 07:39 06/21/14 20: Chloroform ND ug/kg /20/14 07:39 06/21/14 20: Chloromethane ND ug/kg /20/14 07:39 06/21/14 20: Chlorotoluene ND ug/kg /20/14 07:39 06/21/14 20: Chlorotoluene ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:39 06/21/14 20: Dibromochloromethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:39 06/21/14 20: Dibromomethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,3-Dichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,4-Dichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: Dichlorodifluoromethane ND ug/kg /20/14 07:39 06/21/14 20: ,1-Dichloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,1-Dichloroethene ND ug/kg /20/14 07:39 06/21/14 20: cis-1,2-dichloroethene ND ug/kg /20/14 07:39 06/21/14 20: trans-1,2-dichloroethene ND ug/kg /20/14 07:39 06/21/14 20: Dichlorofluoromethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,3-Dichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,1-Dichloropropene ND ug/kg /20/14 07:39 06/21/14 20: cis-1,3-dichloropropene ND ug/kg /20/14 07:39 06/21/14 20: trans-1,3-dichloropropene ND ug/kg /20/14 07:39 06/21/14 20: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:39 06/21/14 20: Ethylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:39 06/21/14 20: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:39 06/21/14 20: Date: 07/02/ :09 PM without the written consent of. Page 44 of 67

52 Sample: Lab ID: Collected: 06/19/14 09:44 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:39 06/21/14 20: Methylene Chloride ND ug/kg /20/14 07:39 06/21/14 20: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:39 06/21/14 20: Methyl-tert-butyl ether ND ug/kg /20/14 07:39 06/21/14 20: Naphthalene ND ug/kg /20/14 07:39 06/21/14 20: n-propylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Styrene ND ug/kg /20/14 07:39 06/21/14 20: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:39 06/21/14 20: Tetrachloroethene ND ug/kg /20/14 07:39 06/21/14 20: Tetrahydrofuran ND ug/kg /20/14 07:39 06/21/14 20: Toluene ND ug/kg /20/14 07:39 06/21/14 20: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,1,1-Trichloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,1,2-Trichloroethane ND ug/kg /20/14 07:39 06/21/14 20: Trichloroethene ND ug/kg /20/14 07:39 06/21/14 20: Trichlorofluoromethane ND ug/kg /20/14 07:39 06/21/14 20: ,2,3-Trichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:39 06/21/14 20: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:39 06/21/14 20: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Vinyl chloride ND ug/kg /20/14 07:39 06/21/14 20: Xylene (Total) ND ug/kg /20/14 07:39 06/21/14 20: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /20/14 07:39 06/21/14 20: Toluene-d8 (S) 106 % /20/14 07:39 06/21/14 20: Bromofluorobenzene (S) 112 % /20/14 07:39 06/21/14 20: Date: 07/02/ :09 PM without the written consent of. Page 45 of 67

53 Sample: Lab ID: Collected: 06/19/14 09:46 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 14.0 % /20/14 00:00 Acetone ND ug/kg /20/14 07:39 06/21/14 20: IS Allyl chloride ND ug/kg /20/14 07:39 06/21/14 20: Benzene ND ug/kg /20/14 07:39 06/21/14 20: Bromobenzene ND ug/kg /20/14 07:39 06/21/14 20: Bromochloromethane ND ug/kg /20/14 07:39 06/21/14 20: Bromodichloromethane ND ug/kg /20/14 07:39 06/21/14 20: Bromoform ND ug/kg /20/14 07:39 06/21/14 20: Bromomethane ND ug/kg /20/14 07:39 06/21/14 20: M1 2-Butanone (MEK) ND ug/kg /20/14 07:39 06/21/14 20: n-butylbenzene ND ug/kg /20/14 07:39 06/21/14 20: sec-butylbenzene ND ug/kg /20/14 07:39 06/21/14 20: tert-butylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Carbon tetrachloride ND ug/kg /20/14 07:39 06/21/14 20: Chlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: Chloroethane ND ug/kg /20/14 07:39 06/21/14 20: Chloroform ND ug/kg /20/14 07:39 06/21/14 20: Chloromethane ND ug/kg /20/14 07:39 06/21/14 20: Chlorotoluene ND ug/kg /20/14 07:39 06/21/14 20: Chlorotoluene ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:39 06/21/14 20: Dibromochloromethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:39 06/21/14 20: Dibromomethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,3-Dichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,4-Dichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: Dichlorodifluoromethane ND ug/kg /20/14 07:39 06/21/14 20: ,1-Dichloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,1-Dichloroethene ND ug/kg /20/14 07:39 06/21/14 20: cis-1,2-dichloroethene ND ug/kg /20/14 07:39 06/21/14 20: trans-1,2-dichloroethene ND ug/kg /20/14 07:39 06/21/14 20: Dichlorofluoromethane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,3-Dichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,2-Dichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,1-Dichloropropene ND ug/kg /20/14 07:39 06/21/14 20: cis-1,3-dichloropropene ND ug/kg /20/14 07:39 06/21/14 20: trans-1,3-dichloropropene ND ug/kg /20/14 07:39 06/21/14 20: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:39 06/21/14 20: Ethylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:39 06/21/14 20: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:39 06/21/14 20: Date: 07/02/ :09 PM without the written consent of. Page 46 of 67

54 Sample: Lab ID: Collected: 06/19/14 09:46 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:39 06/21/14 20: Methylene Chloride ND ug/kg /20/14 07:39 06/21/14 20: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:39 06/21/14 20: Methyl-tert-butyl ether ND ug/kg /20/14 07:39 06/21/14 20: Naphthalene ND ug/kg /20/14 07:39 06/21/14 20: n-propylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Styrene ND ug/kg /20/14 07:39 06/21/14 20: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:39 06/21/14 20: Tetrachloroethene ND ug/kg /20/14 07:39 06/21/14 20: Tetrahydrofuran ND ug/kg /20/14 07:39 06/21/14 20: IS Toluene ND ug/kg /20/14 07:39 06/21/14 20: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:39 06/21/14 20: ,1,1-Trichloroethane ND ug/kg /20/14 07:39 06/21/14 20: ,1,2-Trichloroethane ND ug/kg /20/14 07:39 06/21/14 20: Trichloroethene ND ug/kg /20/14 07:39 06/21/14 20: Trichlorofluoromethane ND ug/kg /20/14 07:39 06/21/14 20: ,2,3-Trichloropropane ND ug/kg /20/14 07:39 06/21/14 20: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:39 06/21/14 20: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:39 06/21/14 20: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:39 06/21/14 20: Vinyl chloride ND ug/kg /20/14 07:39 06/21/14 20: Xylene (Total) ND ug/kg /20/14 07:39 06/21/14 20: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /20/14 07:39 06/21/14 20: Toluene-d8 (S) 103 % /20/14 07:39 06/21/14 20: Bromofluorobenzene (S) 111 % /20/14 07:39 06/21/14 20: Date: 07/02/ :09 PM without the written consent of. Page 47 of 67

55 Sample: DUP-4 Lab ID: Collected: 06/19/14 00:00 Received: 06/19/14 10:27 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 14.4 % /20/14 00:00 Acetone ND ug/kg /20/14 07:40 06/27/14 18: Allyl chloride ND ug/kg /20/14 07:40 06/27/14 18: Benzene ND ug/kg /20/14 07:40 06/27/14 18: Bromobenzene ND ug/kg /20/14 07:40 06/27/14 18: Bromochloromethane ND ug/kg /20/14 07:40 06/27/14 18: Bromodichloromethane ND ug/kg /20/14 07:40 06/27/14 18: Bromoform ND ug/kg /20/14 07:40 06/27/14 18: Bromomethane ND ug/kg /20/14 07:40 06/27/14 18: Butanone (MEK) ND ug/kg /20/14 07:40 06/27/14 18: n-butylbenzene ND ug/kg /20/14 07:40 06/27/14 18: sec-butylbenzene ND ug/kg /20/14 07:40 06/27/14 18: tert-butylbenzene ND ug/kg /20/14 07:40 06/27/14 18: Carbon tetrachloride ND ug/kg /20/14 07:40 06/27/14 18: Chlorobenzene ND ug/kg /20/14 07:40 06/27/14 18: Chloroethane ND ug/kg /20/14 07:40 06/27/14 18: Chloroform ND ug/kg /20/14 07:40 06/27/14 18: Chloromethane ND ug/kg /20/14 07:40 06/27/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/27/14 18: Chlorotoluene ND ug/kg /20/14 07:40 06/27/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /20/14 07:40 06/27/14 18: Dibromochloromethane ND ug/kg /20/14 07:40 06/27/14 18: ,2-Dibromoethane (EDB) ND ug/kg /20/14 07:40 06/27/14 18: Dibromomethane ND ug/kg /20/14 07:40 06/27/14 18: ,2-Dichlorobenzene ND ug/kg /20/14 07:40 06/27/14 18: ,3-Dichlorobenzene ND ug/kg /20/14 07:40 06/27/14 18: ,4-Dichlorobenzene ND ug/kg /20/14 07:40 06/27/14 18: Dichlorodifluoromethane ND ug/kg /20/14 07:40 06/27/14 18: ,1-Dichloroethane ND ug/kg /20/14 07:40 06/27/14 18: ,2-Dichloroethane ND ug/kg /20/14 07:40 06/27/14 18: ,1-Dichloroethene ND ug/kg /20/14 07:40 06/27/14 18: cis-1,2-dichloroethene ND ug/kg /20/14 07:40 06/27/14 18: trans-1,2-dichloroethene ND ug/kg /20/14 07:40 06/27/14 18: Dichlorofluoromethane ND ug/kg /20/14 07:40 06/27/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/27/14 18: ,3-Dichloropropane ND ug/kg /20/14 07:40 06/27/14 18: ,2-Dichloropropane ND ug/kg /20/14 07:40 06/27/14 18: ,1-Dichloropropene ND ug/kg /20/14 07:40 06/27/14 18: cis-1,3-dichloropropene ND ug/kg /20/14 07:40 06/27/14 18: trans-1,3-dichloropropene ND ug/kg /20/14 07:40 06/27/14 18: Diethyl ether (Ethyl ether) ND ug/kg /20/14 07:40 06/27/14 18: Ethylbenzene ND ug/kg /20/14 07:40 06/27/14 18: Hexachloro-1,3-butadiene ND ug/kg /20/14 07:40 06/27/14 18: Isopropylbenzene (Cumene) ND ug/kg /20/14 07:40 06/27/14 18: Date: 07/02/ :09 PM without the written consent of. Page 48 of 67

56 Sample: DUP-4 Lab ID: Collected: 06/19/14 00:00 Received: 06/19/14 10:27 Matrix: Solid p-isopropyltoluene ND ug/kg /20/14 07:40 06/27/14 18: Methylene Chloride ND ug/kg /20/14 07:40 06/27/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /20/14 07:40 06/27/14 18: Methyl-tert-butyl ether ND ug/kg /20/14 07:40 06/27/14 18: Naphthalene ND ug/kg /20/14 07:40 06/27/14 18: n-propylbenzene ND ug/kg /20/14 07:40 06/27/14 18: Styrene ND ug/kg /20/14 07:40 06/27/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/27/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /20/14 07:40 06/27/14 18: Tetrachloroethene ND ug/kg /20/14 07:40 06/27/14 18: Tetrahydrofuran ND ug/kg /20/14 07:40 06/27/14 18: Toluene ND ug/kg /20/14 07:40 06/27/14 18: ,2,3-Trichlorobenzene ND ug/kg /20/14 07:40 06/27/14 18: ,2,4-Trichlorobenzene ND ug/kg /20/14 07:40 06/27/14 18: ,1,1-Trichloroethane ND ug/kg /20/14 07:40 06/27/14 18: ,1,2-Trichloroethane ND ug/kg /20/14 07:40 06/27/14 18: Trichloroethene ND ug/kg /20/14 07:40 06/27/14 18: Trichlorofluoromethane ND ug/kg /20/14 07:40 06/27/14 18: ,2,3-Trichloropropane ND ug/kg /20/14 07:40 06/27/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /20/14 07:40 06/27/14 18: ,2,4-Trimethylbenzene ND ug/kg /20/14 07:40 06/27/14 18: ,3,5-Trimethylbenzene ND ug/kg /20/14 07:40 06/27/14 18: Vinyl chloride ND ug/kg /20/14 07:40 06/27/14 18: Xylene (Total) ND ug/kg /20/14 07:40 06/27/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /20/14 07:40 06/27/14 18: Toluene-d8 (S) 103 % /20/14 07:40 06/27/14 18: Bromofluorobenzene (S) 104 % /20/14 07:40 06/27/14 18: Date: 07/02/ :09 PM without the written consent of. Page 49 of 67

57 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MPRP/46774 ASTM D2974 Analysis Method: Analysis Description: ASTM D2974 Dry Weight/Percent Moisture Associated Lab Samples: , , , , , , , , , , , , , , , , , , SAMPLE DUPLICATE: Parameter Units Result Dup Result Percent Moisture % RPD Max RPD Qualifiers SAMPLE DUPLICATE: Parameter Units Result Dup Result Percent Moisture % RPD Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 50 of 67

58 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MPRP/46775 ASTM D2974 Associated Lab Samples: , Analysis Method: Analysis Description: ASTM D2974 Dry Weight/Percent Moisture SAMPLE DUPLICATE: Parameter Units Result Dup Result Percent Moisture % RPD Max RPD Qualifiers SAMPLE DUPLICATE: Parameter Units Result Dup Result Percent Moisture % RPD Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 51 of 67

59 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MSV/27518 EPA 8260 Analysis Method: Analysis Description: EPA 8260 Associated Lab Samples: , , , , , , , , , , , , , , , , , , , METHOD BLANK: Matrix: Solid Associated Lab Samples: , , , , , , , , , , , , , , , , , , , Parameter Units Blank Result Reporting Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND /21/14 14:46 1,1,1-Trichloroethane ug/kg ND /21/14 14:46 1,1,2,2-Tetrachloroethane ug/kg ND /21/14 14:46 1,1,2-Trichloroethane ug/kg ND /21/14 14:46 1,1,2-Trichlorotrifluoroethane ug/kg ND /21/14 14:46 1,1-Dichloroethane ug/kg ND /21/14 14:46 1,1-Dichloroethene ug/kg ND /21/14 14:46 1,1-Dichloropropene ug/kg ND /21/14 14:46 1,2,3-Trichlorobenzene ug/kg ND /21/14 14:46 1,2,3-Trichloropropane ug/kg ND /21/14 14:46 1,2,4-Trichlorobenzene ug/kg ND /21/14 14:46 1,2,4-Trimethylbenzene ug/kg ND /21/14 14:46 1,2-Dibromo-3-chloropropane ug/kg ND /21/14 14:46 1,2-Dibromoethane (EDB) ug/kg ND /21/14 14:46 1,2-Dichlorobenzene ug/kg ND /21/14 14:46 1,2-Dichloroethane ug/kg ND /21/14 14:46 1,2-Dichloropropane ug/kg ND /21/14 14:46 1,3,5-Trimethylbenzene ug/kg ND /21/14 14:46 1,3-Dichlorobenzene ug/kg ND /21/14 14:46 1,3-Dichloropropane ug/kg ND /21/14 14:46 1,4-Dichlorobenzene ug/kg ND /21/14 14:46 2,2-Dichloropropane ug/kg ND /21/14 14:46 2-Butanone (MEK) ug/kg ND /21/14 14:46 2-Chlorotoluene ug/kg ND /21/14 14:46 4-Chlorotoluene ug/kg ND /21/14 14:46 4-Methyl-2-pentanone (MIBK) ug/kg ND /21/14 14:46 Acetone ug/kg ND /21/14 14:46 Allyl chloride ug/kg ND /21/14 14:46 Benzene ug/kg ND /21/14 14:46 Bromobenzene ug/kg ND /21/14 14:46 Bromochloromethane ug/kg ND /21/14 14:46 Bromodichloromethane ug/kg ND /21/14 14:46 Bromoform ug/kg ND /21/14 14:46 Bromomethane ug/kg ND /21/14 14:46 Carbon tetrachloride ug/kg ND /21/14 14:46 Chlorobenzene ug/kg ND /21/14 14:46 Chloroethane ug/kg ND /21/14 14:46 Chloroform ug/kg ND /21/14 14:46 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 52 of 67

60 #=QC# QUALITY CONTROL DATA METHOD BLANK: Matrix: Solid Associated Lab Samples: , , , , , , , , , , , , , , , , , , , Parameter Units Blank Result Reporting Limit Analyzed Qualifiers Chloromethane ug/kg ND /21/14 14:46 cis-1,2-dichloroethene ug/kg ND /21/14 14:46 cis-1,3-dichloropropene ug/kg ND /21/14 14:46 Dibromochloromethane ug/kg ND /21/14 14:46 Dibromomethane ug/kg ND /21/14 14:46 Dichlorodifluoromethane ug/kg ND /21/14 14:46 Dichlorofluoromethane ug/kg ND /21/14 14:46 Diethyl ether (Ethyl ether) ug/kg ND /21/14 14:46 Ethylbenzene ug/kg ND /21/14 14:46 Hexachloro-1,3-butadiene ug/kg ND /21/14 14:46 Isopropylbenzene (Cumene) ug/kg ND /21/14 14:46 Methyl-tert-butyl ether ug/kg ND /21/14 14:46 Methylene Chloride ug/kg ND /21/14 14:46 n-butylbenzene ug/kg ND /21/14 14:46 n-propylbenzene ug/kg ND /21/14 14:46 Naphthalene ug/kg ND /21/14 14:46 p-isopropyltoluene ug/kg ND /21/14 14:46 sec-butylbenzene ug/kg ND /21/14 14:46 Styrene ug/kg ND /21/14 14:46 tert-butylbenzene ug/kg ND /21/14 14:46 Tetrachloroethene ug/kg ND /21/14 14:46 Tetrahydrofuran ug/kg ND /21/14 14:46 Toluene ug/kg ND /21/14 14:46 trans-1,2-dichloroethene ug/kg ND /21/14 14:46 trans-1,3-dichloropropene ug/kg ND /21/14 14:46 Trichloroethene ug/kg ND /21/14 14:46 Trichlorofluoromethane ug/kg ND /21/14 14:46 Vinyl chloride ug/kg ND /21/14 14:46 Xylene (Total) ug/kg ND /21/14 14:46 1,2-Dichloroethane-d4 (S) % /21/14 14:46 4-Bromofluorobenzene (S) % /21/14 14:46 Toluene-d8 (S) % /21/14 14:46 LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/kg ,1,1-Trichloroethane ug/kg ,1,2,2-Tetrachloroethane ug/kg ,1,2-Trichloroethane ug/kg ,1,2-Trichlorotrifluoroethane ug/kg ,1-Dichloroethane ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 53 of 67

61 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1-Dichloroethene ug/kg ,1-Dichloropropene ug/kg ,2,3-Trichlorobenzene ug/kg ,2,3-Trichloropropane ug/kg ,2,4-Trichlorobenzene ug/kg ,2,4-Trimethylbenzene ug/kg ,2-Dibromo-3-chloropropane ug/kg ,2-Dibromoethane (EDB) ug/kg ,2-Dichlorobenzene ug/kg ,2-Dichloroethane ug/kg ,2-Dichloropropane ug/kg ,3,5-Trimethylbenzene ug/kg ,3-Dichlorobenzene ug/kg ,3-Dichloropropane ug/kg ,4-Dichlorobenzene ug/kg ,2-Dichloropropane ug/kg Butanone (MEK) ug/kg Chlorotoluene ug/kg Chlorotoluene ug/kg Methyl-2-pentanone (MIBK) ug/kg Acetone ug/kg Allyl chloride ug/kg Benzene ug/kg Bromobenzene ug/kg Bromochloromethane ug/kg Bromodichloromethane ug/kg Bromoform ug/kg Bromomethane ug/kg Carbon tetrachloride ug/kg Chlorobenzene ug/kg Chloroethane ug/kg Chloroform ug/kg Chloromethane ug/kg cis-1,2-dichloroethene ug/kg cis-1,3-dichloropropene ug/kg Dibromochloromethane ug/kg Dibromomethane ug/kg Dichlorodifluoromethane ug/kg Dichlorofluoromethane ug/kg Diethyl ether (Ethyl ether) ug/kg Ethylbenzene ug/kg Hexachloro-1,3-butadiene ug/kg Isopropylbenzene (Cumene) ug/kg Methyl-tert-butyl ether ug/kg Methylene Chloride ug/kg n-butylbenzene ug/kg n-propylbenzene ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 54 of 67

62 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Naphthalene ug/kg p-isopropyltoluene ug/kg sec-butylbenzene ug/kg Styrene ug/kg tert-butylbenzene ug/kg Tetrachloroethene ug/kg Tetrahydrofuran ug/kg Toluene ug/kg trans-1,2-dichloroethene ug/kg trans-1,3-dichloropropene ug/kg Trichloroethene ug/kg Trichlorofluoromethane ug/kg Vinyl chloride ug/kg Xylene (Total) ug/kg ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,1,1,2-Tetrachloroethane ug/kg ND ,1,1-Trichloroethane ug/kg ND ,1,2,2-Tetrachloroethane ug/kg ND ,1,2-Trichloroethane ug/kg ND ,1,2-Trichlorotrifluoroethane ug/kg ND ,1-Dichloroethane ug/kg ND ,1-Dichloroethene ug/kg ND ,1-Dichloropropene ug/kg ND ,2,3-Trichlorobenzene ug/kg ND ,2,3-Trichloropropane ug/kg ND ,2,4-Trichlorobenzene ug/kg ND ,2,4-Trimethylbenzene ug/kg ND ,2-Dibromo-3-chloropropane ug/kg ND ,2-Dibromoethane (EDB) ug/kg ND ,2-Dichlorobenzene ug/kg ND ,2-Dichloroethane ug/kg ND ,2-Dichloropropane ug/kg ND ,3,5-Trimethylbenzene ug/kg ND ,3-Dichlorobenzene ug/kg ND ,3-Dichloropropane ug/kg ND ,4-Dichlorobenzene ug/kg ND ,2-Dichloropropane ug/kg ND Butanone (MEK) ug/kg ND Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 55 of 67

63 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD 2-Chlorotoluene ug/kg ND Chlorotoluene ug/kg ND Methyl-2-pentanone (MIBK) ug/kg ND Acetone ug/kg ND IS Allyl chloride ug/kg ND Benzene ug/kg ND Bromobenzene ug/kg ND Bromochloromethane ug/kg ND Bromodichloromethane ug/kg ND Bromoform ug/kg ND Bromomethane ug/kg ND M1 Carbon tetrachloride ug/kg ND Chlorobenzene ug/kg ND Chloroethane ug/kg ND Chloroform ug/kg ND Chloromethane ug/kg ND cis-1,2-dichloroethene ug/kg ND cis-1,3-dichloropropene ug/kg ND Dibromochloromethane ug/kg ND Dibromomethane ug/kg ND Dichlorodifluoromethane ug/kg ND Dichlorofluoromethane ug/kg ND Diethyl ether (Ethyl ether) ug/kg ND Ethylbenzene ug/kg ND Hexachloro-1,3-butadiene ug/kg ND Isopropylbenzene (Cumene) ug/kg ND Methyl-tert-butyl ether ug/kg ND Methylene Chloride ug/kg ND n-butylbenzene ug/kg ND n-propylbenzene ug/kg ND Naphthalene ug/kg ND p-isopropyltoluene ug/kg ND sec-butylbenzene ug/kg ND Styrene ug/kg ND tert-butylbenzene ug/kg ND Tetrachloroethene ug/kg ND Tetrahydrofuran ug/kg ND IS Toluene ug/kg ND trans-1,2-dichloroethene ug/kg ND trans-1,3-dichloropropene ug/kg ND Trichloroethene ug/kg ND Trichlorofluoromethane ug/kg ND Vinyl chloride ug/kg ND Xylene (Total) ug/kg ND ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Qual Date: 07/02/ :09 PM without the written consent of. Page 56 of 67

64 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Toluene-d8 (S) % Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 57 of 67

65 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MSV/27523 EPA 8260 Associated Lab Samples: Analysis Method: Analysis Description: EPA 8260 METHOD BLANK: Associated Lab Samples: Parameter Units Blank Result Matrix: Solid Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND /27/14 18:04 1,1,1-Trichloroethane ug/kg ND /27/14 18:04 1,1,2,2-Tetrachloroethane ug/kg ND /27/14 18:04 1,1,2-Trichloroethane ug/kg ND /27/14 18:04 1,1,2-Trichlorotrifluoroethane ug/kg ND /27/14 18:04 1,1-Dichloroethane ug/kg ND /27/14 18:04 1,1-Dichloroethene ug/kg ND /27/14 18:04 1,1-Dichloropropene ug/kg ND /27/14 18:04 1,2,3-Trichlorobenzene ug/kg ND /27/14 18:04 1,2,3-Trichloropropane ug/kg ND /27/14 18:04 1,2,4-Trichlorobenzene ug/kg ND /27/14 18:04 1,2,4-Trimethylbenzene ug/kg ND /27/14 18:04 1,2-Dibromo-3-chloropropane ug/kg ND /27/14 18:04 1,2-Dibromoethane (EDB) ug/kg ND /27/14 18:04 1,2-Dichlorobenzene ug/kg ND /27/14 18:04 1,2-Dichloroethane ug/kg ND /27/14 18:04 1,2-Dichloropropane ug/kg ND /27/14 18:04 1,3,5-Trimethylbenzene ug/kg ND /27/14 18:04 1,3-Dichlorobenzene ug/kg ND /27/14 18:04 1,3-Dichloropropane ug/kg ND /27/14 18:04 1,4-Dichlorobenzene ug/kg ND /27/14 18:04 2,2-Dichloropropane ug/kg ND /27/14 18:04 2-Butanone (MEK) ug/kg ND /27/14 18:04 2-Chlorotoluene ug/kg ND /27/14 18:04 4-Chlorotoluene ug/kg ND /27/14 18:04 4-Methyl-2-pentanone (MIBK) ug/kg ND /27/14 18:04 Acetone ug/kg ND /27/14 18:04 Allyl chloride ug/kg ND /27/14 18:04 Benzene ug/kg ND /27/14 18:04 Bromobenzene ug/kg ND /27/14 18:04 Bromochloromethane ug/kg ND /27/14 18:04 Bromodichloromethane ug/kg ND /27/14 18:04 Bromoform ug/kg ND /27/14 18:04 Bromomethane ug/kg ND /27/14 18:04 Carbon tetrachloride ug/kg ND /27/14 18:04 Chlorobenzene ug/kg ND /27/14 18:04 Chloroethane ug/kg ND /27/14 18:04 Chloroform ug/kg ND /27/14 18:04 Chloromethane ug/kg ND /27/14 18:04 cis-1,2-dichloroethene ug/kg ND /27/14 18:04 cis-1,3-dichloropropene ug/kg ND /27/14 18:04 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 58 of 67

66 #=QC# QUALITY CONTROL DATA METHOD BLANK: Associated Lab Samples: Parameter Units Blank Result Matrix: Solid Reporting Limit Analyzed Dibromochloromethane ug/kg ND /27/14 18:04 Dibromomethane ug/kg ND /27/14 18:04 Dichlorodifluoromethane ug/kg ND /27/14 18:04 Dichlorofluoromethane ug/kg ND /27/14 18:04 Diethyl ether (Ethyl ether) ug/kg ND /27/14 18:04 Ethylbenzene ug/kg ND /27/14 18:04 Hexachloro-1,3-butadiene ug/kg ND /27/14 18:04 Isopropylbenzene (Cumene) ug/kg ND /27/14 18:04 Methyl-tert-butyl ether ug/kg ND /27/14 18:04 Methylene Chloride ug/kg ND /27/14 18:04 n-butylbenzene ug/kg ND /27/14 18:04 n-propylbenzene ug/kg ND /27/14 18:04 Naphthalene ug/kg ND /27/14 18:04 p-isopropyltoluene ug/kg ND /27/14 18:04 sec-butylbenzene ug/kg ND /27/14 18:04 Styrene ug/kg ND /27/14 18:04 tert-butylbenzene ug/kg ND /27/14 18:04 Tetrachloroethene ug/kg ND /27/14 18:04 Tetrahydrofuran ug/kg ND /27/14 18:04 Toluene ug/kg ND /27/14 18:04 trans-1,2-dichloroethene ug/kg ND /27/14 18:04 trans-1,3-dichloropropene ug/kg ND /27/14 18:04 Trichloroethene ug/kg ND /27/14 18:04 Trichlorofluoromethane ug/kg ND /27/14 18:04 Vinyl chloride ug/kg ND /27/14 18:04 Xylene (Total) ug/kg ND /27/14 18:04 1,2-Dichloroethane-d4 (S) % /27/14 18:04 4-Bromofluorobenzene (S) % /27/14 18:04 Toluene-d8 (S) % /27/14 18:04 Qualifiers LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/kg ,1,1-Trichloroethane ug/kg ,1,2,2-Tetrachloroethane ug/kg ,1,2-Trichloroethane ug/kg ,1,2-Trichlorotrifluoroethane ug/kg ,1-Dichloroethane ug/kg ,1-Dichloroethene ug/kg ,1-Dichloropropene ug/kg ,2,3-Trichlorobenzene ug/kg ,2,3-Trichloropropane ug/kg ,2,4-Trichlorobenzene ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 59 of 67

67 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trimethylbenzene ug/kg ,2-Dibromo-3-chloropropane ug/kg ,2-Dibromoethane (EDB) ug/kg ,2-Dichlorobenzene ug/kg ,2-Dichloroethane ug/kg ,2-Dichloropropane ug/kg ,3,5-Trimethylbenzene ug/kg ,3-Dichlorobenzene ug/kg ,3-Dichloropropane ug/kg ,4-Dichlorobenzene ug/kg ,2-Dichloropropane ug/kg Butanone (MEK) ug/kg Chlorotoluene ug/kg Chlorotoluene ug/kg Methyl-2-pentanone (MIBK) ug/kg Acetone ug/kg Allyl chloride ug/kg Benzene ug/kg Bromobenzene ug/kg Bromochloromethane ug/kg Bromodichloromethane ug/kg Bromoform ug/kg Bromomethane ug/kg Carbon tetrachloride ug/kg Chlorobenzene ug/kg Chloroethane ug/kg Chloroform ug/kg Chloromethane ug/kg cis-1,2-dichloroethene ug/kg cis-1,3-dichloropropene ug/kg Dibromochloromethane ug/kg Dibromomethane ug/kg Dichlorodifluoromethane ug/kg Dichlorofluoromethane ug/kg Diethyl ether (Ethyl ether) ug/kg Ethylbenzene ug/kg Hexachloro-1,3-butadiene ug/kg Isopropylbenzene (Cumene) ug/kg Methyl-tert-butyl ether ug/kg Methylene Chloride ug/kg n-butylbenzene ug/kg n-propylbenzene ug/kg Naphthalene ug/kg p-isopropyltoluene ug/kg sec-butylbenzene ug/kg Styrene ug/kg tert-butylbenzene ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 60 of 67

68 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Tetrachloroethene ug/kg Tetrahydrofuran ug/kg Toluene ug/kg trans-1,2-dichloroethene ug/kg trans-1,3-dichloropropene ug/kg Trichloroethene ug/kg Trichlorofluoromethane ug/kg Vinyl chloride ug/kg Xylene (Total) ug/kg ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,1,1,2-Tetrachloroethane ug/kg ND ,1,1-Trichloroethane ug/kg ND ,1,2,2-Tetrachloroethane ug/kg ND ,1,2-Trichloroethane ug/kg ND ,1,2-Trichlorotrifluoroethane ug/kg ND ,1-Dichloroethane ug/kg ND ,1-Dichloroethene ug/kg ND ,1-Dichloropropene ug/kg ND ,2,3-Trichlorobenzene ug/kg ND ,2,3-Trichloropropane ug/kg ND ,2,4-Trichlorobenzene ug/kg ND ,2,4-Trimethylbenzene ug/kg ND ,2-Dibromo-3-chloropropane ug/kg ND ,2-Dibromoethane (EDB) ug/kg ND ,2-Dichlorobenzene ug/kg ND ,2-Dichloroethane ug/kg ND ,2-Dichloropropane ug/kg ND ,3,5-Trimethylbenzene ug/kg ND ,3-Dichlorobenzene ug/kg ND ,3-Dichloropropane ug/kg ND ,4-Dichlorobenzene ug/kg ND ,2-Dichloropropane ug/kg ND Butanone (MEK) ug/kg ND R1 2-Chlorotoluene ug/kg ND Chlorotoluene ug/kg ND Methyl-2-pentanone (MIBK) ug/kg ND Acetone ug/kg ND M1,R1 Allyl chloride ug/kg ND Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 61 of 67

69 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Benzene ug/kg ND Bromobenzene ug/kg ND Bromochloromethane ug/kg ND Bromodichloromethane ug/kg ND Bromoform ug/kg ND Bromomethane ug/kg ND Carbon tetrachloride ug/kg ND Chlorobenzene ug/kg ND Chloroethane ug/kg ND Chloroform ug/kg ND Chloromethane ug/kg ND cis-1,2-dichloroethene ug/kg ND cis-1,3-dichloropropene ug/kg ND Dibromochloromethane ug/kg ND Dibromomethane ug/kg ND Dichlorodifluoromethane ug/kg ND Dichlorofluoromethane ug/kg ND Diethyl ether (Ethyl ether) ug/kg ND Ethylbenzene ug/kg ND Hexachloro-1,3-butadiene ug/kg ND Isopropylbenzene (Cumene) ug/kg ND Methyl-tert-butyl ether ug/kg ND Methylene Chloride ug/kg ND n-butylbenzene ug/kg ND n-propylbenzene ug/kg ND Naphthalene ug/kg ND p-isopropyltoluene ug/kg ND sec-butylbenzene ug/kg ND Styrene ug/kg ND tert-butylbenzene ug/kg ND Tetrachloroethene ug/kg ND Tetrahydrofuran ug/kg ND Toluene ug/kg ND trans-1,2-dichloroethene ug/kg ND trans-1,3-dichloropropene ug/kg ND Trichloroethene ug/kg ND Trichlorofluoromethane ug/kg ND Vinyl chloride ug/kg ND Xylene (Total) ug/kg ND ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 07/02/ :09 PM without the written consent of. Page 62 of 67

70 #=QL# QUALIFIERS DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-M Pace Analytical Services - Minneapolis ANALYTE QUALIFIERS IS The internal standard recovery associated with this result exceeds the lower control limit. The reported result should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. Date: 07/02/ :09 PM without the written consent of. Page 63 of 67

71 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ DUP-1 ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ DUP-4 ASTM D2974 MPRP/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ DUP-1 EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ EPA 5035A MSV/27507 EPA 8260 MSV/ DUP-4 EPA 5035A MSV/27507 EPA 8260 MSV/27523 Date: 07/02/ :09 PM without the written consent of. Page 64 of 67

72 Page 65 of 67

73 Page 66 of 67

74 Page 67 of 67

75 #=CL# LIMS USE: FR - SHANE WATERMAN LIMS OBJECT ID: June 25, 2014 Shane Waterman Wenck Associates Inc 1802 Wooddale Drive Suite 100 Saint Paul, MN RE: Dear Shane Waterman: Enclosed are the analytical results for sample(s) received by the laboratory on June 16, The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Dennsa Mohamed for Kabor Xiong kabor.xiong@pacelabs.com Project Manager Enclosures cc: Matt Bowers, Wenck Associate Inc without the written consent of. Page 1 of 93

76 #=CP# CERTIFICATIONS Minnesota Certification IDs 1700 Elm Street SE Suite 200, A2LA Certification #: Alabama Certification #40770 Alabama Certification #40770 Alaska Certification #: UST-078 Alaska Certification #MN00064 Arizona Certification #: AZ-0014 Arkansas Certification #: California Certification #: 01155CA Colorado Certification #Pace Connecticut Certification #: PH-0256 EPA Region 8 Certification #: 8TMS-L Florida/NELAP Certification #: E87605 Guam Certification #: Pace Georgia Certification #: 959 Idaho Certification #: MN00064 Hawaii Certification #MN00064 Illinois Certification #: Indiana Certification#C-MN-01 Iowa Certification #: 368 Kansas Certification #: E Kentucky Dept of Envi. Protection - DW #90062 Kentucky Dept of Envi. Protection - WW #:90062 Louisiana DEQ Certification #: 3086 Louisiana DHH #: LA Maine Certification #: Maryland Certification #: 322 Michigan DEPH Certification #: 9909 Minnesota Certification #: Mississippi Certification #: Pace Montana Certification #: MT0092 Nebraska Certification #: Pace New Jersey Certification #: MN-002 New Jersey Certification #: MN-002 New York Certification #: North Carolina Certification #: 530 North Carolina State Public Health #: North Dakota Certification #: R-036 Ohio EPA #: 4150 Ohio VAP Certification #: CL101 Oklahoma Certification #: 9507 Oregon Certification #: MN Oregon Certification #: MN Pennsylvania Certification #: Puerto Rico Certification Saipan (CNMI) #:MP0003 South Carolina #: Texas Certification #: T Tennessee Certification #: Utah Certification #: MN Virginia DGS Certification #: 251 Virginia/VELAP Certification #: Pace Washington Certification #: C486 Wisconsin Certification #: West Virginia Certification #: 382 West Virginia TO-15 Approval West Virginia DHHR #:9952C without the written consent of. Page 2 of 93

77 #=SS# SAMPLE SUMMARY Lab ID Sample ID Matrix Date Collected Date Received Solid 06/16/14 14:02 06/16/14 15: Solid 06/16/14 14:25 06/16/14 15: Solid 06/16/14 14:20 06/16/14 15: Solid 06/16/14 14:15 06/16/14 15: Solid 06/16/14 13:45 06/16/14 15: Solid 06/16/14 13:40 06/16/14 15: Solid 06/16/14 13:35 06/16/14 15: Solid 06/16/14 13:56 06/16/14 15: DUP-3 Solid 06/16/14 00:00 06/16/14 15: Solid 06/16/14 13:58 06/16/14 15: Solid 06/16/14 14:00 06/16/14 15: Solid 06/16/14 13:30 06/16/14 15: Solid 06/16/14 13:25 06/16/14 15: Solid 06/16/14 14:12 06/16/14 15: Solid 06/16/14 13:20 06/16/14 15: Solid 06/16/14 13:15 06/16/14 15: Solid 06/16/14 14:10 06/16/14 15: Solid 06/16/14 14:00 06/16/14 15: Solid 06/16/14 14:06 06/16/14 15: Solid 06/16/14 14:04 06/16/14 15: Solid 06/16/14 13:10 06/16/14 15: Solid 06/16/14 13:05 06/16/14 15: Solid 06/16/14 13:00 06/16/14 15: Solid 06/16/14 12:58 06/16/14 15: Solid 06/16/14 12:54 06/16/14 15: Solid 06/16/14 12:50 06/16/14 15: MS/MSD Solid 06/16/14 12:48 06/16/14 15: DUP-5 Solid 06/16/14 00:00 06/16/14 15: MS/MSD Solid 06/16/14 13:50 06/16/14 15: DUP-2 Solid 06/16/14 00:00 06/16/14 15: Solid 06/16/14 14:30 06/16/14 15: Solid 06/16/14 13:52 06/16/14 15: Solid 06/16/14 13:54 06/16/14 15:45 without the written consent of. Page 3 of 93

78 #=SA# SAMPLE ANALYTE COUNT Lab ID Sample ID Method Analysts Analytes Reported Laboratory ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M DUP-3 ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M without the written consent of. Page 4 of 93

79 #=SA# SAMPLE ANALYTE COUNT Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M MS/MSD ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M DUP-5 ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M MS/MSD ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M DUP-2 ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M ASTM D2974 JDL 1 PASI-M EPA 8260 MJH 70 PASI-M without the written consent of. Page 5 of 93

80 #=NA# PROJECT NARRATIVE Method: EPA 8260 Description: Client: Wenck Associates, Inc. Date: June 25, 2014 General Information: 33 samples were analyzed for EPA All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 5035A with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. QC Batch: MSV/27468 L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits. LCS (Lab ID: ) Diethyl ether (Ethyl ether) QC Batch: MSV/27486 L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias. LCS (Lab ID: ) Diethyl ether (Ethyl ether) Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. without the written consent of. Page 6 of 93

81 #=NA# PROJECT NARRATIVE Method: EPA 8260 Description: Client: Wenck Associates, Inc. Date: June 25, 2014 QC Batch: MSV/27468 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 027 M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. MS (Lab ID: ) Diethyl ether (Ethyl ether) M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MS (Lab ID: ) Acetone MSD (Lab ID: ) Acetone QC Batch: MSV/27486 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 029 M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MS (Lab ID: ) Acetone Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. without the written consent of. Page 7 of 93

82 Sample: Lab ID: 001 Collected: 06/16/14 14:02 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 9.4 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 14: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 14: Benzene ND ug/kg /17/14 07:50 06/18/14 14: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 14: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 14: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 14: Bromoform ND ug/kg /17/14 07:50 06/18/14 14: Bromomethane ND ug/kg /17/14 07:50 06/18/14 14: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 14: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 14: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: Chloroethane ND ug/kg /17/14 07:50 06/18/14 14: Chloroform ND ug/kg /17/14 07:50 06/18/14 14: Chloromethane ND ug/kg /17/14 07:50 06/18/14 14: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 14: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 14: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 14: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 14: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 14: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 14: Date: 06/25/ :55 PM without the written consent of. Page 8 of 93

83 Sample: Lab ID: 001 Collected: 06/16/14 14:02 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 14: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 14: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 14: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 14: Naphthalene ND ug/kg /17/14 07:50 06/18/14 14: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Styrene ND ug/kg /17/14 07:50 06/18/14 14: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 14: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 14: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 14: Toluene ND ug/kg /17/14 07:50 06/18/14 14: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 14: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 14: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 14: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 14: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 14: Surrogates 1,2-Dichloroethane-d4 (S) 107 % /17/14 07:50 06/18/14 14: Toluene-d8 (S) 105 % /17/14 07:50 06/18/14 14: Bromofluorobenzene (S) 113 % /17/14 07:50 06/18/14 14: Date: 06/25/ :55 PM without the written consent of. Page 9 of 93

84 Sample: Lab ID: 002 Collected: 06/16/14 14:25 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.0 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 14: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 14: Benzene ND ug/kg /17/14 07:50 06/18/14 14: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 14: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 14: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 14: Bromoform ND ug/kg /17/14 07:50 06/18/14 14: Bromomethane ND ug/kg /17/14 07:50 06/18/14 14: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 14: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 14: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: Chloroethane ND ug/kg /17/14 07:50 06/18/14 14: Chloroform ND ug/kg /17/14 07:50 06/18/14 14: Chloromethane ND ug/kg /17/14 07:50 06/18/14 14: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 14: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 14: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 14: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 14: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 14: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 14: Date: 06/25/ :55 PM without the written consent of. Page 10 of 93

85 Sample: Lab ID: 002 Collected: 06/16/14 14:25 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 14: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 14: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 14: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 14: Naphthalene ND ug/kg /17/14 07:50 06/18/14 14: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Styrene ND ug/kg /17/14 07:50 06/18/14 14: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 14: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 14: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 14: Toluene ND ug/kg /17/14 07:50 06/18/14 14: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 14: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 14: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 14: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 14: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 14: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /17/14 07:50 06/18/14 14: Toluene-d8 (S) 105 % /17/14 07:50 06/18/14 14: Bromofluorobenzene (S) 112 % /17/14 07:50 06/18/14 14: Date: 06/25/ :55 PM without the written consent of. Page 11 of 93

86 Sample: Lab ID: 003 Collected: 06/16/14 14:20 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.2 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 14: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 14: Benzene ND ug/kg /17/14 07:50 06/18/14 14: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 14: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 14: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 14: Bromoform ND ug/kg /17/14 07:50 06/18/14 14: Bromomethane ND ug/kg /17/14 07:50 06/18/14 14: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 14: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 14: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: Chloroethane ND ug/kg /17/14 07:50 06/18/14 14: Chloroform ND ug/kg /17/14 07:50 06/18/14 14: Chloromethane ND ug/kg /17/14 07:50 06/18/14 14: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 14: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 14: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 14: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 14: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 14: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 14: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 14: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 14: Date: 06/25/ :55 PM without the written consent of. Page 12 of 93

87 Sample: Lab ID: 003 Collected: 06/16/14 14:20 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 14: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 14: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 14: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 14: Naphthalene ND ug/kg /17/14 07:50 06/18/14 14: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Styrene ND ug/kg /17/14 07:50 06/18/14 14: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 14: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 14: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 14: Toluene ND ug/kg /17/14 07:50 06/18/14 14: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 14: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 14: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 14: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 14: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 14: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 14: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 14: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 14: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 14: Surrogates 1,2-Dichloroethane-d4 (S) 106 % /17/14 07:50 06/18/14 14: Toluene-d8 (S) 105 % /17/14 07:50 06/18/14 14: Bromofluorobenzene (S) 98 % /17/14 07:50 06/18/14 14: Date: 06/25/ :55 PM without the written consent of. Page 13 of 93

88 Sample: Lab ID: 004 Collected: 06/16/14 14:15 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.8 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 15: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 15: Benzene ND ug/kg /17/14 07:50 06/18/14 15: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 15: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 15: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 15: Bromoform ND ug/kg /17/14 07:50 06/18/14 15: Bromomethane ND ug/kg /17/14 07:50 06/18/14 15: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 15: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 15: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: Chloroethane ND ug/kg /17/14 07:50 06/18/14 15: Chloroform ND ug/kg /17/14 07:50 06/18/14 15: Chloromethane ND ug/kg /17/14 07:50 06/18/14 15: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 15: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 15: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 15: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 15: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 15: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 15: Date: 06/25/ :55 PM without the written consent of. Page 14 of 93

89 Sample: Lab ID: 004 Collected: 06/16/14 14:15 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 15: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 15: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 15: Naphthalene ND ug/kg /17/14 07:50 06/18/14 15: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Styrene ND ug/kg /17/14 07:50 06/18/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 15: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 15: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 15: Toluene ND ug/kg /17/14 07:50 06/18/14 15: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 15: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 15: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 15: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 15: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 108 % /17/14 07:50 06/18/14 15: Toluene-d8 (S) 106 % /17/14 07:50 06/18/14 15: Bromofluorobenzene (S) 112 % /17/14 07:50 06/18/14 15: Date: 06/25/ :55 PM without the written consent of. Page 15 of 93

90 Sample: Lab ID: 005 Collected: 06/16/14 13:45 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 15.8 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 15: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 15: Benzene ND ug/kg /17/14 07:50 06/18/14 15: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 15: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 15: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 15: Bromoform ND ug/kg /17/14 07:50 06/18/14 15: Bromomethane ND ug/kg /17/14 07:50 06/18/14 15: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 15: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 15: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: Chloroethane ND ug/kg /17/14 07:50 06/18/14 15: Chloroform ND ug/kg /17/14 07:50 06/18/14 15: Chloromethane ND ug/kg /17/14 07:50 06/18/14 15: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 15: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 15: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 15: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 15: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 15: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 15: Date: 06/25/ :55 PM without the written consent of. Page 16 of 93

91 Sample: Lab ID: 005 Collected: 06/16/14 13:45 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 15: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 15: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 15: Naphthalene ND ug/kg /17/14 07:50 06/18/14 15: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Styrene ND ug/kg /17/14 07:50 06/18/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 15: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 15: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 15: Toluene ND ug/kg /17/14 07:50 06/18/14 15: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 15: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 15: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 15: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 15: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /17/14 07:50 06/18/14 15: Toluene-d8 (S) 107 % /17/14 07:50 06/18/14 15: Bromofluorobenzene (S) 107 % /17/14 07:50 06/18/14 15: Date: 06/25/ :55 PM without the written consent of. Page 17 of 93

92 Sample: Lab ID: 006 Collected: 06/16/14 13:40 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.0 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 15: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 15: Benzene ND ug/kg /17/14 07:50 06/18/14 15: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 15: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 15: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 15: Bromoform ND ug/kg /17/14 07:50 06/18/14 15: Bromomethane ND ug/kg /17/14 07:50 06/18/14 15: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 15: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 15: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: Chloroethane ND ug/kg /17/14 07:50 06/18/14 15: Chloroform ND ug/kg /17/14 07:50 06/18/14 15: Chloromethane ND ug/kg /17/14 07:50 06/18/14 15: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 15: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 15: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 15: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 15: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 15: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 15: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 15: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 15: Date: 06/25/ :55 PM without the written consent of. Page 18 of 93

93 Sample: Lab ID: 006 Collected: 06/16/14 13:40 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 15: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 15: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 15: Naphthalene ND ug/kg /17/14 07:50 06/18/14 15: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Styrene ND ug/kg /17/14 07:50 06/18/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 15: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 15: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 15: Toluene ND ug/kg /17/14 07:50 06/18/14 15: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 15: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 15: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 15: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 15: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 15: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 15: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 15: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 110 % /17/14 07:50 06/18/14 15: Toluene-d8 (S) 106 % /17/14 07:50 06/18/14 15: Bromofluorobenzene (S) 110 % /17/14 07:50 06/18/14 15: Date: 06/25/ :55 PM without the written consent of. Page 19 of 93

94 Sample: Lab ID: 007 Collected: 06/16/14 13:35 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.4 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 16: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Benzene ND ug/kg /17/14 07:50 06/18/14 16: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 16: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromoform ND ug/kg /17/14 07:50 06/18/14 16: Bromomethane ND ug/kg /17/14 07:50 06/18/14 16: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 16: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 16: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Chloroethane ND ug/kg /17/14 07:50 06/18/14 16: Chloroform ND ug/kg /17/14 07:50 06/18/14 16: Chloromethane ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 16: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 16: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 16: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 16: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 20 of 93

95 Sample: Lab ID: 007 Collected: 06/16/14 13:35 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 16: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 16: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 16: Naphthalene ND ug/kg /17/14 07:50 06/18/14 16: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Styrene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 16: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 16: Toluene ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /17/14 07:50 06/18/14 16: Toluene-d8 (S) 108 % /17/14 07:50 06/18/14 16: Bromofluorobenzene (S) 111 % /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 21 of 93

96 Sample: Lab ID: 008 Collected: 06/16/14 13:56 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 11.0 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 16: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Benzene ND ug/kg /17/14 07:50 06/18/14 16: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 16: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromoform ND ug/kg /17/14 07:50 06/18/14 16: Bromomethane ND ug/kg /17/14 07:50 06/18/14 16: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 16: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 16: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Chloroethane ND ug/kg /17/14 07:50 06/18/14 16: Chloroform ND ug/kg /17/14 07:50 06/18/14 16: Chloromethane ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 16: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 16: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 16: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 16: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 22 of 93

97 Sample: Lab ID: 008 Collected: 06/16/14 13:56 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 16: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 16: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 16: Naphthalene ND ug/kg /17/14 07:50 06/18/14 16: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Styrene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 16: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 16: Toluene ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 110 % /17/14 07:50 06/18/14 16: Toluene-d8 (S) 103 % /17/14 07:50 06/18/14 16: Bromofluorobenzene (S) 111 % /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 23 of 93

98 Sample: DUP-3 Lab ID: 009 Collected: 06/16/14 00:00 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 10.9 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 16: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Benzene ND ug/kg /17/14 07:50 06/18/14 16: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 16: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromoform ND ug/kg /17/14 07:50 06/18/14 16: Bromomethane ND ug/kg /17/14 07:50 06/18/14 16: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 16: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 16: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Chloroethane ND ug/kg /17/14 07:50 06/18/14 16: Chloroform ND ug/kg /17/14 07:50 06/18/14 16: Chloromethane ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 16: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 16: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 16: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 16: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 24 of 93

99 Sample: DUP-3 Lab ID: 009 Collected: 06/16/14 00:00 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 16: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 16: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 16: Naphthalene ND ug/kg /17/14 07:50 06/18/14 16: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Styrene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 16: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 16: Toluene ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 111 % /17/14 07:50 06/18/14 16: Toluene-d8 (S) 99 % /17/14 07:50 06/18/14 16: Bromofluorobenzene (S) 124 % /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 25 of 93

100 Sample: Lab ID: 010 Collected: 06/16/14 13:58 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.3 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 16: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Benzene ND ug/kg /17/14 07:50 06/18/14 16: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 16: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 16: Bromoform ND ug/kg /17/14 07:50 06/18/14 16: Bromomethane ND ug/kg /17/14 07:50 06/18/14 16: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 16: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 16: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Chloroethane ND ug/kg /17/14 07:50 06/18/14 16: Chloroform ND ug/kg /17/14 07:50 06/18/14 16: Chloromethane ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 16: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 16: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 16: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 16: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 16: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 26 of 93

101 Sample: Lab ID: 010 Collected: 06/16/14 13:58 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 16: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 16: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 16: Naphthalene ND ug/kg /17/14 07:50 06/18/14 16: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Styrene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 16: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 16: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 16: Toluene ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 16: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 16: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 16: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 16: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 16: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 16: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 111 % /17/14 07:50 06/18/14 16: Toluene-d8 (S) 107 % /17/14 07:50 06/18/14 16: Bromofluorobenzene (S) 112 % /17/14 07:50 06/18/14 16: Date: 06/25/ :55 PM without the written consent of. Page 27 of 93

102 Sample: Lab ID: 011 Collected: 06/16/14 14:00 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 10.4 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 17: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 17: Benzene ND ug/kg /17/14 07:50 06/18/14 17: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 17: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 17: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 17: Bromoform ND ug/kg /17/14 07:50 06/18/14 17: Bromomethane ND ug/kg /17/14 07:50 06/18/14 17: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 17: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 17: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: Chloroethane ND ug/kg /17/14 07:50 06/18/14 17: Chloroform ND ug/kg /17/14 07:50 06/18/14 17: Chloromethane ND ug/kg /17/14 07:50 06/18/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 17: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 17: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 17: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 17: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 17: Date: 06/25/ :55 PM without the written consent of. Page 28 of 93

103 Sample: Lab ID: 011 Collected: 06/16/14 14:00 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 17: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 17: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 17: Naphthalene ND ug/kg /17/14 07:50 06/18/14 17: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Styrene ND ug/kg /17/14 07:50 06/18/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 17: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 17: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 17: Toluene ND ug/kg /17/14 07:50 06/18/14 17: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 17: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 17: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 17: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 17: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /17/14 07:50 06/18/14 17: Toluene-d8 (S) 104 % /17/14 07:50 06/18/14 17: Bromofluorobenzene (S) 103 % /17/14 07:50 06/18/14 17: Date: 06/25/ :55 PM without the written consent of. Page 29 of 93

104 Sample: Lab ID: 012 Collected: 06/16/14 13:30 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 8.8 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 17: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 17: Benzene ND ug/kg /17/14 07:50 06/18/14 17: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 17: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 17: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 17: Bromoform ND ug/kg /17/14 07:50 06/18/14 17: Bromomethane ND ug/kg /17/14 07:50 06/18/14 17: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 17: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 17: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: Chloroethane ND ug/kg /17/14 07:50 06/18/14 17: Chloroform ND ug/kg /17/14 07:50 06/18/14 17: Chloromethane ND ug/kg /17/14 07:50 06/18/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 17: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 17: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 17: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 17: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 17: Date: 06/25/ :55 PM without the written consent of. Page 30 of 93

105 Sample: Lab ID: 012 Collected: 06/16/14 13:30 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 17: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 17: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 17: Naphthalene ND ug/kg /17/14 07:50 06/18/14 17: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Styrene ND ug/kg /17/14 07:50 06/18/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 17: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 17: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 17: Toluene ND ug/kg /17/14 07:50 06/18/14 17: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 17: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 17: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 17: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 17: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 108 % /17/14 07:50 06/18/14 17: Toluene-d8 (S) 94 % /17/14 07:50 06/18/14 17: Bromofluorobenzene (S) 121 % /17/14 07:50 06/18/14 17: Date: 06/25/ :55 PM without the written consent of. Page 31 of 93

106 Sample: Lab ID: 013 Collected: 06/16/14 13:25 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 9.2 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 17: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 17: Benzene ND ug/kg /17/14 07:50 06/18/14 17: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 17: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 17: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 17: Bromoform ND ug/kg /17/14 07:50 06/18/14 17: Bromomethane ND ug/kg /17/14 07:50 06/18/14 17: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 17: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 17: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: Chloroethane ND ug/kg /17/14 07:50 06/18/14 17: Chloroform ND ug/kg /17/14 07:50 06/18/14 17: Chloromethane ND ug/kg /17/14 07:50 06/18/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 17: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 17: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 17: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 17: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 17: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 17: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 17: Date: 06/25/ :55 PM without the written consent of. Page 32 of 93

107 Sample: Lab ID: 013 Collected: 06/16/14 13:25 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 17: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 17: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 17: Naphthalene ND ug/kg /17/14 07:50 06/18/14 17: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Styrene ND ug/kg /17/14 07:50 06/18/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 17: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 17: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 17: Toluene ND ug/kg /17/14 07:50 06/18/14 17: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 17: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 17: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 17: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 17: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 17: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 17: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 17: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /17/14 07:50 06/18/14 17: Toluene-d8 (S) 103 % /17/14 07:50 06/18/14 17: Bromofluorobenzene (S) 103 % /17/14 07:50 06/18/14 17: Date: 06/25/ :55 PM without the written consent of. Page 33 of 93

108 Sample: Lab ID: 014 Collected: 06/16/14 14:12 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.1 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 18: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 18: Benzene ND ug/kg /17/14 07:50 06/18/14 18: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 18: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 18: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 18: Bromoform ND ug/kg /17/14 07:50 06/18/14 18: Bromomethane ND ug/kg /17/14 07:50 06/18/14 18: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 18: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 18: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: Chloroethane ND ug/kg /17/14 07:50 06/18/14 18: Chloroform ND ug/kg /17/14 07:50 06/18/14 18: Chloromethane ND ug/kg /17/14 07:50 06/18/14 18: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 18: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 18: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 18: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 18: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 18: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 18: Date: 06/25/ :55 PM without the written consent of. Page 34 of 93

109 Sample: Lab ID: 014 Collected: 06/16/14 14:12 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 18: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 18: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 18: Naphthalene ND ug/kg /17/14 07:50 06/18/14 18: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Styrene ND ug/kg /17/14 07:50 06/18/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 18: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 18: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 18: Toluene ND ug/kg /17/14 07:50 06/18/14 18: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 18: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 18: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 18: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 18: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /17/14 07:50 06/18/14 18: Toluene-d8 (S) 95 % /17/14 07:50 06/18/14 18: Bromofluorobenzene (S) 111 % /17/14 07:50 06/18/14 18: Date: 06/25/ :55 PM without the written consent of. Page 35 of 93

110 Sample: Lab ID: 015 Collected: 06/16/14 13:20 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 11.4 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 18: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 18: Benzene ND ug/kg /17/14 07:50 06/18/14 18: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 18: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 18: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 18: Bromoform ND ug/kg /17/14 07:50 06/18/14 18: Bromomethane ND ug/kg /17/14 07:50 06/18/14 18: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 18: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 18: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: Chloroethane ND ug/kg /17/14 07:50 06/18/14 18: Chloroform ND ug/kg /17/14 07:50 06/18/14 18: Chloromethane ND ug/kg /17/14 07:50 06/18/14 18: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 18: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 18: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 18: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 18: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 18: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 18: Date: 06/25/ :55 PM without the written consent of. Page 36 of 93

111 Sample: Lab ID: 015 Collected: 06/16/14 13:20 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 18: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 18: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 18: Naphthalene ND ug/kg /17/14 07:50 06/18/14 18: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Styrene ND ug/kg /17/14 07:50 06/18/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 18: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 18: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 18: Toluene ND ug/kg /17/14 07:50 06/18/14 18: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 18: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 18: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 18: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 18: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 108 % /17/14 07:50 06/18/14 18: Toluene-d8 (S) 106 % /17/14 07:50 06/18/14 18: Bromofluorobenzene (S) 110 % /17/14 07:50 06/18/14 18: Date: 06/25/ :55 PM without the written consent of. Page 37 of 93

112 Sample: Lab ID: 016 Collected: 06/16/14 13:15 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 10.7 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/18/14 18: Allyl chloride ND ug/kg /17/14 07:50 06/18/14 18: Benzene ND ug/kg /17/14 07:50 06/18/14 18: Bromobenzene ND ug/kg /17/14 07:50 06/18/14 18: Bromochloromethane ND ug/kg /17/14 07:50 06/18/14 18: Bromodichloromethane ND ug/kg /17/14 07:50 06/18/14 18: Bromoform ND ug/kg /17/14 07:50 06/18/14 18: Bromomethane ND ug/kg /17/14 07:50 06/18/14 18: Butanone (MEK) ND ug/kg /17/14 07:50 06/18/14 18: n-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: sec-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: tert-butylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Carbon tetrachloride ND ug/kg /17/14 07:50 06/18/14 18: Chlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: Chloroethane ND ug/kg /17/14 07:50 06/18/14 18: Chloroform ND ug/kg /17/14 07:50 06/18/14 18: Chloromethane ND ug/kg /17/14 07:50 06/18/14 18: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 18: Chlorotoluene ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/18/14 18: Dibromochloromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/18/14 18: Dibromomethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/18/14 18: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/18/14 18: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/18/14 18: L3 Ethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/18/14 18: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/18/14 18: Date: 06/25/ :55 PM without the written consent of. Page 38 of 93

113 Sample: Lab ID: 016 Collected: 06/16/14 13:15 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/18/14 18: Methylene Chloride ND ug/kg /17/14 07:50 06/18/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/18/14 18: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/18/14 18: Naphthalene ND ug/kg /17/14 07:50 06/18/14 18: n-propylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Styrene ND ug/kg /17/14 07:50 06/18/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/18/14 18: Tetrachloroethene ND ug/kg /17/14 07:50 06/18/14 18: Tetrahydrofuran ND ug/kg /17/14 07:50 06/18/14 18: Toluene ND ug/kg /17/14 07:50 06/18/14 18: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/18/14 18: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/18/14 18: Trichloroethene ND ug/kg /17/14 07:50 06/18/14 18: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/18/14 18: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/18/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/18/14 18: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/18/14 18: Vinyl chloride ND ug/kg /17/14 07:50 06/18/14 18: Xylene (Total) ND ug/kg /17/14 07:50 06/18/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 107 % /17/14 07:50 06/18/14 18: Toluene-d8 (S) 110 % /17/14 07:50 06/18/14 18: Bromofluorobenzene (S) 96 % /17/14 07:50 06/18/14 18: Date: 06/25/ :55 PM without the written consent of. Page 39 of 93

114 Sample: Lab ID: 017 Collected: 06/16/14 14:10 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 9.9 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/18/14 19: Allyl chloride ND ug/kg /17/14 07:49 06/18/14 19: Benzene ND ug/kg /17/14 07:49 06/18/14 19: Bromobenzene ND ug/kg /17/14 07:49 06/18/14 19: Bromochloromethane ND ug/kg /17/14 07:49 06/18/14 19: Bromodichloromethane ND ug/kg /17/14 07:49 06/18/14 19: Bromoform ND ug/kg /17/14 07:49 06/18/14 19: Bromomethane ND ug/kg /17/14 07:49 06/18/14 19: Butanone (MEK) ND ug/kg /17/14 07:49 06/18/14 19: n-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: sec-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: tert-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Carbon tetrachloride ND ug/kg /17/14 07:49 06/18/14 19: Chlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: Chloroethane ND ug/kg /17/14 07:49 06/18/14 19: Chloroform ND ug/kg /17/14 07:49 06/18/14 19: Chloromethane ND ug/kg /17/14 07:49 06/18/14 19: Chlorotoluene ND ug/kg /17/14 07:49 06/18/14 19: Chlorotoluene ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/18/14 19: Dibromochloromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/18/14 19: Dibromomethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/18/14 19: L3 Ethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/18/14 19: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/18/14 19: Date: 06/25/ :55 PM without the written consent of. Page 40 of 93

115 Sample: Lab ID: 017 Collected: 06/16/14 14:10 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/18/14 19: Methylene Chloride ND ug/kg /17/14 07:49 06/18/14 19: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/18/14 19: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/18/14 19: Naphthalene ND ug/kg /17/14 07:49 06/18/14 19: n-propylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Styrene ND ug/kg /17/14 07:49 06/18/14 19: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/18/14 19: Tetrachloroethene ND ug/kg /17/14 07:49 06/18/14 19: Tetrahydrofuran ND ug/kg /17/14 07:49 06/18/14 19: Toluene ND ug/kg /17/14 07:49 06/18/14 19: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/18/14 19: Trichloroethene ND ug/kg /17/14 07:49 06/18/14 19: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/18/14 19: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Vinyl chloride ND ug/kg /17/14 07:49 06/18/14 19: Xylene (Total) ND ug/kg /17/14 07:49 06/18/14 19: Surrogates 1,2-Dichloroethane-d4 (S) 109 % /17/14 07:49 06/18/14 19: Toluene-d8 (S) 108 % /17/14 07:49 06/18/14 19: Bromofluorobenzene (S) 112 % /17/14 07:49 06/18/14 19: Date: 06/25/ :55 PM without the written consent of. Page 41 of 93

116 Sample: Lab ID: 018 Collected: 06/16/14 14:00 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.6 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/18/14 19: Allyl chloride ND ug/kg /17/14 07:49 06/18/14 19: Benzene ND ug/kg /17/14 07:49 06/18/14 19: Bromobenzene ND ug/kg /17/14 07:49 06/18/14 19: Bromochloromethane ND ug/kg /17/14 07:49 06/18/14 19: Bromodichloromethane ND ug/kg /17/14 07:49 06/18/14 19: Bromoform ND ug/kg /17/14 07:49 06/18/14 19: Bromomethane ND ug/kg /17/14 07:49 06/18/14 19: Butanone (MEK) ND ug/kg /17/14 07:49 06/18/14 19: n-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: sec-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: tert-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Carbon tetrachloride ND ug/kg /17/14 07:49 06/18/14 19: Chlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: Chloroethane ND ug/kg /17/14 07:49 06/18/14 19: Chloroform ND ug/kg /17/14 07:49 06/18/14 19: Chloromethane ND ug/kg /17/14 07:49 06/18/14 19: Chlorotoluene ND ug/kg /17/14 07:49 06/18/14 19: Chlorotoluene ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/18/14 19: Dibromochloromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/18/14 19: Dibromomethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/18/14 19: L3 Ethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/18/14 19: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/18/14 19: Date: 06/25/ :55 PM without the written consent of. Page 42 of 93

117 Sample: Lab ID: 018 Collected: 06/16/14 14:00 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/18/14 19: Methylene Chloride ND ug/kg /17/14 07:49 06/18/14 19: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/18/14 19: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/18/14 19: Naphthalene ND ug/kg /17/14 07:49 06/18/14 19: n-propylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Styrene ND ug/kg /17/14 07:49 06/18/14 19: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/18/14 19: Tetrachloroethene ND ug/kg /17/14 07:49 06/18/14 19: Tetrahydrofuran ND ug/kg /17/14 07:49 06/18/14 19: Toluene ND ug/kg /17/14 07:49 06/18/14 19: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/18/14 19: Trichloroethene ND ug/kg /17/14 07:49 06/18/14 19: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/18/14 19: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Vinyl chloride ND ug/kg /17/14 07:49 06/18/14 19: Xylene (Total) ND ug/kg /17/14 07:49 06/18/14 19: Surrogates 1,2-Dichloroethane-d4 (S) 107 % /17/14 07:49 06/18/14 19: Toluene-d8 (S) 107 % /17/14 07:49 06/18/14 19: Bromofluorobenzene (S) 110 % /17/14 07:49 06/18/14 19: Date: 06/25/ :55 PM without the written consent of. Page 43 of 93

118 Sample: Lab ID: 019 Collected: 06/16/14 14:06 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.7 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 14: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 14: Benzene ND ug/kg /17/14 07:49 06/19/14 14: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 14: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 14: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 14: Bromoform ND ug/kg /17/14 07:49 06/19/14 14: Bromomethane ND ug/kg /17/14 07:49 06/19/14 14: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 14: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 14: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: Chloroethane ND ug/kg /17/14 07:49 06/19/14 14: Chloroform ND ug/kg /17/14 07:49 06/19/14 14: Chloromethane ND ug/kg /17/14 07:49 06/19/14 14: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 14: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 14: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 14: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 14: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 14: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 14: Date: 06/25/ :55 PM without the written consent of. Page 44 of 93

119 Sample: Lab ID: 019 Collected: 06/16/14 14:06 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 14: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 14: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 14: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 14: Naphthalene ND ug/kg /17/14 07:49 06/19/14 14: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Styrene ND ug/kg /17/14 07:49 06/19/14 14: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 14: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 14: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 14: Toluene ND ug/kg /17/14 07:49 06/19/14 14: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 14: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 14: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 14: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 14: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 14: Surrogates 1,2-Dichloroethane-d4 (S) 106 % /17/14 07:49 06/19/14 14: Toluene-d8 (S) 103 % /17/14 07:49 06/19/14 14: Bromofluorobenzene (S) 118 % /17/14 07:49 06/19/14 14: Date: 06/25/ :55 PM without the written consent of. Page 45 of 93

120 Sample: Lab ID: 020 Collected: 06/16/14 14:04 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 15.7 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 14: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 14: Benzene ND ug/kg /17/14 07:49 06/19/14 14: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 14: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 14: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 14: Bromoform ND ug/kg /17/14 07:49 06/19/14 14: Bromomethane ND ug/kg /17/14 07:49 06/19/14 14: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 14: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 14: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: Chloroethane ND ug/kg /17/14 07:49 06/19/14 14: Chloroform ND ug/kg /17/14 07:49 06/19/14 14: Chloromethane ND ug/kg /17/14 07:49 06/19/14 14: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 14: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 14: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 14: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 14: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 14: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 14: Date: 06/25/ :55 PM without the written consent of. Page 46 of 93

121 Sample: Lab ID: 020 Collected: 06/16/14 14:04 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 14: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 14: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 14: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 14: Naphthalene ND ug/kg /17/14 07:49 06/19/14 14: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Styrene ND ug/kg /17/14 07:49 06/19/14 14: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 14: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 14: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 14: Toluene ND ug/kg /17/14 07:49 06/19/14 14: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 14: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 14: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 14: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 14: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 14: Surrogates 1,2-Dichloroethane-d4 (S) 106 % /17/14 07:49 06/19/14 14: Toluene-d8 (S) 100 % /17/14 07:49 06/19/14 14: Bromofluorobenzene (S) 111 % /17/14 07:49 06/19/14 14: Date: 06/25/ :55 PM without the written consent of. Page 47 of 93

122 Sample: Lab ID: 021 Collected: 06/16/14 13:10 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 11.6 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 14: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 14: Benzene ND ug/kg /17/14 07:49 06/19/14 14: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 14: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 14: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 14: Bromoform ND ug/kg /17/14 07:49 06/19/14 14: Bromomethane ND ug/kg /17/14 07:49 06/19/14 14: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 14: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 14: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: Chloroethane ND ug/kg /17/14 07:49 06/19/14 14: Chloroform ND ug/kg /17/14 07:49 06/19/14 14: Chloromethane ND ug/kg /17/14 07:49 06/19/14 14: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 14: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 14: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 14: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 14: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 14: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 14: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 14: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 14: Date: 06/25/ :55 PM without the written consent of. Page 48 of 93

123 Sample: Lab ID: 021 Collected: 06/16/14 13:10 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 14: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 14: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 14: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 14: Naphthalene ND ug/kg /17/14 07:49 06/19/14 14: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Styrene ND ug/kg /17/14 07:49 06/19/14 14: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 14: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 14: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 14: Toluene ND ug/kg /17/14 07:49 06/19/14 14: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 14: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 14: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 14: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 14: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 14: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 14: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 14: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 14: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 14: Surrogates 1,2-Dichloroethane-d4 (S) 106 % /17/14 07:49 06/19/14 14: Toluene-d8 (S) 106 % /17/14 07:49 06/19/14 14: Bromofluorobenzene (S) 110 % /17/14 07:49 06/19/14 14: Date: 06/25/ :55 PM without the written consent of. Page 49 of 93

124 Sample: Lab ID: 022 Collected: 06/16/14 13:05 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.3 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 15: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 15: Benzene ND ug/kg /17/14 07:49 06/19/14 15: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 15: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 15: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 15: Bromoform ND ug/kg /17/14 07:49 06/19/14 15: Bromomethane ND ug/kg /17/14 07:49 06/19/14 15: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 15: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 15: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: Chloroethane ND ug/kg /17/14 07:49 06/19/14 15: Chloroform ND ug/kg /17/14 07:49 06/19/14 15: Chloromethane ND ug/kg /17/14 07:49 06/19/14 15: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 15: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 15: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 15: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 15: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 15: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 15: Date: 06/25/ :55 PM without the written consent of. Page 50 of 93

125 Sample: Lab ID: 022 Collected: 06/16/14 13:05 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 15: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 15: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 15: Naphthalene ND ug/kg /17/14 07:49 06/19/14 15: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Styrene ND ug/kg /17/14 07:49 06/19/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 15: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 15: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 15: Toluene ND ug/kg /17/14 07:49 06/19/14 15: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 15: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 15: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 15: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 15: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 106 % /17/14 07:49 06/19/14 15: Toluene-d8 (S) 103 % /17/14 07:49 06/19/14 15: Bromofluorobenzene (S) 109 % /17/14 07:49 06/19/14 15: Date: 06/25/ :55 PM without the written consent of. Page 51 of 93

126 Sample: Lab ID: 023 Collected: 06/16/14 13:00 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.4 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 15: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 15: Benzene ND ug/kg /17/14 07:49 06/19/14 15: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 15: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 15: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 15: Bromoform ND ug/kg /17/14 07:49 06/19/14 15: Bromomethane ND ug/kg /17/14 07:49 06/19/14 15: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 15: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 15: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: Chloroethane ND ug/kg /17/14 07:49 06/19/14 15: Chloroform ND ug/kg /17/14 07:49 06/19/14 15: Chloromethane ND ug/kg /17/14 07:49 06/19/14 15: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 15: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 15: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 15: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 15: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 15: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 15: Date: 06/25/ :55 PM without the written consent of. Page 52 of 93

127 Sample: Lab ID: 023 Collected: 06/16/14 13:00 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 15: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 15: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 15: Naphthalene ND ug/kg /17/14 07:49 06/19/14 15: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Styrene ND ug/kg /17/14 07:49 06/19/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 15: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 15: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 15: Toluene ND ug/kg /17/14 07:49 06/19/14 15: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 15: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 15: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 15: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 15: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /17/14 07:49 06/19/14 15: Toluene-d8 (S) 105 % /17/14 07:49 06/19/14 15: Bromofluorobenzene (S) 109 % /17/14 07:49 06/19/14 15: Date: 06/25/ :55 PM without the written consent of. Page 53 of 93

128 Sample: Lab ID: 024 Collected: 06/16/14 12:58 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 10.4 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 15: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 15: Benzene ND ug/kg /17/14 07:49 06/19/14 15: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 15: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 15: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 15: Bromoform ND ug/kg /17/14 07:49 06/19/14 15: Bromomethane ND ug/kg /17/14 07:49 06/19/14 15: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 15: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 15: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: Chloroethane ND ug/kg /17/14 07:49 06/19/14 15: Chloroform ND ug/kg /17/14 07:49 06/19/14 15: Chloromethane ND ug/kg /17/14 07:49 06/19/14 15: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 15: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 15: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 15: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 15: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 15: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 15: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 15: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 15: Date: 06/25/ :55 PM without the written consent of. Page 54 of 93

129 Sample: Lab ID: 024 Collected: 06/16/14 12:58 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 15: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 15: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 15: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 15: Naphthalene ND ug/kg /17/14 07:49 06/19/14 15: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Styrene ND ug/kg /17/14 07:49 06/19/14 15: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 15: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 15: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 15: Toluene ND ug/kg /17/14 07:49 06/19/14 15: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 15: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 15: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 15: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 15: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 15: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 15: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 15: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 15: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 15: Surrogates 1,2-Dichloroethane-d4 (S) 105 % /17/14 07:49 06/19/14 15: Toluene-d8 (S) 103 % /17/14 07:49 06/19/14 15: Bromofluorobenzene (S) 108 % /17/14 07:49 06/19/14 15: Date: 06/25/ :55 PM without the written consent of. Page 55 of 93

130 Sample: Lab ID: 025 Collected: 06/16/14 12:54 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 11.1 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 16: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 16: Benzene ND ug/kg /17/14 07:49 06/19/14 16: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 16: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 16: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 16: Bromoform ND ug/kg /17/14 07:49 06/19/14 16: Bromomethane ND ug/kg /17/14 07:49 06/19/14 16: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 16: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 16: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 16: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 16: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: Chloroethane ND ug/kg /17/14 07:49 06/19/14 16: Chloroform ND ug/kg /17/14 07:49 06/19/14 16: Chloromethane ND ug/kg /17/14 07:49 06/19/14 16: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 16: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 16: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 16: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 16: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 16: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 16: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 16: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 16: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 16: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 16: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 16: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 16: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 16: Date: 06/25/ :55 PM without the written consent of. Page 56 of 93

131 Sample: Lab ID: 025 Collected: 06/16/14 12:54 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 16: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 16: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 16: Naphthalene ND ug/kg /17/14 07:49 06/19/14 16: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Styrene ND ug/kg /17/14 07:49 06/19/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 16: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 16: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 16: Toluene ND ug/kg /17/14 07:49 06/19/14 16: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 16: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 16: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 16: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 16: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 16: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 16: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 105 % /17/14 07:49 06/19/14 16: Toluene-d8 (S) 106 % /17/14 07:49 06/19/14 16: Bromofluorobenzene (S) 112 % /17/14 07:49 06/19/14 16: Date: 06/25/ :55 PM without the written consent of. Page 57 of 93

132 Sample: Lab ID: 026 Collected: 06/16/14 12:50 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.2 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 16: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 16: Benzene ND ug/kg /17/14 07:49 06/19/14 16: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 16: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 16: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 16: Bromoform ND ug/kg /17/14 07:49 06/19/14 16: Bromomethane ND ug/kg /17/14 07:49 06/19/14 16: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 16: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 16: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 16: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 16: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: Chloroethane ND ug/kg /17/14 07:49 06/19/14 16: Chloroform ND ug/kg /17/14 07:49 06/19/14 16: Chloromethane ND ug/kg /17/14 07:49 06/19/14 16: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 16: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 16: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 16: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 16: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 16: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 16: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 16: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 16: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 16: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 16: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 16: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 16: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 16: Date: 06/25/ :55 PM without the written consent of. Page 58 of 93

133 Sample: Lab ID: 026 Collected: 06/16/14 12:50 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 16: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 16: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 16: Naphthalene ND ug/kg /17/14 07:49 06/19/14 16: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Styrene ND ug/kg /17/14 07:49 06/19/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 16: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 16: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 16: Toluene ND ug/kg /17/14 07:49 06/19/14 16: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 16: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 16: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 16: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 16: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 16: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 16: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 16: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 16: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 16: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /17/14 07:49 06/19/14 16: Toluene-d8 (S) 107 % /17/14 07:49 06/19/14 16: Bromofluorobenzene (S) 112 % /17/14 07:49 06/19/14 16: Date: 06/25/ :55 PM without the written consent of. Page 59 of 93

134 Sample: MS/MSD Lab ID: 027 Collected: 06/16/14 12:48 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.3 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/18/14 19: M1 Allyl chloride ND ug/kg /17/14 07:49 06/18/14 19: Benzene ND ug/kg /17/14 07:49 06/18/14 19: Bromobenzene ND ug/kg /17/14 07:49 06/18/14 19: Bromochloromethane ND ug/kg /17/14 07:49 06/18/14 19: Bromodichloromethane ND ug/kg /17/14 07:49 06/18/14 19: Bromoform ND ug/kg /17/14 07:49 06/18/14 19: Bromomethane ND ug/kg /17/14 07:49 06/18/14 19: Butanone (MEK) ND ug/kg /17/14 07:49 06/18/14 19: n-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: sec-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: tert-butylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Carbon tetrachloride ND ug/kg /17/14 07:49 06/18/14 19: Chlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: Chloroethane ND ug/kg /17/14 07:49 06/18/14 19: Chloroform ND ug/kg /17/14 07:49 06/18/14 19: Chloromethane ND ug/kg /17/14 07:49 06/18/14 19: Chlorotoluene ND ug/kg /17/14 07:49 06/18/14 19: Chlorotoluene ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/18/14 19: Dibromochloromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/18/14 19: Dibromomethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/18/14 19: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/18/14 19: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/18/14 19: L3,M0 Ethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/18/14 19: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/18/14 19: Date: 06/25/ :55 PM without the written consent of. Page 60 of 93

135 Sample: MS/MSD Lab ID: 027 Collected: 06/16/14 12:48 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/18/14 19: Methylene Chloride ND ug/kg /17/14 07:49 06/18/14 19: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/18/14 19: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/18/14 19: Naphthalene ND ug/kg /17/14 07:49 06/18/14 19: n-propylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Styrene ND ug/kg /17/14 07:49 06/18/14 19: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/18/14 19: Tetrachloroethene ND ug/kg /17/14 07:49 06/18/14 19: Tetrahydrofuran ND ug/kg /17/14 07:49 06/18/14 19: Toluene ND ug/kg /17/14 07:49 06/18/14 19: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/18/14 19: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/18/14 19: Trichloroethene ND ug/kg /17/14 07:49 06/18/14 19: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/18/14 19: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/18/14 19: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/18/14 19: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/18/14 19: Vinyl chloride ND ug/kg /17/14 07:49 06/18/14 19: Xylene (Total) ND ug/kg /17/14 07:49 06/18/14 19: Surrogates 1,2-Dichloroethane-d4 (S) 105 % /17/14 07:49 06/18/14 19: Toluene-d8 (S) 112 % /17/14 07:49 06/18/14 19: Bromofluorobenzene (S) 106 % /17/14 07:49 06/18/14 19: Date: 06/25/ :55 PM without the written consent of. Page 61 of 93

136 Sample: DUP-5 Lab ID: 028 Collected: 06/16/14 00:00 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 13.6 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/19/14 16: Allyl chloride ND ug/kg /17/14 07:50 06/19/14 16: Benzene ND ug/kg /17/14 07:50 06/19/14 16: Bromobenzene ND ug/kg /17/14 07:50 06/19/14 16: Bromochloromethane ND ug/kg /17/14 07:50 06/19/14 16: Bromodichloromethane ND ug/kg /17/14 07:50 06/19/14 16: Bromoform ND ug/kg /17/14 07:50 06/19/14 16: Bromomethane ND ug/kg /17/14 07:50 06/19/14 16: Butanone (MEK) ND ug/kg /17/14 07:50 06/19/14 16: n-butylbenzene ND ug/kg /17/14 07:50 06/19/14 16: sec-butylbenzene ND ug/kg /17/14 07:50 06/19/14 16: tert-butylbenzene ND ug/kg /17/14 07:50 06/19/14 16: Carbon tetrachloride ND ug/kg /17/14 07:50 06/19/14 16: Chlorobenzene ND ug/kg /17/14 07:50 06/19/14 16: Chloroethane ND ug/kg /17/14 07:50 06/19/14 16: Chloroform ND ug/kg /17/14 07:50 06/19/14 16: Chloromethane ND ug/kg /17/14 07:50 06/19/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/19/14 16: Chlorotoluene ND ug/kg /17/14 07:50 06/19/14 16: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/19/14 16: Dibromochloromethane ND ug/kg /17/14 07:50 06/19/14 16: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/19/14 16: Dibromomethane ND ug/kg /17/14 07:50 06/19/14 16: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/19/14 16: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/19/14 16: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/19/14 16: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/19/14 16: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/19/14 16: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/19/14 16: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/19/14 16: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/19/14 16: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/19/14 16: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/19/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/19/14 16: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/19/14 16: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/19/14 16: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/19/14 16: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/19/14 16: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/19/14 16: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/19/14 16: Ethylbenzene ND ug/kg /17/14 07:50 06/19/14 16: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/19/14 16: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/19/14 16: Date: 06/25/ :55 PM without the written consent of. Page 62 of 93

137 Sample: DUP-5 Lab ID: 028 Collected: 06/16/14 00:00 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/19/14 16: Methylene Chloride ND ug/kg /17/14 07:50 06/19/14 16: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/19/14 16: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/19/14 16: Naphthalene ND ug/kg /17/14 07:50 06/19/14 16: n-propylbenzene ND ug/kg /17/14 07:50 06/19/14 16: Styrene ND ug/kg /17/14 07:50 06/19/14 16: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/19/14 16: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/19/14 16: Tetrachloroethene ND ug/kg /17/14 07:50 06/19/14 16: Tetrahydrofuran ND ug/kg /17/14 07:50 06/19/14 16: Toluene ND ug/kg /17/14 07:50 06/19/14 16: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/19/14 16: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/19/14 16: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/19/14 16: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/19/14 16: Trichloroethene ND ug/kg /17/14 07:50 06/19/14 16: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/19/14 16: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/19/14 16: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/19/14 16: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/19/14 16: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/19/14 16: Vinyl chloride ND ug/kg /17/14 07:50 06/19/14 16: Xylene (Total) ND ug/kg /17/14 07:50 06/19/14 16: Surrogates 1,2-Dichloroethane-d4 (S) 107 % /17/14 07:50 06/19/14 16: Toluene-d8 (S) 101 % /17/14 07:50 06/19/14 16: Bromofluorobenzene (S) 109 % /17/14 07:50 06/19/14 16: Date: 06/25/ :55 PM without the written consent of. Page 63 of 93

138 Sample: MS/MSD Lab ID: 029 Collected: 06/16/14 13:50 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 18.3 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 17: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 17: Benzene ND ug/kg /17/14 07:49 06/19/14 17: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 17: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 17: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 17: Bromoform ND ug/kg /17/14 07:49 06/19/14 17: Bromomethane ND ug/kg /17/14 07:49 06/19/14 17: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 17: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 17: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: Chloroethane ND ug/kg /17/14 07:49 06/19/14 17: Chloroform ND ug/kg /17/14 07:49 06/19/14 17: Chloromethane ND ug/kg /17/14 07:49 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 17: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 17: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 17: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 17: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 64 of 93

139 Sample: MS/MSD Lab ID: 029 Collected: 06/16/14 13:50 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 17: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 17: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 17: Naphthalene ND ug/kg /17/14 07:49 06/19/14 17: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Styrene ND ug/kg /17/14 07:49 06/19/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 17: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 17: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 17: Toluene ND ug/kg /17/14 07:49 06/19/14 17: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 17: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 17: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 17: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 17: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 104 % /17/14 07:49 06/19/14 17: Toluene-d8 (S) 101 % /17/14 07:49 06/19/14 17: Bromofluorobenzene (S) 105 % /17/14 07:49 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 65 of 93

140 Sample: DUP-2 Lab ID: 030 Collected: 06/16/14 00:00 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 17.5 % /17/14 00:00 Acetone ND ug/kg /17/14 07:50 06/19/14 17: Allyl chloride ND ug/kg /17/14 07:50 06/19/14 17: Benzene ND ug/kg /17/14 07:50 06/19/14 17: Bromobenzene ND ug/kg /17/14 07:50 06/19/14 17: Bromochloromethane ND ug/kg /17/14 07:50 06/19/14 17: Bromodichloromethane ND ug/kg /17/14 07:50 06/19/14 17: Bromoform ND ug/kg /17/14 07:50 06/19/14 17: Bromomethane ND ug/kg /17/14 07:50 06/19/14 17: Butanone (MEK) ND ug/kg /17/14 07:50 06/19/14 17: n-butylbenzene ND ug/kg /17/14 07:50 06/19/14 17: sec-butylbenzene ND ug/kg /17/14 07:50 06/19/14 17: tert-butylbenzene ND ug/kg /17/14 07:50 06/19/14 17: Carbon tetrachloride ND ug/kg /17/14 07:50 06/19/14 17: Chlorobenzene ND ug/kg /17/14 07:50 06/19/14 17: Chloroethane ND ug/kg /17/14 07:50 06/19/14 17: Chloroform ND ug/kg /17/14 07:50 06/19/14 17: Chloromethane ND ug/kg /17/14 07:50 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:50 06/19/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:50 06/19/14 17: Dibromochloromethane ND ug/kg /17/14 07:50 06/19/14 17: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:50 06/19/14 17: Dibromomethane ND ug/kg /17/14 07:50 06/19/14 17: ,2-Dichlorobenzene ND ug/kg /17/14 07:50 06/19/14 17: ,3-Dichlorobenzene ND ug/kg /17/14 07:50 06/19/14 17: ,4-Dichlorobenzene ND ug/kg /17/14 07:50 06/19/14 17: Dichlorodifluoromethane ND ug/kg /17/14 07:50 06/19/14 17: ,1-Dichloroethane ND ug/kg /17/14 07:50 06/19/14 17: ,2-Dichloroethane ND ug/kg /17/14 07:50 06/19/14 17: ,1-Dichloroethene ND ug/kg /17/14 07:50 06/19/14 17: cis-1,2-dichloroethene ND ug/kg /17/14 07:50 06/19/14 17: trans-1,2-dichloroethene ND ug/kg /17/14 07:50 06/19/14 17: Dichlorofluoromethane ND ug/kg /17/14 07:50 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/19/14 17: ,3-Dichloropropane ND ug/kg /17/14 07:50 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:50 06/19/14 17: ,1-Dichloropropene ND ug/kg /17/14 07:50 06/19/14 17: cis-1,3-dichloropropene ND ug/kg /17/14 07:50 06/19/14 17: trans-1,3-dichloropropene ND ug/kg /17/14 07:50 06/19/14 17: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:50 06/19/14 17: Ethylbenzene ND ug/kg /17/14 07:50 06/19/14 17: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:50 06/19/14 17: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:50 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 66 of 93

141 Sample: DUP-2 Lab ID: 030 Collected: 06/16/14 00:00 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:50 06/19/14 17: Methylene Chloride ND ug/kg /17/14 07:50 06/19/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:50 06/19/14 17: Methyl-tert-butyl ether ND ug/kg /17/14 07:50 06/19/14 17: Naphthalene ND ug/kg /17/14 07:50 06/19/14 17: n-propylbenzene ND ug/kg /17/14 07:50 06/19/14 17: Styrene ND ug/kg /17/14 07:50 06/19/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/19/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:50 06/19/14 17: Tetrachloroethene ND ug/kg /17/14 07:50 06/19/14 17: Tetrahydrofuran ND ug/kg /17/14 07:50 06/19/14 17: Toluene ND ug/kg /17/14 07:50 06/19/14 17: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:50 06/19/14 17: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:50 06/19/14 17: ,1,1-Trichloroethane ND ug/kg /17/14 07:50 06/19/14 17: ,1,2-Trichloroethane ND ug/kg /17/14 07:50 06/19/14 17: Trichloroethene ND ug/kg /17/14 07:50 06/19/14 17: Trichlorofluoromethane ND ug/kg /17/14 07:50 06/19/14 17: ,2,3-Trichloropropane ND ug/kg /17/14 07:50 06/19/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:50 06/19/14 17: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:50 06/19/14 17: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:50 06/19/14 17: Vinyl chloride ND ug/kg /17/14 07:50 06/19/14 17: Xylene (Total) ND ug/kg /17/14 07:50 06/19/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 107 % /17/14 07:50 06/19/14 17: Toluene-d8 (S) 96 % /17/14 07:50 06/19/14 17: Bromofluorobenzene (S) 109 % /17/14 07:50 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 67 of 93

142 Sample: Lab ID: 031 Collected: 06/16/14 14:30 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 12.1 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 17: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 17: Benzene ND ug/kg /17/14 07:49 06/19/14 17: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 17: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 17: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 17: Bromoform ND ug/kg /17/14 07:49 06/19/14 17: Bromomethane ND ug/kg /17/14 07:49 06/19/14 17: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 17: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 17: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: Chloroethane ND ug/kg /17/14 07:49 06/19/14 17: Chloroform ND ug/kg /17/14 07:49 06/19/14 17: Chloromethane ND ug/kg /17/14 07:49 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 17: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 17: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 17: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 17: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 68 of 93

143 Sample: Lab ID: 031 Collected: 06/16/14 14:30 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 17: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 17: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 17: Naphthalene ND ug/kg /17/14 07:49 06/19/14 17: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Styrene ND ug/kg /17/14 07:49 06/19/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 17: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 17: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 17: Toluene ND ug/kg /17/14 07:49 06/19/14 17: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 17: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 17: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 17: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 17: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 108 % /17/14 07:49 06/19/14 17: Toluene-d8 (S) 102 % /17/14 07:49 06/19/14 17: Bromofluorobenzene (S) 110 % /17/14 07:49 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 69 of 93

144 Sample: Lab ID: 032 Collected: 06/16/14 13:52 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 9.9 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 17: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 17: Benzene ND ug/kg /17/14 07:49 06/19/14 17: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 17: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 17: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 17: Bromoform ND ug/kg /17/14 07:49 06/19/14 17: Bromomethane ND ug/kg /17/14 07:49 06/19/14 17: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 17: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 17: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: Chloroethane ND ug/kg /17/14 07:49 06/19/14 17: Chloroform ND ug/kg /17/14 07:49 06/19/14 17: Chloromethane ND ug/kg /17/14 07:49 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 17: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 17: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 17: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 17: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 17: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 17: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 17: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 70 of 93

145 Sample: Lab ID: 032 Collected: 06/16/14 13:52 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 17: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 17: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 17: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 17: Naphthalene ND ug/kg /17/14 07:49 06/19/14 17: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Styrene ND ug/kg /17/14 07:49 06/19/14 17: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 17: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 17: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 17: Toluene ND ug/kg /17/14 07:49 06/19/14 17: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 17: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 17: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 17: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 17: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 17: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 17: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 17: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 17: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 17: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /17/14 07:49 06/19/14 17: Toluene-d8 (S) 105 % /17/14 07:49 06/19/14 17: Bromofluorobenzene (S) 111 % /17/14 07:49 06/19/14 17: Date: 06/25/ :55 PM without the written consent of. Page 71 of 93

146 Sample: Lab ID: 033 Collected: 06/16/14 13:54 Received: 06/16/14 15:45 Matrix: Solid Dry Weight Analytical Method: ASTM D2974 Percent Moisture 9.5 % /17/14 00:00 Acetone ND ug/kg /17/14 07:49 06/19/14 18: Allyl chloride ND ug/kg /17/14 07:49 06/19/14 18: Benzene ND ug/kg /17/14 07:49 06/19/14 18: Bromobenzene ND ug/kg /17/14 07:49 06/19/14 18: Bromochloromethane ND ug/kg /17/14 07:49 06/19/14 18: Bromodichloromethane ND ug/kg /17/14 07:49 06/19/14 18: Bromoform ND ug/kg /17/14 07:49 06/19/14 18: Bromomethane ND ug/kg /17/14 07:49 06/19/14 18: Butanone (MEK) ND ug/kg /17/14 07:49 06/19/14 18: n-butylbenzene ND ug/kg /17/14 07:49 06/19/14 18: sec-butylbenzene ND ug/kg /17/14 07:49 06/19/14 18: tert-butylbenzene ND ug/kg /17/14 07:49 06/19/14 18: Carbon tetrachloride ND ug/kg /17/14 07:49 06/19/14 18: Chlorobenzene ND ug/kg /17/14 07:49 06/19/14 18: Chloroethane ND ug/kg /17/14 07:49 06/19/14 18: Chloroform ND ug/kg /17/14 07:49 06/19/14 18: Chloromethane ND ug/kg /17/14 07:49 06/19/14 18: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 18: Chlorotoluene ND ug/kg /17/14 07:49 06/19/14 18: ,2-Dibromo-3-chloropropane ND ug/kg /17/14 07:49 06/19/14 18: Dibromochloromethane ND ug/kg /17/14 07:49 06/19/14 18: ,2-Dibromoethane (EDB) ND ug/kg /17/14 07:49 06/19/14 18: Dibromomethane ND ug/kg /17/14 07:49 06/19/14 18: ,2-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 18: ,3-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 18: ,4-Dichlorobenzene ND ug/kg /17/14 07:49 06/19/14 18: Dichlorodifluoromethane ND ug/kg /17/14 07:49 06/19/14 18: ,1-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 18: ,2-Dichloroethane ND ug/kg /17/14 07:49 06/19/14 18: ,1-Dichloroethene ND ug/kg /17/14 07:49 06/19/14 18: cis-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 18: trans-1,2-dichloroethene ND ug/kg /17/14 07:49 06/19/14 18: Dichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 18: ,3-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 18: ,2-Dichloropropane ND ug/kg /17/14 07:49 06/19/14 18: ,1-Dichloropropene ND ug/kg /17/14 07:49 06/19/14 18: cis-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 18: trans-1,3-dichloropropene ND ug/kg /17/14 07:49 06/19/14 18: Diethyl ether (Ethyl ether) ND ug/kg /17/14 07:49 06/19/14 18: Ethylbenzene ND ug/kg /17/14 07:49 06/19/14 18: Hexachloro-1,3-butadiene ND ug/kg /17/14 07:49 06/19/14 18: Isopropylbenzene (Cumene) ND ug/kg /17/14 07:49 06/19/14 18: Date: 06/25/ :55 PM without the written consent of. Page 72 of 93

147 Sample: Lab ID: 033 Collected: 06/16/14 13:54 Received: 06/16/14 15:45 Matrix: Solid p-isopropyltoluene ND ug/kg /17/14 07:49 06/19/14 18: Methylene Chloride ND ug/kg /17/14 07:49 06/19/14 18: Methyl-2-pentanone (MIBK) ND ug/kg /17/14 07:49 06/19/14 18: Methyl-tert-butyl ether ND ug/kg /17/14 07:49 06/19/14 18: Naphthalene ND ug/kg /17/14 07:49 06/19/14 18: n-propylbenzene ND ug/kg /17/14 07:49 06/19/14 18: Styrene ND ug/kg /17/14 07:49 06/19/14 18: ,1,1,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 18: ,1,2,2-Tetrachloroethane ND ug/kg /17/14 07:49 06/19/14 18: Tetrachloroethene ND ug/kg /17/14 07:49 06/19/14 18: Tetrahydrofuran ND ug/kg /17/14 07:49 06/19/14 18: Toluene ND ug/kg /17/14 07:49 06/19/14 18: ,2,3-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 18: ,2,4-Trichlorobenzene ND ug/kg /17/14 07:49 06/19/14 18: ,1,1-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 18: ,1,2-Trichloroethane ND ug/kg /17/14 07:49 06/19/14 18: Trichloroethene ND ug/kg /17/14 07:49 06/19/14 18: Trichlorofluoromethane ND ug/kg /17/14 07:49 06/19/14 18: ,2,3-Trichloropropane ND ug/kg /17/14 07:49 06/19/14 18: ,1,2-Trichlorotrifluoroethane ND ug/kg /17/14 07:49 06/19/14 18: ,2,4-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 18: ,3,5-Trimethylbenzene ND ug/kg /17/14 07:49 06/19/14 18: Vinyl chloride ND ug/kg /17/14 07:49 06/19/14 18: Xylene (Total) ND ug/kg /17/14 07:49 06/19/14 18: Surrogates 1,2-Dichloroethane-d4 (S) 103 % /17/14 07:49 06/19/14 18: Toluene-d8 (S) 102 % /17/14 07:49 06/19/14 18: Bromofluorobenzene (S) 107 % /17/14 07:49 06/19/14 18: Date: 06/25/ :55 PM without the written consent of. Page 73 of 93

148 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MPRP/46680 ASTM D2974 Analysis Method: Analysis Description: ASTM D2974 Dry Weight/Percent Moisture Associated Lab Samples: 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012, 013, 014, 015, 016, 017, 018, 019, 020 SAMPLE DUPLICATE: Parameter Units 001 Result Dup Result Percent Moisture % RPD Max RPD Qualifiers SAMPLE DUPLICATE: Parameter Units 020 Result Dup Result Percent Moisture % RPD Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 74 of 93

149 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MPRP/46683 ASTM D2974 Analysis Method: Analysis Description: ASTM D2974 Dry Weight/Percent Moisture Associated Lab Samples: 021, 022, 023, 024, 025, 026, 027, 028, 029, 030, 031, 032, 033 SAMPLE DUPLICATE: Parameter Units 027 Result Dup Result Percent Moisture % RPD Max RPD Qualifiers SAMPLE DUPLICATE: Parameter Units 029 Result Dup Result Percent Moisture % RPD Max RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 75 of 93

150 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MSV/27468 EPA 8260 Analysis Method: Analysis Description: EPA 8260 Associated Lab Samples: 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012, 013, 014, 015, 016, 017, 018, 027 METHOD BLANK: Matrix: Solid Associated Lab Samples: 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012, 013, 014, 015, 016, 017, 018, 027 Parameter Units Blank Result Reporting Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND /18/14 13:34 1,1,1-Trichloroethane ug/kg ND /18/14 13:34 1,1,2,2-Tetrachloroethane ug/kg ND /18/14 13:34 1,1,2-Trichloroethane ug/kg ND /18/14 13:34 1,1,2-Trichlorotrifluoroethane ug/kg ND /18/14 13:34 1,1-Dichloroethane ug/kg ND /18/14 13:34 1,1-Dichloroethene ug/kg ND /18/14 13:34 1,1-Dichloropropene ug/kg ND /18/14 13:34 1,2,3-Trichlorobenzene ug/kg ND /18/14 13:34 1,2,3-Trichloropropane ug/kg ND /18/14 13:34 1,2,4-Trichlorobenzene ug/kg ND /18/14 13:34 1,2,4-Trimethylbenzene ug/kg ND /18/14 13:34 1,2-Dibromo-3-chloropropane ug/kg ND /18/14 13:34 1,2-Dibromoethane (EDB) ug/kg ND /18/14 13:34 1,2-Dichlorobenzene ug/kg ND /18/14 13:34 1,2-Dichloroethane ug/kg ND /18/14 13:34 1,2-Dichloropropane ug/kg ND /18/14 13:34 1,3,5-Trimethylbenzene ug/kg ND /18/14 13:34 1,3-Dichlorobenzene ug/kg ND /18/14 13:34 1,3-Dichloropropane ug/kg ND /18/14 13:34 1,4-Dichlorobenzene ug/kg ND /18/14 13:34 2,2-Dichloropropane ug/kg ND /18/14 13:34 2-Butanone (MEK) ug/kg ND /18/14 13:34 2-Chlorotoluene ug/kg ND /18/14 13:34 4-Chlorotoluene ug/kg ND /18/14 13:34 4-Methyl-2-pentanone (MIBK) ug/kg ND /18/14 13:34 Acetone ug/kg ND /18/14 13:34 Allyl chloride ug/kg ND /18/14 13:34 Benzene ug/kg ND /18/14 13:34 Bromobenzene ug/kg ND /18/14 13:34 Bromochloromethane ug/kg ND /18/14 13:34 Bromodichloromethane ug/kg ND /18/14 13:34 Bromoform ug/kg ND /18/14 13:34 Bromomethane ug/kg ND /18/14 13:34 Carbon tetrachloride ug/kg ND /18/14 13:34 Chlorobenzene ug/kg ND /18/14 13:34 Chloroethane ug/kg ND /18/14 13:34 Chloroform ug/kg ND /18/14 13:34 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 76 of 93

151 #=QC# QUALITY CONTROL DATA METHOD BLANK: Matrix: Solid Associated Lab Samples: 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012, 013, 014, 015, 016, 017, 018, 027 Parameter Units Blank Result Reporting Limit Analyzed Qualifiers Chloromethane ug/kg ND /18/14 13:34 cis-1,2-dichloroethene ug/kg ND /18/14 13:34 cis-1,3-dichloropropene ug/kg ND /18/14 13:34 Dibromochloromethane ug/kg ND /18/14 13:34 Dibromomethane ug/kg ND /18/14 13:34 Dichlorodifluoromethane ug/kg ND /18/14 13:34 Dichlorofluoromethane ug/kg ND /18/14 13:34 Diethyl ether (Ethyl ether) ug/kg ND /18/14 13:34 Ethylbenzene ug/kg ND /18/14 13:34 Hexachloro-1,3-butadiene ug/kg ND /18/14 13:34 Isopropylbenzene (Cumene) ug/kg ND /18/14 13:34 Methyl-tert-butyl ether ug/kg ND /18/14 13:34 Methylene Chloride ug/kg ND /18/14 13:34 n-butylbenzene ug/kg ND /18/14 13:34 n-propylbenzene ug/kg ND /18/14 13:34 Naphthalene ug/kg ND /18/14 13:34 p-isopropyltoluene ug/kg ND /18/14 13:34 sec-butylbenzene ug/kg ND /18/14 13:34 Styrene ug/kg ND /18/14 13:34 tert-butylbenzene ug/kg ND /18/14 13:34 Tetrachloroethene ug/kg ND /18/14 13:34 Tetrahydrofuran ug/kg ND /18/14 13:34 Toluene ug/kg ND /18/14 13:34 trans-1,2-dichloroethene ug/kg ND /18/14 13:34 trans-1,3-dichloropropene ug/kg ND /18/14 13:34 Trichloroethene ug/kg ND /18/14 13:34 Trichlorofluoromethane ug/kg ND /18/14 13:34 Vinyl chloride ug/kg ND /18/14 13:34 Xylene (Total) ug/kg ND /18/14 13:34 1,2-Dichloroethane-d4 (S) % /18/14 13:34 4-Bromofluorobenzene (S) % /18/14 13:34 Toluene-d8 (S) % /18/14 13:34 LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/kg ,1,1-Trichloroethane ug/kg ,1,2,2-Tetrachloroethane ug/kg ,1,2-Trichloroethane ug/kg ,1,2-Trichlorotrifluoroethane ug/kg ,1-Dichloroethane ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 77 of 93

152 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1-Dichloroethene ug/kg ,1-Dichloropropene ug/kg ,2,3-Trichlorobenzene ug/kg ,2,3-Trichloropropane ug/kg ,2,4-Trichlorobenzene ug/kg ,2,4-Trimethylbenzene ug/kg ,2-Dibromo-3-chloropropane ug/kg ,2-Dibromoethane (EDB) ug/kg ,2-Dichlorobenzene ug/kg ,2-Dichloroethane ug/kg ,2-Dichloropropane ug/kg ,3,5-Trimethylbenzene ug/kg ,3-Dichlorobenzene ug/kg ,3-Dichloropropane ug/kg ,4-Dichlorobenzene ug/kg ,2-Dichloropropane ug/kg Butanone (MEK) ug/kg Chlorotoluene ug/kg Chlorotoluene ug/kg Methyl-2-pentanone (MIBK) ug/kg Acetone ug/kg Allyl chloride ug/kg Benzene ug/kg Bromobenzene ug/kg Bromochloromethane ug/kg Bromodichloromethane ug/kg Bromoform ug/kg Bromomethane ug/kg Carbon tetrachloride ug/kg Chlorobenzene ug/kg Chloroethane ug/kg Chloroform ug/kg Chloromethane ug/kg cis-1,2-dichloroethene ug/kg cis-1,3-dichloropropene ug/kg Dibromochloromethane ug/kg Dibromomethane ug/kg Dichlorodifluoromethane ug/kg Dichlorofluoromethane ug/kg Diethyl ether (Ethyl ether) ug/kg L0 Ethylbenzene ug/kg Hexachloro-1,3-butadiene ug/kg Isopropylbenzene (Cumene) ug/kg Methyl-tert-butyl ether ug/kg Methylene Chloride ug/kg n-butylbenzene ug/kg n-propylbenzene ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 78 of 93

153 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Naphthalene ug/kg p-isopropyltoluene ug/kg sec-butylbenzene ug/kg Styrene ug/kg tert-butylbenzene ug/kg Tetrachloroethene ug/kg Tetrahydrofuran ug/kg Toluene ug/kg trans-1,2-dichloroethene ug/kg trans-1,3-dichloropropene ug/kg Trichloroethene ug/kg Trichlorofluoromethane ug/kg Vinyl chloride ug/kg Xylene (Total) ug/kg ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS 027 Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,1,1,2-Tetrachloroethane ug/kg ND ,1,1-Trichloroethane ug/kg ND ,1,2,2-Tetrachloroethane ug/kg ND ,1,2-Trichloroethane ug/kg ND ,1,2-Trichlorotrifluoroethane ug/kg ND ,1-Dichloroethane ug/kg ND ,1-Dichloroethene ug/kg ND ,1-Dichloropropene ug/kg ND ,2,3-Trichlorobenzene ug/kg ND ,2,3-Trichloropropane ug/kg ND ,2,4-Trichlorobenzene ug/kg ND ,2,4-Trimethylbenzene ug/kg ND ,2-Dibromo-3-chloropropane ug/kg ND ,2-Dibromoethane (EDB) ug/kg ND ,2-Dichlorobenzene ug/kg ND ,2-Dichloroethane ug/kg ND ,2-Dichloropropane ug/kg ND ,3,5-Trimethylbenzene ug/kg ND ,3-Dichlorobenzene ug/kg ND ,3-Dichloropropane ug/kg ND ,4-Dichlorobenzene ug/kg ND ,2-Dichloropropane ug/kg ND Butanone (MEK) ug/kg ND Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 79 of 93

154 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS 027 Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD 2-Chlorotoluene ug/kg ND Chlorotoluene ug/kg ND Methyl-2-pentanone (MIBK) ug/kg ND Acetone ug/kg ND M1 Allyl chloride ug/kg ND Benzene ug/kg ND Bromobenzene ug/kg ND Bromochloromethane ug/kg ND Bromodichloromethane ug/kg ND Bromoform ug/kg ND Bromomethane ug/kg ND Carbon tetrachloride ug/kg ND Chlorobenzene ug/kg ND Chloroethane ug/kg ND Chloroform ug/kg ND Chloromethane ug/kg ND cis-1,2-dichloroethene ug/kg ND cis-1,3-dichloropropene ug/kg ND Dibromochloromethane ug/kg ND Dibromomethane ug/kg ND Dichlorodifluoromethane ug/kg ND Dichlorofluoromethane ug/kg ND Diethyl ether (Ethyl ether) ug/kg ND M0 Ethylbenzene ug/kg ND Hexachloro-1,3-butadiene ug/kg ND Isopropylbenzene (Cumene) ug/kg ND Methyl-tert-butyl ether ug/kg ND Methylene Chloride ug/kg ND n-butylbenzene ug/kg ND n-propylbenzene ug/kg ND Naphthalene ug/kg ND p-isopropyltoluene ug/kg ND sec-butylbenzene ug/kg ND Styrene ug/kg ND tert-butylbenzene ug/kg ND Tetrachloroethene ug/kg ND Tetrahydrofuran ug/kg ND Toluene ug/kg ND trans-1,2-dichloroethene ug/kg ND trans-1,3-dichloropropene ug/kg ND Trichloroethene ug/kg ND Trichlorofluoromethane ug/kg ND Vinyl chloride ug/kg ND Xylene (Total) ug/kg ND ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Qual Date: 06/25/ :55 PM without the written consent of. Page 80 of 93

155 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS 027 Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Toluene-d8 (S) % Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 81 of 93

156 #=QC# QUALITY CONTROL DATA QC Batch: QC Batch Method: MSV/27486 EPA 8260 Analysis Method: Analysis Description: EPA 8260 Associated Lab Samples: 019, 020, 021, 022, 023, 024, 025, 026, 028, 029, 030, 031, 032, 033 METHOD BLANK: Matrix: Solid Associated Lab Samples: 019, 020, 021, 022, 023, 024, 025, 026, 028, 029, 030, 031, 032, 033 Parameter Units Blank Result Reporting Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND /19/14 13:57 1,1,1-Trichloroethane ug/kg ND /19/14 13:57 1,1,2,2-Tetrachloroethane ug/kg ND /19/14 13:57 1,1,2-Trichloroethane ug/kg ND /19/14 13:57 1,1,2-Trichlorotrifluoroethane ug/kg ND /19/14 13:57 1,1-Dichloroethane ug/kg ND /19/14 13:57 1,1-Dichloroethene ug/kg ND /19/14 13:57 1,1-Dichloropropene ug/kg ND /19/14 13:57 1,2,3-Trichlorobenzene ug/kg ND /19/14 13:57 1,2,3-Trichloropropane ug/kg ND /19/14 13:57 1,2,4-Trichlorobenzene ug/kg ND /19/14 13:57 1,2,4-Trimethylbenzene ug/kg ND /19/14 13:57 1,2-Dibromo-3-chloropropane ug/kg ND /19/14 13:57 1,2-Dibromoethane (EDB) ug/kg ND /19/14 13:57 1,2-Dichlorobenzene ug/kg ND /19/14 13:57 1,2-Dichloroethane ug/kg ND /19/14 13:57 1,2-Dichloropropane ug/kg ND /19/14 13:57 1,3,5-Trimethylbenzene ug/kg ND /19/14 13:57 1,3-Dichlorobenzene ug/kg ND /19/14 13:57 1,3-Dichloropropane ug/kg ND /19/14 13:57 1,4-Dichlorobenzene ug/kg ND /19/14 13:57 2,2-Dichloropropane ug/kg ND /19/14 13:57 2-Butanone (MEK) ug/kg ND /19/14 13:57 2-Chlorotoluene ug/kg ND /19/14 13:57 4-Chlorotoluene ug/kg ND /19/14 13:57 4-Methyl-2-pentanone (MIBK) ug/kg ND /19/14 13:57 Acetone ug/kg ND /19/14 13:57 Allyl chloride ug/kg ND /19/14 13:57 Benzene ug/kg ND /19/14 13:57 Bromobenzene ug/kg ND /19/14 13:57 Bromochloromethane ug/kg ND /19/14 13:57 Bromodichloromethane ug/kg ND /19/14 13:57 Bromoform ug/kg ND /19/14 13:57 Bromomethane ug/kg ND /19/14 13:57 Carbon tetrachloride ug/kg ND /19/14 13:57 Chlorobenzene ug/kg ND /19/14 13:57 Chloroethane ug/kg ND /19/14 13:57 Chloroform ug/kg ND /19/14 13:57 Chloromethane ug/kg ND /19/14 13:57 cis-1,2-dichloroethene ug/kg ND /19/14 13:57 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 82 of 93

157 #=QC# QUALITY CONTROL DATA METHOD BLANK: Matrix: Solid Associated Lab Samples: 019, 020, 021, 022, 023, 024, 025, 026, 028, 029, 030, 031, 032, 033 Parameter Units Blank Result Reporting Limit Analyzed Qualifiers cis-1,3-dichloropropene ug/kg ND /19/14 13:57 Dibromochloromethane ug/kg ND /19/14 13:57 Dibromomethane ug/kg ND /19/14 13:57 Dichlorodifluoromethane ug/kg ND /19/14 13:57 Dichlorofluoromethane ug/kg ND /19/14 13:57 Diethyl ether (Ethyl ether) ug/kg ND /19/14 13:57 Ethylbenzene ug/kg ND /19/14 13:57 Hexachloro-1,3-butadiene ug/kg ND /19/14 13:57 Isopropylbenzene (Cumene) ug/kg ND /19/14 13:57 Methyl-tert-butyl ether ug/kg ND /19/14 13:57 Methylene Chloride ug/kg ND /19/14 13:57 n-butylbenzene ug/kg ND /19/14 13:57 n-propylbenzene ug/kg ND /19/14 13:57 Naphthalene ug/kg ND /19/14 13:57 p-isopropyltoluene ug/kg ND /19/14 13:57 sec-butylbenzene ug/kg ND /19/14 13:57 Styrene ug/kg ND /19/14 13:57 tert-butylbenzene ug/kg ND /19/14 13:57 Tetrachloroethene ug/kg ND /19/14 13:57 Tetrahydrofuran ug/kg ND /19/14 13:57 Toluene ug/kg ND /19/14 13:57 trans-1,2-dichloroethene ug/kg ND /19/14 13:57 trans-1,3-dichloropropene ug/kg ND /19/14 13:57 Trichloroethene ug/kg ND /19/14 13:57 Trichlorofluoromethane ug/kg ND /19/14 13:57 Vinyl chloride ug/kg ND /19/14 13:57 Xylene (Total) ug/kg ND /19/14 13:57 1,2-Dichloroethane-d4 (S) % /19/14 13:57 4-Bromofluorobenzene (S) % /19/14 13:57 Toluene-d8 (S) % /19/14 13:57 LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/kg ,1,1-Trichloroethane ug/kg ,1,2,2-Tetrachloroethane ug/kg ,1,2-Trichloroethane ug/kg ,1,2-Trichlorotrifluoroethane ug/kg ,1-Dichloroethane ug/kg ,1-Dichloroethene ug/kg ,1-Dichloropropene ug/kg ,2,3-Trichlorobenzene ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 83 of 93

158 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,3-Trichloropropane ug/kg ,2,4-Trichlorobenzene ug/kg ,2,4-Trimethylbenzene ug/kg ,2-Dibromo-3-chloropropane ug/kg ,2-Dibromoethane (EDB) ug/kg ,2-Dichlorobenzene ug/kg ,2-Dichloroethane ug/kg ,2-Dichloropropane ug/kg ,3,5-Trimethylbenzene ug/kg ,3-Dichlorobenzene ug/kg ,3-Dichloropropane ug/kg ,4-Dichlorobenzene ug/kg ,2-Dichloropropane ug/kg Butanone (MEK) ug/kg Chlorotoluene ug/kg Chlorotoluene ug/kg Methyl-2-pentanone (MIBK) ug/kg Acetone ug/kg Allyl chloride ug/kg Benzene ug/kg Bromobenzene ug/kg Bromochloromethane ug/kg Bromodichloromethane ug/kg Bromoform ug/kg Bromomethane ug/kg Carbon tetrachloride ug/kg Chlorobenzene ug/kg Chloroethane ug/kg Chloroform ug/kg Chloromethane ug/kg cis-1,2-dichloroethene ug/kg cis-1,3-dichloropropene ug/kg Dibromochloromethane ug/kg Dibromomethane ug/kg Dichlorodifluoromethane ug/kg Dichlorofluoromethane ug/kg Diethyl ether (Ethyl ether) ug/kg L3 Ethylbenzene ug/kg Hexachloro-1,3-butadiene ug/kg Isopropylbenzene (Cumene) ug/kg Methyl-tert-butyl ether ug/kg Methylene Chloride ug/kg n-butylbenzene ug/kg n-propylbenzene ug/kg Naphthalene ug/kg p-isopropyltoluene ug/kg sec-butylbenzene ug/kg Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 84 of 93

159 #=QC# QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Styrene ug/kg tert-butylbenzene ug/kg Tetrachloroethene ug/kg Tetrahydrofuran ug/kg Toluene ug/kg trans-1,2-dichloroethene ug/kg trans-1,3-dichloropropene ug/kg Trichloroethene ug/kg Trichlorofluoromethane ug/kg Vinyl chloride ug/kg Xylene (Total) ug/kg ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS 029 Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,1,1,2-Tetrachloroethane ug/kg ND ,1,1-Trichloroethane ug/kg ND ,1,2,2-Tetrachloroethane ug/kg ND ,1,2-Trichloroethane ug/kg ND ,1,2-Trichlorotrifluoroethane ug/kg ND ,1-Dichloroethane ug/kg ND ,1-Dichloroethene ug/kg ND ,1-Dichloropropene ug/kg ND ,2,3-Trichlorobenzene ug/kg ND ,2,3-Trichloropropane ug/kg ND ,2,4-Trichlorobenzene ug/kg ND ,2,4-Trimethylbenzene ug/kg ND ,2-Dibromo-3-chloropropane ug/kg ND ,2-Dibromoethane (EDB) ug/kg ND ,2-Dichlorobenzene ug/kg ND ,2-Dichloroethane ug/kg ND ,2-Dichloropropane ug/kg ND ,3,5-Trimethylbenzene ug/kg ND ,3-Dichlorobenzene ug/kg ND ,3-Dichloropropane ug/kg ND ,4-Dichlorobenzene ug/kg ND ,2-Dichloropropane ug/kg ND Butanone (MEK) ug/kg ND Chlorotoluene ug/kg ND Chlorotoluene ug/kg ND Methyl-2-pentanone (MIBK) ug/kg ND Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 85 of 93

160 #=QC# QUALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS 029 Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Acetone ug/kg ND M1 Allyl chloride ug/kg ND Benzene ug/kg ND Bromobenzene ug/kg ND Bromochloromethane ug/kg ND Bromodichloromethane ug/kg ND Bromoform ug/kg ND Bromomethane ug/kg ND Carbon tetrachloride ug/kg ND Chlorobenzene ug/kg ND Chloroethane ug/kg ND Chloroform ug/kg ND Chloromethane ug/kg ND cis-1,2-dichloroethene ug/kg ND cis-1,3-dichloropropene ug/kg ND Dibromochloromethane ug/kg ND Dibromomethane ug/kg ND Dichlorodifluoromethane ug/kg ND Dichlorofluoromethane ug/kg ND Diethyl ether (Ethyl ether) ug/kg ND Ethylbenzene ug/kg ND Hexachloro-1,3-butadiene ug/kg ND Isopropylbenzene (Cumene) ug/kg ND Methyl-tert-butyl ether ug/kg ND Methylene Chloride ug/kg ND n-butylbenzene ug/kg ND n-propylbenzene ug/kg ND Naphthalene ug/kg ND p-isopropyltoluene ug/kg ND sec-butylbenzene ug/kg ND Styrene ug/kg ND tert-butylbenzene ug/kg ND Tetrachloroethene ug/kg ND Tetrahydrofuran ug/kg ND Toluene ug/kg ND trans-1,2-dichloroethene ug/kg ND trans-1,3-dichloropropene ug/kg ND Trichloroethene ug/kg ND Trichlorofluoromethane ug/kg ND Vinyl chloride ug/kg ND Xylene (Total) ug/kg ND ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 06/25/ :55 PM without the written consent of. Page 86 of 93

161 #=QL# QUALIFIERS DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-M Pace Analytical Services - Minneapolis ANALYTE QUALIFIERS L0 L3 M0 M1 Analyte recovery in the laboratory control sample (LCS) was outside QC limits. Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias. Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Date: 06/25/ :55 PM without the written consent of. Page 87 of 93

162 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ DUP-3 ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ MS/MSD ASTM D2974 MPRP/ DUP-5 ASTM D2974 MPRP/ MS/MSD ASTM D2974 MPRP/ DUP-2 ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ ASTM D2974 MPRP/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ DUP-3 EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/27468 Date: 06/25/ :55 PM without the written consent of. Page 88 of 93

163 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ MS/MSD EPA 5035A MSV/27448 EPA 8260 MSV/ DUP-5 EPA 5035A MSV/27448 EPA 8260 MSV/ MS/MSD EPA 5035A MSV/27448 EPA 8260 MSV/ DUP-2 EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/ EPA 5035A MSV/27448 EPA 8260 MSV/27486 Date: 06/25/ :55 PM without the written consent of. Page 89 of 93

164 Page 90 of 93

165 Page 91 of 93

166 Page 92 of 93